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CONTENT

1 PARAMETER MENU OF THE CONTROLLER (FIRMWARE V1.10) .......................... 4

2 DIP INSTALLATION PROCEDURE ............................................................................ 5

2.1 Replacing the ion source ........................................................................................... 5

2.2 Installing the DIP on the Agilent 5975 MSD ............................................................... 5

2.3 Installing the DIP on the Agilent 7000 Triple Q ........................................................... 7

2.4 Connecting the DIP and the GC ................................................................................. 8

2.5 Configuration of the DIP-Controller ............................................................................ 9

2.6 Installing the DIP Software ......................................................................................... 9

2.7 Insert the ChemStation/MassHunter methods for the DIP .........................................10

2.7.1 5975 MSD: ChemStation methods .........................................................................10

2.7.2 7000 Triple Q MS/MS: MassHunter methods .........................................................10

2.8 Adjustment of the CombiPAL to the MS-DIP System (optional) ................................10

2.9 Push rod performance test ........................................................................................10

2.10 Tuning of the DIP-MS System ...................................................................................10

2.10.1 Autotune 5975 MSD with DIP .................................................................................10

2.10.2 Autotune 7000 TripleQ MS/MS with DIP .................................................................11

2.11 Controller: Update of the firmware ............................................................................11

3 EXACT POSITIONING OF THE PUSH ROD IN THE ION SOURCE .........................12

4 TEMPERATURE CALIBRATION OF THE CONTROLLER ........................................14

4.1 Menu: General Configuration ....................................................................................14

4.2 Temperature Calibration ...........................................................................................14

5 DIP TEST PROCEDURES ........................................................................................16

5.1 DIP Temperature accuracy test ................................................................................16

5.2 Leak test ...................................................................................................................17

5.3 Coupling test: CombiPAL with MSD-DIP and GC (optional, for DIP - 45° type with

5975 MSD) ...........................................................................................................................18

5.4 DIP (EI) Performance test .........................................................................................19

5.5 DIP (PCI) Performance test for DIP/5975 MSD Systems ..........................................22

APPENDIX ...........................................................................................................................24

Agilent Technologies 5975 MSD Service Manual

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