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Agilent Technologies 5975 Series

Agilent Technologies 5975 Series
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Agilent 5975/5977 MSD for OpenLAB CDS
Operating Manual

Table of Contents

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Agilent Technologies 5975 Series Specifications

General IconGeneral
CategoryGas Chromatograph/Mass Spectrometer (GC/MS)
Mass ResolutionUnit mass resolution
Ionization ModeElectron Ionization (EI)
InterfaceEthernet, USB, optional analog and digital I/O
GC CompatibilityAgilent GC systems
Sensitivity1 pg octafluoronaphthalene (OFN), S/N ≥ 1000:1 (EI mode)

Summary

Notices

Warranty Information

Legal terms for the manual's content and its use, including warranty disclaimers.

Safety Notices Explained

Explains CAUTION and WARNING notices used in the manual for hazard identification.

About This Manual

Manual Overview and Scope

Describes the manual's content and scope for operating and maintaining the MSD.

Hardware User Information

5977 B MSD Documentation

Details accompanying manuals and tools for the 5977B MSD.

Older MSD Documentation Reference

Refers users to documentation for models prior to the 5977B.

1 Introduction

MSD Hardware Description

Provides a detailed description of the MSD hardware components.

Important Safety Warnings

Lists critical safety notices to be observed when using the MSD.

Hydrogen Safety Precautions

Details the hazards and precautions associated with using hydrogen as a carrier gas.

Safety and Regulatory Certifications

Lists safety standards and regulatory compliance for the MSD.

2 Installing 7890782068906850 GC Columns

GC Columns

Discusses GC column types, restrictions, and gas flow rates for MSD compatibility.

Conditioning Capillary Columns

Explains the importance and procedure for conditioning capillary columns before use.

Installing a Capillary Column

Provides step-by-step instructions for installing a capillary column into a GC inlet.

Calibrating Column Flow

Describes how to calibrate column flow linear velocity for accurate measurements.

GCMSD Interface

Explains the heated conduit connecting GC and MSD for capillary columns.

3 Intuvo 9000 GC Column Maintenance

Intuvo 9000 GC Columns

Discusses Intuvo 9000 GC column types and restrictions for MSD use.

Conditioning Intuvo Columns

Explains the process of conditioning Intuvo columns before GC/MS interface connection.

Replacing an Intuvo GC Column

Step-by-step guide for replacing an Intuvo GC column.

Installing Column Guard or Jumper Chip

Instructions for installing consumable column guard or jumper chips.

Replacing the 9000 GCMS Tail

Procedure for replacing the GC/MS tail component.

4 Operating in EI Mode

Operating MSD from Data System (DS)

Explains automated tasks using OpenLAB CDS software for MSD operation.

Operating MSD from GC Control Panel

Details how to control the MSD using the 7890B GC control panel.

Configuring MSD Network Settings

Steps to configure MSD network settings via Web User Interface (WUI).

Operating from Local Control Panel (LCP)

Explains operation of MSD using the Local Control Panel (LCP).

5 General Maintenance

Before Starting Maintenance

General information and safety precautions before performing maintenance.

Scheduled Maintenance Tasks

Outlines the maintenance schedule for reducing problems and prolonging system life.

Maintaining the Vacuum System

Describes periodic tasks for maintaining the instrument's vacuum system.

Maintaining the Analyzer

Details maintenance tasks for analyzer components like ion source and filaments.

Opening the Analyzer Chamber

Step-by-step guide for opening the analyzer chamber for maintenance.

Removing EI HES Components

Procedures for removing specific components of the EI HES.

Replacing EI Filaments

Instructions for replacing filaments in EI HES, XTR, SS, or Inert sources.

Cleaning EI Components

Steps for cleaning EI source parts to maintain performance.

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