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CEM MARS 6 Synthesis User Manual

CEM MARS 6 Synthesis
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MARS 6 Synthesis
Parallel & Scale-Up Microwave Synthesizer
Manual

Table of Contents

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CEM MARS 6 Synthesis Specifications

General IconGeneral
BrandCEM
ModelMARS 6 Synthesis
CategorySynthesizer
LanguageEnglish

Summary

Safety

Safety Notations

Explains the use of three safety alert words (NOTE, CAUTION, WARNING) for potential hazards.

Introduction

About the Instrument

Describes the MARS 6 Synthesis as a multi-mode microwave system with parallel reaction processing.

Important Safeguards

Solvent Chart

Lists representative examples of microwave absorptive properties for common synthetic solvents.

Minimum Cavity Load

Details the minimum cavity load required based on solvent, number of vessels, and vessel type.

Microwave Safeguards

Lists safety precautions for operating the microwave system and vessels.

Instrument Safeguards

Instrument Overview

Front and Side View

Identifies and describes the front and side components of the instrument with numbered labels.

Back and Side View

Identifies and describes the back and side components of the instrument with numbered labels.

Cavity

Details the components within the microwave cavity, including seals, covers, and sensors.

Software Overview

Software Icons

Provides a visual guide to the icons used in the software interface and their meanings.

Home Screen

Describes the initial screen displayed upon system startup and its accessible areas.

System Menu

Provides a basic review of each section within the System Menu for locating software items.

Settings

Details the various settings available for system configuration, user management, and run adjustments.

Logout

Displays the logout screen and the confirmation prompt for exiting the system.

System Installation

Unboxing

Provides step-by-step instructions for unboxing the MARS 6 Synthesis instrument.

System Setup

Details the steps for connecting the exhaust hose, power cord, and ensuring proper installation.

Vessels

Methods

Create a Classic Method

Guides users through the process of creating a new classic method for synthetic chemistry applications.

Edit Method

Explains how to edit existing methods and the consequences of saving changes.

Delete Method

Outlines the procedure for deleting methods from the system.

Export Method

Describes how to export methods to a USB drive for backup or transfer.

Import Method

Details the process of importing methods from a USB drive into the system.

Users

Create User

Guides administrators on creating new user accounts with different access levels.

Edit/Delete User

Explains how administrators can edit or delete existing user accounts.

Auto Login

Describes how to configure the auto login feature for user access.

Password Configuration

Data Management

View, Print, and Export Data

Explains how to view, print, and export data associated with a specific method run.

Activity Log

Describes the activity log, how to filter it, and how to export or print entries.

Calibrations

Fiber Optic Probe

States that calibration is not required for the fiber optic probe, but GF number entry is needed.

Pressure Control

States that calibration is not required for pressure control.

Temperature Verification (IR Sensors)

Details the process of verifying temperature using the optional AutoCal device.

Temperature Calibration (IR Sensors)

Explains the procedure for calibrating IR sensors using the AutoCal device.

Pressure Calibration

States that pressure calibration must be performed by a CEM Certified Service Representative.

Power Test

Printer (Optional)

Internal Printer

Describes the functionality of the optional internal thermal printer for method data.

Fiber Optic Temperature Control

Fiber Optic Installation

Guides on installing the fiber optic probe and entering the GF number.

Fiber Optic Temperature Verification

Explains how to verify the installed fiber optic probe's temperature reading.

Fiber Optic Care

Provides instructions on proper care and handling of the fiber optic temperature probe.

Software Update

Routine Maintenance

Troubleshooting

Problems and Possible Solutions

Lists common problems, their possible causes, and suggested solutions for the instrument.

System Specifications

Location Requirements

Outlines the necessary environmental and spatial requirements for installing the instrument.

Electrical Requirements

Details the electrical specifications, voltage, and plug types required for operation.

Environmental Requirements

Lists the environmental conditions (temperature, humidity, altitude) for instrument operation.

Warranty

Limited Warranty Information

Provides details about what is covered, for how long, and what is not covered by the warranty.

Warranty Disclaimer

States the warranty disclaimer, excluding implied warranties and limiting liability.

Appendix A: GlassChem 20 Vessels

Vessel Components

Identifies and describes the individual parts of the GlassChem 20 vessels.

Operating Parameters

Lists the operating parameters, power settings, and ideal chemistry for GlassChem 20 vessels.

New Cap and Vent Plug Conditioning

Details the break-in procedure to condition new vessel caps and vent plugs for proper sealing.

Perform a Reaction

Provides step-by-step instructions for assembling vessels and performing a reaction.

Turntable Setup

Guides on how to properly place vessel assemblies onto the turntable for optimal distribution.

Load and perform a Method

Explains how to load a method and perform a reaction using the GlassChem 20 vessels.

Vessel Removal

Provides instructions for safely removing vessels from the instrument after a reaction.

Vessel Cleaning

Outlines the procedure for cleaning GlassChem 20 vessels and vent plugs.

Appendix B: EasyPrep and EasyPrep Plus Vessels

Vessel Components

Identifies and illustrates the components of EasyPrep and EasyPrep Plus vessels.

Operating Parameters

Lists operating parameters, power settings, and ideal chemistry for EasyPrep vessels.

New Liner and Cover Conditioning

Details the break-in procedure for conditioning new EasyPrep liners and covers.

Perform a Reaction

Provides general instructions for performing reactions with EasyPrep vessels.

Turntable Setup

Guides on loading the control vessel and ensuring proper engagement with the turntable.

Load and perform a Method

Explains how to load a method and perform a reaction using EasyPrep vessels.

Vessel Removal

Provides instructions for safely removing EasyPrep vessels after a reaction.

Vessel Cleaning

Outlines the procedure for cleaning EasyPrep liners and covers.

Appendix C: Open Vessel Reactions

Vessel Components

Identifies and describes the components of open vessels used in reactions.

Operating Parameters

Lists operating parameters, power settings, and ideal chemistry for open vessels.

Prepare the Flask

Guides on preparing round bottom flasks for reactions, including inspection and reagent addition.

Load and perform a Method

Explains how to load a method and perform a reaction using open vessels.

Flask Removal

Provides instructions for safely removing flasks after an open vessel reaction.

Glossary

Technical Assistance

Technical Support

Provides contact information and resources for technical support and service.

Contact Information