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Labconco FreeZone Plus User Manual

Labconco FreeZone Plus
62 pages
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FreeZone
®
Plus
4.5 Liter Cascade
Freeze Dry Systems
Models
7386020 7387020
7386021 7387021
7386030 7387030
7386031 7387031
7386040 7387040
7386041 7387041
Labconco Corporation
8811 Prospect Avenue
Kansas City, MO 64132-2696
800-821-5525, 816-333-8811
FAX 816-363-0130
E-MAIL labconco@labconco.com
HOME PAGE www.labconco.com
To receive important product updates,
complete your product registration card
online at register.labconco.com
User’s Manual
Please read the User’s Manual before operating the equipment.

Table of Contents

Other manuals for Labconco FreeZone Plus

Questions and Answers:

Labconco FreeZone Plus Specifications

General IconGeneral
BrandLabconco
ModelFreeZone Plus
CategoryCommercial Food Equipment
LanguageEnglish

Summary

Chapter 1: Introduction

Freeze Dry Process

Explains the process of removing water or solvent from frozen material via sublimation.

Freeze Dry Rates

Discusses factors affecting freeze-drying efficiency like surface area, thickness, and temperature.

Freeze Dry Capacity

Relates sample volume capacity to factors like surface area and eutectic temperature.

Samples Containing Volatile Substances

Discusses how volatile components affect freeze-drying and sample melt tendency.

Safety Symbols

Explains the meaning and use of safety alert symbols and warning words.

Chapter 2: Prerequisites

Electrical Requirements

Details the electrical specifications needed for installation, including voltage and amperage.

Location Requirements

Specifies the ideal placement for the freeze dryer for proper airflow and cooling.

Vacuum Pump Requirements

Outlines the necessary specifications for the user-provided vacuum pump.

Chamber or Manifold Requirements

Mentions the included 12-port drying chamber and available manifolds.

Chapter 3: Getting Started

Unpacking Your Freeze Dryer

Instructions for carefully unpacking and inspecting the freeze dryer for transit damage.

Freeze Dryer Components

Lists catalog numbers and product descriptions to verify received parts.

Setting Up Your Freeze Dryer

Provides steps for connecting the vacuum pump and electrical supply.

Chemical Resistance of Freeze Dryer Components

Details the resistance of components to various acids, buffers, and solvents.

Solvent Safety Precautions

Advises on safe handling of flammable or hazardous solvents and proper ventilation.

Chapter 4: Using Your Freeze Dryer

Freeze Dryer Controls

Explains the function of each control panel button, switch, and indicator.

Operation Checklist

A step-by-step guide to follow before each use of the freeze dryer.

Vacuum Pump Ballast Setting

Recommends closing the gas ballast during operation to prevent pump damage.

Operating the Freeze Dryer Set-Up

Details how to configure vacuum and temperature units and set operating parameters.

Automatic Start-Up

Describes how to initiate the freeze dry process using the Auto Mode.

Manual Start-Up

Explains how to manually start the refrigeration and vacuum systems.

Setting the Operating Vacuum Level

Provides guidelines for optimizing the vacuum level for different sample types.

Pre-Freezing Samples

Recommends container types and pre-freezing temperatures for samples.

Adding Sample

Outlines the procedure for connecting and using sample valves.

Shut Down

Steps for properly turning off the freeze dryer at the end of a run.

Defrosting

Provides instructions for melting ice from the collector coil.

Alarms

Explains common alarms like Power Failure, Voltage, Temperature, and others.

Chapter 5: Maintaining Your Freeze Dryer

As needed Maintenance

Routine tasks like cleaning spills, checking oil, and cleaning chambers.

Monthly Maintenance

Tasks to perform monthly, such as checking rubber components and cleaning surfaces.

Annually Maintenance

Annual task of cleaning the refrigeration system condenser for optimal airflow.

Front Access Panel Removal (Console Models)

Instructions for removing the front panel on console models for maintenance access.

Chapter 6: Using the RS232 Receptacle

Computer Connection for Computer Interface

Details how to connect the freeze dryer to a computer via the RS232 port.

Chapter 7: Troubleshooting

Vacuum Pump

Steps to diagnose and resolve issues related to the vacuum pump's operation.

Gaskets, Tubing, Connections, Sample Valves

Troubleshooting for leaks and issues with seals, hoses, and valves.

System Components and Collection Chamber Isolation

Tests to isolate leaks within the drying chamber or plumbing.

Refrigeration Module Operation

Addresses potential issues with the refrigeration system's performance.

Chapter 8: Modifying Your Freeze Dryer Display

Temperature and Vacuum Display

How to adjust offsets for temperature and vacuum readings.

Line Voltage Alarm Points

How to modify alarm points for voltage fluctuations.

Moisture Sensor Alarm

Information on disabling the moisture sensor alarm.

Modifying the Display

Steps to enter the production menu and adjust various settings.

Appendix A: Freeze Dryer Components

Models 73860xx and 73870xx

Lists common replacement parts for specific freeze dryer models.

Appendix B: Freeze Dryer Dimensions

Model 73860xx

Provides detailed physical dimensions for the 73860xx benchtop model.

Model 73870xx

Provides detailed physical dimensions for the 73870xx console model.

Appendix C: Freeze Dryer Specifications

Electrical Specifications

Details voltage, frequency, phase, and amperage for various models.

Environmental Conditions

Specifies operating conditions such as altitude, temperature, and humidity.

Wiring Diagram

Provides electrical wiring diagrams for 115V and 230V models.

Appendix D: Freeze Dryer Accessories

Vacuum Pump

Lists available vacuum pumps with specifications and part numbers.

Pump Inlet Filter

Describes filters to protect the vacuum pump from oil back streaming.

Pump Exhaust Filter

Filters designed to remove oil mist and odor from pump exhaust.

Vacuum Pump Oil, 1 Liter

Details the type of oil recommended for vacuum pumps.

Soda Acid Trap

Secondary trap to prevent corrosive chemicals from entering the vacuum pump.

Carbon Solvent Trap

Secondary trap to prevent organic solvents from entering the vacuum pump.

Secondary Vacuum Cold Trap

Trap for processing low eutectic samples, cools to -75°C.

Heated Drying Chamber, 115V

Details the heated drying chamber specifications for 115V.

Product Heater, 115V

Describes the product heater for use in chamber 7522800.

Clear Drying Chamber with 8 Valves

Information on the clear drying chamber for bulk drying or flasks.

Drying Rack- Unheated

Details the unheated drying rack with three shelves.

20 Port Manifold

Specifications for the 20-port manifold with freeze dry valves.

48 Port Ampule Manifold

Details the 48-port ampule manifold with tube stems.

Sample Valve Kit

Kit for sample valves, including body, knob, and parts.

16 Port Drying Chamber

Specifications for the 16-port drying chamber.

Serum Bottles and Vials

Information on serum bottles and vials for sample storage.

Fast-Freeze® Flasks

Describes Fast-Freeze flasks for ease of handling, loading, and lyophilization.

Lyph-Lock® Flasks

Explains Lyph-Lock flasks, their components, and advantages for sample loading.

Ampules

Details Labconco ampules for lyophilization requirements and flame sealing.

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