Agilent Technologies 5975 MSD

Agilent Technologies
Agilent 5975/5977 MSD
for OpenLAB CDS
Operation Manual

Agilent Technologies 5975 MSD Specifications

General

Brand	Agilent Technologies
Model	5975 MSD
Category	Laboratory Equipment
Language	English

Summary

Notices

Safety Notices

Provides definitions and explanations for CAUTION and WARNING notices.

Introduction

Important Safety Warnings

Critical safety information regarding potential hazards and precautions.

Hydrogen Safety

Essential safety information and precautions for using hydrogen as carrier gas.

To Replace the Primary Fuses

Installing GC Columns

Conditioning columns

Essential steps for preparing capillary columns before use.

To Install a Capillary Column in a SplitSplitless Inlet

Procedure for installing a capillary column into a split/splitless inlet.

To Condition a Capillary Column

Detailed steps for conditioning a capillary column properly.

To Install a Capillary Column in the GCMS Interface Using the Self-Tightening Column Nut

Procedure for installing a column using a self-tightening nut.

To Install a Capillary Column in the GCMS Interface Using a Standard Column Nut

Procedure for installing a column using a standard column nut.

Operating in Electron Ionization (EI) Mode

Operating the MSD from the Data System

How to automate tasks using OpenLAB CDS software.

Operating the MSD from the GC control panel

Controlling the MSD via the 7890B GC control panel.

Configuring the MSD through the Web User Interface (WUI)

Operating the 59755977 MSD from the local control panel (LCP)

Before You Turn On the MSD

Pre-operation checks and conditions before powering on the MSD.

Pumping Down

Procedure for evacuating the MSD system.

Controlling Temperatures

Controlling Column Flow

Venting the MSD

Steps to safely vent the MSD to atmosphere.

Set MS Analyzer Temperatures

To Calibrate Column Flow Linear Velocity

To Run an Autotune

To Pump Down the MS

Steps to evacuate the Mass Spectrometer (MS) system.

General Maintenance

Before Starting

Guidelines and safety checks before performing maintenance.

Scheduled maintenance

High voltage precautions

Safety warnings regarding high voltages within the MSD.

Dangerous temperatures

Warnings about hot components and burn hazards.

Chemical residue

Electrostatic discharge

Precautions and procedures to prevent ESD damage to sensitive components.

Maintaining the Vacuum System

Maintaining the Analyzer

To Open the Analyzer Chamber

To Remove the EI Ion Source

Procedure for removing the Electron Ionization (EI) ion source.

To Disassemble the Standard or Inert EI Ion Source

To Disassemble the Extractor EI Ion Source

To Clean the EI Ion Source

To Assemble a Standard or Inert EI Ion Source

To Assemble the Extractor EI Ion Source

To Replace a Filament in an EI Ion Source

To Install the EI Ion Source

To Attach Wiring from the Ion Source to the feedthrough board

To Replace the Electron Multiplier Horn

To Close the Analyzer Chamber