Bruker CryoProbe System User Manual

BRUKER
CryoProbe System
Installation
Version 1

Bruker CryoProbe System Specifications

General

Application	NMR spectroscopy
Technology	Cryogenic cooling
Compatibility	Bruker NMR spectrometers
Target Nuclei	1H, 13C, 15N
Temperature Range	Approx. 20K
Probe Type	Triple resonance
Sample Spinning	Yes
Automatic Tuning and Matching	Yes

Summary

Safety

Terms and Safety Symbols

Defines warning symbols and terms used for safe operation of the CryoProbe System.

Personnel and Equipment Safety

Covers safety guidelines for personnel and specific precautions for the CryoProbe equipment.

Emergency Procedures and First Aid

Outlines emergency shutdown, first aid measures, and disclaimer information.

Introduction to the CryoProbe System

Manual Usage and System Overview

Explains manual navigation and provides a general overview of the CryoProbe System's components.

Conventions and Related Documentation

Details text conventions and lists related documents for system operation.

Initial Setup and Installation

Site Preparation and Delivery Procedures

Covers site requirements, checks, and delivery procedures before installation.

Component Positioning and Magnet Modifications

Guides on unit placement, magnet modifications, and optional tests for installation.

CryoProbe Handling and Mounting

Step-by-step instructions for safely handling and mounting the CryoProbe into the magnet.

System Connections and Power-on

Details connecting He, power, and other system components, followed by initial power-up.

VT Setup, Cool-down, and Software

Explains VT setup, He fill, system cool-down, and software installation steps.

System Customization and Testing

Experimental Parameter Configuration

Discusses adjusting experimental parameters like RF power and sample temperature for optimal performance.

Acceptance Tests and User Training

Covers final system acceptance tests and essential user training topics.

Troubleshooting and Maintenance

Component Checks and General Failures

Guides on checking fuses, reset buttons, and diagnosing general system failures.

Cool-down, Compressor, and Leak Issues

Addresses problems during cool-down, He supply leaks, and He Compressor operational errors.

System Refill and Unit Access

Details procedures for refilling He and safely opening the CryoCooling Unit for access.

System Relocation and Disposal

Relocation, Storage, and Disposal Procedures

Provides instructions for moving, storing, and disposing of the CryoProbe System components.

Pressure Release and Material Safety

Covers gas pressure release and handling of toxic materials associated with the system.

Bruker Support Information

CryoProbe Sales and General Information

Lists contact details for sales, information, and general inquiries about CryoProbe systems.

CryoProbe Service and Technical Support

Provides contact information for technical service, repair, and support for CryoProbe systems.

Installation Checklists and User Training

Site Preparation Checklist

A comprehensive checklist to ensure all site prerequisites are met before CryoProbe installation.

User Training and Documentation Requirements

Covers essential topics for user familiarization and required documentation for the system.

Related Documents

Conversion of Metric Units

Glossary of Terms