Bruker CryoProbe System User Manual

CryoProbe Installation BRUKER 17 (93)
Initial setup 3
3000000
Before delivery 3.1
0
Before an installation date with B
RUKER is fixed, the customer needs to read the
following remarks and work through the "Site preparation checks" on page 75
for the NMR laboratory.
The checklist "Preparations for the installation visit" on page 75
is intended
for the B
RUKER engineer.
General
All necessary preparations for the CryoProbe System must have been completed
before B
RUKER engineers arrive at the customer site and perform the installation.
B
RUKER personnel will connect all units of a the CryoProbe System as far as re-
quired for test and operation but they will not work on the laboratory infrastructure
(e.g. mount cable channels, fix tubes to the wall, drill holes or the like) to make the
installation ‘look nice’.
NOTE: The spectrometer cannot be used for NMR experiments (with e.g. a con-
ventional setup) during installation and test of the CryoProbe System.
Other laboratory equipment
Other devices in the laboratory may depend on the same supplies as the Cryo-
Probe System, e.g. pneumatic gas and electricity. It must be checked if these de-
vices can continue their operation while the CryoProbe System is hooked up to
the shared supplies.
Reference data
Get a set of reference spectra with a conventional probe to estimate spectrometer
performance and external disturbances. The spectra should be fairly new. Check
e.g. lineshape, sensitivity, water suppression, lock stability spikes and vibrations,
t
1
-noise etc.
NOTE: Sensitivity is the major issue for the CryoProbe and it is influenced by nu-
merous external factors. The CryoProbe cannot reach its specs if any other spec-
trometer component fails to do so!
Transport 3.2
0
The CryoProbe System is shipped in three steps: first a Site Preparation Set con-
taining the He Compressor and some tubes which must be installed by the cus-
tomer in the NMR lab to provide the infrastructure for the CryoProbe System. After
the site preparation work has been completed, CryoCooling Unit and HPPR CRP
are sent off and installed by a B
RUKER engineer. Finally, the CryoProbe is deliv-

Bruker CryoProbe System Specifications

General

Brand	Bruker
Model	CryoProbe System
Category	Laboratory Equipment
Language	English