70
Appendix C: Open Vessel Reactions
5. After completion of the method, permit the vessels to cool in the microwave cavity to 50 °C.
Flask Removal
1. Allow the ask to cool in the microwave to 50 °C.
WARNING
To prevent the possibility of severe burns, ensure that gloves and protective gear as outlined in your safety
program are worn.
2. Remove ber optic probe.
3. If applicable, remove the extension glasswear and condenser.
4. Remove the ask.
5. Proceed with work-up.