CryoProbe Installation BRUKER 3 (93)
Contents
Contents ............................................................... 3
1 Safety .................................................................... 7
1.1 Terms and symbols .............................................................. 7
1.2 Disclaimer ........................................................................... 8
1.3 Emergency .......................................................................... 8
1.4 Personnel safety .................................................................. 9
1.5 Safety of CryoProbe equipment ......................................... 11
1.6 First aid ............................................................................. 11
2 Introduction ........................................................ 13
2.1 How to use this manual ..................................................... 13
2.2 CryoProbe System overview .............................................. 13
2.3 Conventions ...................................................................... 14
3 Initial setup ......................................................... 17
3.1 Before delivery .................................................................. 17
3.2 Transport ........................................................................... 17
3.3 Check the site preparations ............................................... 18
3.4 Before you unpack ............................................................. 19
3.5 Unpacking ......................................................................... 19
3.6 Positioning the units .......................................................... 21
3.7 BCU05 cooling test (optional) ............................................ 22
3.8 Spectrometer modifications ............................................... 22
Access to the magnet bottom ........................................ 22
Cranked magnet pillar braces (optional) ........................ 23
Blue spinning stator ...................................................... 24
Replacing the shim system (optional) ............................ 24
Attach the Mounting Hardware ...................................... 25
3.9 Handling ............................................................................ 27
3.10 Mounting ........................................................................... 28
3.11 Sample spinning test ......................................................... 33
3.12 Joining the CryoCoupler .................................................... 34
3.13 Load firmware ................................................................... 38
3.14 Boot the CryoController ..................................................... 39
3.15 Hook up the He steel-cylinder ............................................ 41
3.16 Interconnect the He Compressor ....................................... 43
3.17 Warning labels ................................................................... 45
3.18 Connecting ........................................................................ 46
3.19 Power-on ........................................................................... 49
3.20 VT setup ........................................................................... 50
3.21 Initial He fill ....................................................................... 52
3.22 Cool-down ......................................................................... 52