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Bruker Anton Paar User Manual

Bruker Anton Paar
136 pages
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Innovation with Integrity
XRD
Anton Paar
Temperature Chambers
for D8 ADVANCE / D8 DISCOVER
User Manual
Original Instructions (English)

Table of Contents

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Bruker Anton Paar Specifications

General IconGeneral
BrandBruker
ModelAnton Paar
CategoryLaboratory Equipment
LanguageEnglish

Summary

Safety Guidelines

About this Manual

Provides general information and guidelines for safe operation and product protection.

Qualified Personnel

Specifies requirements for personnel authorized to set up, operate, maintain, and repair the equipment.

Correct and Intended Usage

Defines proper use of the device and its components, and consequences of improper use.

Disclaimer and Liability

Outlines limitations of the manual's agreement with hardware/software and welcomes suggestions.

General Safety Precautions

Warns about extreme temperatures and touching internal components or sample holder.

Signage

Explains symbols and information signs found on the instrument for safety.

General Remarks

Heating Principles

Categorizes heating/cooling devices and describes features of direct heaters.

Temperature Measurement and Calibration

Discusses methods and sensors for temperature measurement.

Temperature Measurement

Details temperature sensor types (Si-diodes, Pt100, Thermocouples) used for different ranges.

Temperature Calibration

Explains methods to eliminate errors by using standards like MgO or phase transitions.

Temperature Calibration by Thermal Expansion of MgO (Periclase)

Describes using MgO as a calibration standard based on its thermal expansion coefficient.

Temperature Calibration by Phase Transitions

Lists samples with structural phase transitions useful for temperature calibration.

Vacuum Equipment

Installation of the Edwards High Vacuum Stage with TIC

Details the installation of the Edwards turbomolecular pump and its components.

Mounting of the Edwards High Vacuum Stage

Step-by-step guide for connecting vacuum tubes and mounting the pump.

Operation of the Edwards High Vacuum Stage

Instructions for operating the Turbo Instrument Controller (TIC) for vacuum stage control.

Installation of the Edwards Backing-Pump

Describes the installation of an Edwards backing pump for lower vacuum applications.

Adjustment of a Chamber on the D8

Adjustment Procedures

General alignment procedures for Anton Paar chambers on the D8 goniometer.

Adjustment Procedure with Alignment Slit

Step-by-step guide for chamber alignment using a dedicated alignment slit.

Alternative Procedure Without Alignment Slit

Procedure for chamber alignment when no specific alignment slit is available.

Using Automated Height Correction

Details how to implement automated height correction for thermal expansion.

Mounting the Temperature Controller into the D8 Enclosure

Installation and Operation of the HTK-Series, TTK 600, XRK 900, and HPC 900 Chambers

Introduction

Overview of Anton Paar temperature chambers and their operational similarities.

Mounting the Chamber to the Goniometer

Describes the procedure for mounting various Anton Paar chambers onto the goniometer.

Temperature Controllers for Anton Paar Chambers

Introduces TCU and CCU series temperature controllers for Anton Paar chambers.

Connecting the TCU Controller

Details the physical serial line connections for the TCU controller.

Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER

Guidance on configuring chambers within the DIFFRAC.MEASUREMENT CENTER software.

Operation

Provides operational notes, including warnings for heater shielding and vacuum requirements.

Alignment

Refers to the general alignment method described in 'Adjustment of a Chamber on the D8'.

Installation and Operation of the CHC plus Humidity Chamber

Introduction

Describes the CHC plus chamber's capabilities for humidification and temperature control.

Mounting the Chamber to the Goniometer

Explains that mounting is similar to other chambers, referring to chapter 5.

Temperature Controllers and Water Circuit for CHC plus

Details the TCU/CCU controllers and water bath required for CHC plus operation.

Connecting the CCU Controller

Describes the serial line connections for the CCU controller to the Universal IO-Board.

Connecting the MHG for CHC plus

Details the connections for the MHG (Modular Humidity Generator) controller.

Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER

Guidance on configuring the CHC plus chamber in the measurement software.

Operation

Provides operational notes, including vacuum and inert gas requirements.

Alignment

Refers to the general alignment method described in 'Adjustment of a Chamber on the D8'.

Installation and Operation of the DCS 350 and DHS 1100 Chambers

Introduction

Introduces the DCS 350 (Cooling Stage) and DHS 1100 (Hot Stage) chambers.

Mounting the Chamber to the Goniometer

Describes the mounting procedure for DCS 350 and DHS 1100 stages onto the goniometer.

Temperature Controllers DC S350 and DHS 1100

Identifies TCU and CCU controllers used with DCS 350 and DHS 1100 chambers.

Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER

Guidance on configuring DCS 350 and DHS 1100 chambers in the measurement software.

Operation

Basic operation steps for the DCS 350 and DHS 1100 chambers.

Activating the Chamber in DA VINCI

Manual activation procedure for domed stages within the DA VINCI software.

Alignment

Describes alignment for domed stages, differing slightly from standard stages.

Aligning the Chamber for Automated Height Correction

Procedure for aligning chambers mounted on Eulerian cradles for automated height correction.

Installation and Operation of the BTS 150 and BTS 500 Chambers

Introduction

Introduces the BTS 150/500 as compact XRD non-ambient stages.

Mounting the Chamber to the Goniometer

Details the mounting procedure for BTS 150/500 chambers onto the diffractometer.

USB Connection of the BTS 150/500 to the CPU1 Board

Explains connecting the BTS 150/500 via USB cable to the CPU1 board.

Configuring the Chamber in DIFFRAC.MEASUREMENT CENTER

Guidance on configuring BTS 150/500 chambers in the measurement software.

Operation and Alignment

Refers to operation and alignment procedures described in earlier chapters.

Appendix / Service Details

Vacuum Equipment

Details on vacuum equipment, including programming the Edwards High Vacuum Stage.

Programming of the Edwards High Vacuum Stage

Procedure for resetting the Edwards TIC controller to factory defaults and programming it.

Configuring a Chamber in DIFFRAC.MEASUREMENT CENTER

Procedure for configuring various Anton Paar chambers in the measurement software.

HTK-series, TTK 600, XRK 900, and HPC 900 Chambers

Configuration steps for HTK, TTK, XRK, and HPC chambers in the software.

CHC plus

Configuration details for the CHC plus chamber.

CHC plus with TCU 110 and HE-4 Water Bath

Configuration for CHC plus with TCU 110 controller and HE-4 water bath.

CHC plus with CCU100 and Corio Water Bath

Configuration for CHC plus with CCU100 controller and Corio water bath.

DCS 350 and DHS 1100

Configuration procedure for DCS 350 and DHS 1100 stages.

BTS 150 and BTS 500

Configuration steps for BTS 150 and BTS 500 chambers.

References

Lists the documentation and manuals referenced in this user manual.

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