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Agilent Technologies 5100 User Manual
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Operation
54
Agilent
5100 and 5110 ICP-OES User’s Guide
This page is int
entionally left b
lank.
53
55
Table of Contents
Default Chapter
3
Table of Contents
3
1 Safety Practices and Hazards
7
General
7
Verifying Safe State
8
Plasma
8
Heat, Vapors and Fumes
9
Compressed Gas Hazards
10
Electrical Hazards
11
Other Precautions
11
Warning Symbols
13
CE Compliance
14
Electromagnetic Compatibility
15
En55011/Cispr11
15
Ices/Nmb-001
16
South Korean Class a EMC Declaration
16
2 Introduction
17
Site Preparation Requirements
17
User Documentation
18
Conventions
18
Notes and Tips
18
Specifications
19
Temperature Control
19
Environmental Conditions
19
Electrical Power Supplies
19
Circuit Breaker
19
Other Connections
20
Personal Computer Requirements
20
Gas Supplies
20
Exhaust System
21
ICP-OES Instrument Cooling Air Supply
21
Water Chiller System
22
Drain Vessel
23
3 Installation
25
Agilent ICP-OES Instrument Overview
26
Instrument Status LED Color Coding
28
Front Power On/Off Button
28
ICP Expert Software
29
Connecting ICP Expert Software to the ICP-OES
30
Performing a Detector and Instrument Calibration
30
Saving and Viewing the Calibration Data
32
Hardware Components Replacement
32
ICP-OES Torches
33
Torch Assembly and Disassembly
34
Torch Assembly
35
Torch Disassembly
37
Accessories
38
Advanced Valve System (AVS) - AVS 4, AVS 6 and AVS
38
SVS 2 and SVS 2
40
5-Channel Peristaltic Pump
40
External Inlet Duct Adapter
41
Air Inlet Dust Filter
41
Vapor Generation Accessory (VGA)
41
Multimode Sample Introduction System (MSIS)
41
Argon Humidifier
42
Isomist Programmable Temperature Spray Chamber
42
4 Operation
43
Analysis Checklist
43
Turning on the Instrument and Software
44
Turning on the Instrument for the First Time (or from Long Term Shutdown)
44
Running the Instrument from an Idle State
45
Preparing for Analysis
46
Performing a Detector and Instrument Calibration
46
Creating/Opening a Worksheet
47
Creating a New Worksheet
47
Opening an Existing Worksheet
47
Creating a New Worksheet from a Template
47
Developing a Method
47
Running Samples
49
Printing a Report
50
Instrument Idle State
50
Setting the Instrument to Idle
50
Turning off the Instrument for Long Term Shutdown
52
5 Maintenance and Troubleshooting
55
Routine
56
Cleaning
58
Torch Cleaning
58
Acid Cleaning of the Torch for Aqueous or Acid Based Samples
59
Rinsing the Torch
61
Drying the Torch
62
Additional Checks after Cleaning
63
Troubleshooting
63
Spare Parts
63
Technical Support
64
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Agilent Technologies 5100 Specifications
General
Brand
Agilent Technologies
Model
5100
Category
Laboratory Equipment
Language
English
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