Agilent Technologies 5975 MSD Service Manual

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RESULTS
DIP Temperature Accuracy Test
Setpoint
[°C]
Measured
Value
[°C]
Typical Range
of Operation
Pass/Fail Verified By/Date
30 30 ± 5
150 150 ± 5
250 250 ± 7
350 350 ± 7
5.2 Leak test
This procedure consists of the Tune evalutation results (MS ChemStation) or the Air/Water
Check (MassHunter software) described in section 2.10 (DIP in “Ready” status with the push
rod outside the MS ion source and the results of an Air/Water check while the push rod is
located in the ion source. The leak test of DIP/MS-System is passed, when the results of
both measurements do not essentially differ.
REQUIREMENTS
- an autotune and tune evalutation test (for 5975 MSD) or “Air And Water Check” (for 7000
Triple Q) have just been performed.
CONDITIONS
- MS – “Ready”
- DIP – “Ready/Bereit”
PROCEDURE
1. Start the DIP Software and load the method “a_w_check.dip”.
2. Start the DIP (start button in the software or controller): The push rod will be inserted
into the ion source, heated up to the source temperature (230 °C) and be kept there
for 10 minutes.
3. When the setpoint is reached and the reading stabilizes, perform a tune evaluation or
an “air/water check” (5975 MSD: go to “Instrument / Edit MS Tune Parmeters” and
select “Air/water check”; 7000 Triple Q MS/MS: go to “Manual Tune / Vacuum
Control” and select “Air and Water check”.
4. Compare this result with the tune evaluation report (5975 MSD)/air and water check
(7000 Triple Q MS/MS)when the push rod was in the “Ready” position outside the MS
ion source (see this manual, section 2.10) and complete the table in the Results
section.

Agilent Technologies 5975 MSD Specifications

General

Brand	Agilent Technologies
Model	5975 MSD
Category	Laboratory Equipment
Language	English