Operation
40 H155936_3_003
• Fix the insulated transfer line to the top of the magnet using the transfer line holder or
Velcro tape.
Figure7.2: Mounting the Insulated Transfer Line
• Switch the pump on.
• Check that the solvent returns to the vessel and that the total volume remains stable.
• Check that the liquid level in the thermostat remains stable.
• Start the process to monitor (e.g. by adding the last reagent to the reaction mixture).
7.2 Acquiring NMR Data Using InsightMR Software
Upon  installation  of  InsightMR,  launch  the  program  by  clicking  on  the  InsightMR  desktop
Icon.
Refer to the InsightMR quick start guide under Help - QuickStart for instructions on how to
use the software. Under Help there are also manuals for IconNMR and Dynamics Center, the
foundation platforms of InsightMR.
Additional  information,  a  video  and  an  educational  webinar  can  be  found  at  our  webpage:
https://www.bruker.com/insightmr
NOTICE
Material damage to flow unit due to incorrect automation mode
Failure to set the Sample Changer/Automation mode to Flow Tube (InsightMR) may result
in flow tube breakage.
u Set the Sample Changer/Automation to Flow Tube (InsightMR) in IconNMR
configuration Automation/Master Switches.