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Bruker NMR 400 89 Ascend DNP User Manual

Bruker NMR 400 89 Ascend DNP
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43
ZTKS0243 / Z31993 / 03
Troubleshooting
Continued from page before
Indicator Possible reason Solution By
Helium bore tube
and radiation shield
are not concentric.
Alignment rod is
loose or broken.
Replace alignment rod
a
.
Bruker Service
Reduction flange is
not concentric.
Check orientation. Bruker Service
Vacuum Valve
collides with the
magnet stand.
Vacuum Valve
collides with the
magnet stand.
Turn the Vacuum Valve. Be
careful if the RT vessel is
evacuated.
Bruker Service
Vacuum in RT
vessel does not
reach
5 x 10
-5
mbar in
48 hours.
O-rings may be
damaged.
Check and clean O-rings and
slots; replace O-rings if nec-
essary:
of the Vacuum Valve
of the drop-off plate
of the reduction and
sealing flanges
of the bottom plate
a
Bruker Service
Defective pumping
unit or pumping line.
Check pumping unit and
pumping line:
A vacuum less than 10
-6
mbar
must be reached with a
closed sealing plug.
Replace if necessary.
Bruker Service
Room temperature
bore tube has
scratches or dust on
the sealing surfaces.
Check sealing surfaces on the
room temperature bore tube:
No scratches and no dust
should be visible.
Bruker Service
Moisture in the RT
vessel.
Pump and flush the RT vessel
several times with dry
nitrogen gas.
Bruker Service
Super insulation
touches RT vessel or
bore tube or
radiation shield.
Super insulation was
not fixed correctly
during assembly.
Fix super insulation on the
outer radiation shield with
polyester tape
a
. Carefully
prevent any connection
between different vessels or
bore tubes in the cryostat.
Bruker Service
a. For this work the bottom plate has to be removed. Check the suspension tubes of the helium vessel
are not broken. Install the safety device for fall protection (not supplied). Contact Bruker Service for
further information.

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Bruker NMR 400 89 Ascend DNP Specifications

General IconGeneral
BrandBruker
ModelNMR 400 89 Ascend DNP
CategoryLaboratory Equipment
LanguageEnglish

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