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Bruker CryoProbe System User Manual
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BRUKER
CryoProbe System
Inst
allation
V
ersion 1
2
Table of Contents
Table of Contents
3
Default Chapter
3
Contents
3
1 Safety
7
Terms and Symbols
7
Disclaimer
8
Emergency
8
Personnel Safety
9
Safety of Cryoprobe Equipment
11
First Aid
11
2 Introduction
13
How to Use this Manual
13
Cryoprobe System Overview
13
Conventions
14
Figure 2.1. the Cryoprobe™ System
14
3 Initial Setup
17
Before Delivery
17
Transport
17
Check the Site Preparations
18
Initial Setup
18
Before You Unpack
19
Unpacking
19
Figure 3.1. Cryoprobe Handling
20
Positioning the Units
21
BCU05 Cooling Test (Optional)
22
Spectrometer Modifications
22
Access to the Magnet Bottom
22
Cranked Magnet Pillar Braces (Optional)
23
Blue Spinning Stator
24
Replacing the Shim System (Optional)
24
Attach the Mounting Hardware
25
Handling
27
Mounting
28
Figure 3.4. Preparing the Mounting Hardware
29
Figure 3.5. Sliding the Cryoprobe into the Magnet
31
Figure 3.6. Cryoprobe and Optional Cranked Pillar Braces
32
Sample Spinning Test
33
Figure 3.7. Final Positioning of the Cryoprobe
33
Joining the Cryocoupler
34
Figure 3.8. Unlock the Vaccum Flange Screws
35
Figure 3.9. O-Rings on the Cryocoupler
35
Figure 3.10. Turn the Cryocoupler
36
Figure 3.11. Inserting the Cryocoupler
37
Load Firmware
38
Boot the Cryocontroller
39
Hook up the He Steel-Cylinder
41
Figure 3.12. Attaching the He Hose
42
Interconnect the He Compressor
43
Warning Labels
45
Connecting
46
Figure 3.14. Connecting VT Sensor Cable and VT Hose (Bottom View)
47
Figure 3.15. Open the Cryoprobe Vacuum Plug
48
Power-On
49
VT Setup
50
Figure 3.16. Switching on the He Compressor
50
Initial He Fill
52
Cool-Down
52
Load Additional X WIN - NMR
54
Put HPPR CRP Assembly into Operation
54
How to Proceed
55
4 Customizing the Cryoprobe System
57
Experimental Parameters
57
Lock Power
57
RF Power Levels
57
Safety Attenuators
57
Sample Temperature Control
57
Standard Parameter Sets
57
Receiver Sensitivity
58
Sample Tubes and Spinners
58
Acceptance Tests
58
User Training
58
5 Troubleshooting
59
Fuses and Reset Buttons
59
General Failure
60
No Mains
60
Spinning Problems
60
Cryocontroller Failure
61
Indicator on Cryoprobe Sticks out
61
Leak in He Supply
62
Cool-Down Problems
62
COOL down Command Is Ignored
62
Insufficient Vacuum
62
He Compressor Does Not Run
63
Periodic Hiss Is Missing
65
Cool-Down Doesn't Reach Cold State
66
How to Open the Cryocooling Unit
67
Refill He
67
6 Relocation of a Cryoplatform
69
Relocation
69
Cryoprobe System Storage
69
Disposal
69
Figure 6.1. Releasing the Gas from the Cryocooling Unit
70
Pressure Release
70
Toxic Materials
70
7 Bruker Contact
73
Cryoprobe Information
73
Cryoprobe Service
73
Check Lists
75
Site Preparation Checks
75
Preparations for the Installation Visit
75
User Training
76
Related Documents
79
Figure A.1. When to Use Which Cryoprobe Document
80
Conversion of Metric Units
81
Conversion of Metric Units
82
Glossary
83
Figures
89
Tables
91
4
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Bruker CryoProbe System Specifications
General
Brand
Bruker
Model
CryoProbe System
Category
Laboratory Equipment
Language
English
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