- 23 -
Scientific Instruments Manufacturer GmbH
D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de
PROCEDURE
Set up the Methods
1. Load method DIP_CI_Q1.M for the 5975 MSD (MS ChemStation).
2. Select PCICH4.U using Instrument/Select MS Tune File.
3. Save the method to “…\1\METHODS\DIP_CI_Q1.M”
4. Print the method and verify that method and conditions are the same
5. Load method “check_CI.dip” for the DIP-system (via DIP software, see DIP manual).
The following steps have to be performed with the push rod tip for liquid samples (A) and the
tip for solid samples (B):
6. After loading the DIP method, click the Start button (green arrow) in the Instrument
Control view (of the MS Software) and specify all sample information in the Sample
Information panel.
7. Click on “Start Run” and wait for the Ready-signal of the MSD (“Acquisition: Waiting
for remote start …”).
8. If the Ready-signal appears in the status display (green field), you can inject the
sample according to the DIP manual (see 6.3) by pressing the “START” key to move
the push rod into the “Load” position.
9. Start the DIP using the controller or the “DIP”-software (see DIP manual, 6.2): Click
on the “START” key of the controller or in the “DIP” program to start the
measurement.
RESULTS
CI PERFORMANCE
Item
t
max
(TIC)
[min]
To Next Page
Loading...
