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Bruker InsightMR User Manual

Bruker InsightMR
60 pages
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InsightMR
User Manual
Version 003
Innovation with Integrity
ā—
NMR

Table of Contents

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Bruker InsightMR Specifications

General IconGeneral
BrandBruker
ModelInsightMR
CategoryAnalytical Instruments
LanguageEnglish

Summary

About This Manual

1.1 Policy Statement

Bruker's policy on product improvement and right to change specifications.

1.2 Symbols and Safety Conventions

Explanation of safety symbols, conventions, and alert levels used in the manual.

Introduction

2.1 Concept

Overview of InsightMR's purpose and components for chemical process analysis.

2.2 Intended Use

Description of the glass flow tube's function and system usage.

2.3 Legal & Support Information

Legal disclaimers, copyright, warranty, and customer service contact details.

Safety

3.1 System Owner's Responsibility

Obligations of the system owner regarding safety, regulations, and personnel training.

3.2 Personnel Requirements

Qualifications and suitability requirements for laboratory personnel operating the device.

3.3 Personal Protective Equipment

Importance of wearing personal protective equipment for safety.

3.4 General Workplace Dangers

Hazards related to toxic liquids, vapors, broken glass, and assembly movement.

Design and Function

4.1 Description

Detailed description of the InsightMR hardware components and their arrangement.

4.2 Software

Introduction to the InsightMR software and its capabilities.

Transport, Packaging and Storage

5.1 Symbols on the Packaging

Explanation of various symbols used on packaging material for handling.

5.2 Inspection at Delivery

Procedure for inspecting deliveries for completeness and transport damage.

5.3 Packaging

Information on packaging materials, handling, and disposal.

5.4 Storage

Instructions for storing the flow unit for extended periods.

Flow Unit Installation

6.1 Choose the Position of the Reactor

Guidance on selecting the optimal position for the reactor and transfer line.

6.2 Connecting the Transfer Line Holder

Instructions for attaching the transfer line holder.

6.3 Testing the Flow Unit Prior to Inserting it into the Magnet

Steps for testing the flow unit before installation into the magnet.

6.4 Temperature Control (optional)

Steps for connecting and setting up the optional temperature control.

6.5 Software Installation

Detailed instructions for installing the InsightMR software and its components.

6.6 Software Configuration

Configuration steps for TopSpin, InsightMR flow mode, and adding solvents.

Operation

7.1 Inserting and Using the Flow Unit

Step-by-step guide for inserting and operating the flow unit.

7.2 Acquiring NMR Data Using InsightMR Software

Instructions for launching and using InsightMR software for data acquisition.

7.3 Removing the Flow Unit for Storage

Procedure for safely removing and storing the flow unit.

7.4 Returning the Spectrometer to Normal Operation

Steps to revert the spectrometer to its normal non-flow operating state.

Flow Tube Assembly - Insertion Checklist

8.1 Prepare the NMR System

Steps to prepare the NMR system before flow tube assembly insertion.

8.2 Prepare the Flow Tube Assembly

Instructions for preparing the flow tube assembly before insertion.

8.3 Connect the Temperature Control Equipment

Steps to connect the optional temperature control equipment.

8.4 Connect the Sample Supply

Procedure for connecting the sample supply to the flow unit.

8.5 Insert the Flow Tube Assembly

Detailed steps for inserting the flow tube assembly into the magnet.

8.6 The System is Ready to be Used

Confirmation that the system is ready for use after installation.

Flow Tube Assembly - Removal Checklist

9.1 Prepare the Flow Tube Assembly

Steps to prepare the flow tube assembly for removal.

9.2 Remove the Flow Tube Assembly

Procedure for safely removing the flow tube assembly from the magnet.

9.3 Storage

Instructions for storing the flow tube assembly after removal.

9.4 Prepare the NMR System

Steps to return the NMR system to its normal configuration.

9.5 The system is ready for normal usage

Confirmation that the system is ready for normal usage after removal.

InsightMR Glass Flow Tube Exchange Instructions

10.1 Removing the Glass Flow Tube

Step-by-step guide for safely removing the glass flow tube from the holder.

10.2 Mounting the Glass Flow Tube

Instructions for safely mounting the glass flow tube onto the tube holder.

Dismantling and Disposal

11.1 Dismantling

Procedures and precautions for dismantling the device.

11.2 Disposal Europe

Environmental information and regulations for disposal in the EU.

11.3 Disposal USA and Other Countries

Disposal information for materials in the USA and other countries.

Technical Data

NMR System Requirements

Specifications for the NMR system required for InsightMR.

Data Acquisition and Analysis

Recommendation for using InsightMR software for data acquisition and analysis.

Recommended Temperature Range

Specified temperature range for operation and measurement.

Recommended Pressure

Recommended operating pressure for the system.

Wetted Materials for Sample and Control Lines

Lists materials in contact with sample and control liquids.

Contact

Manufacturer Information

Contact information for Bruker BioSpin GmbH.

NMR Hotlines and Support

Contact details for NMR service centers and technical support.

Applications Support

Contact email for InsightMR specific application support.