EasyManua.ls Logo

Malvern Mastersizer X Series User Manual

Malvern Mastersizer X Series
183 pages
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Page #1 background imageLoading...
Page #1 background image
Getting Started
Getting Started
MAN 0101 Issue1.3 August 1997

Table of Contents

Question and Answer IconNeed help?

Do you have a question about the Malvern Mastersizer X Series and is the answer not in the manual?

Malvern Mastersizer X Series Specifications

General IconGeneral
Measurement PrincipleLaser diffraction
ConnectivityUSB, Ethernet
Sample DispersionWet or dry dispersion
Measurement Range0.01 to 3500 µm
Data OutputParticle size distribution
SoftwareMastersizer software
Optical ModelMie theory, Fraunhofer approximation
ComplianceISO 13320
Laser TypeHe-Ne gas laser and solid-state blue light source

Summary

Introduction to this manual

Instrument Access and Responsibilities

Details responsibilities of Malvern personnel, supervisor, and operator regarding instrument access.

Getting to know your system

The Optical Unit Components

Details the three main components of the optical unit: transmitter, receiver, and sample area.

Transmitter End Panel Connectors

Details connectors on the transmitter end panel, including power, interlock, and remote sockets.

Transmitter Features

Explains laser power key, indicator, switch, and the QSpec logo.

The Sample Area and Range Lenses

Details the beam expander and range lenses, including their functions and available types.

Sample Cell Types and Panel Features

Explains sample cell types (stirred, flow, air), cell pipe connectors, and removable accessory panels.

The Receiver Unit

Describes the receiver unit, its function in collecting scattered light data, and the detector.

The Malvern Software Overview

Introduces the Windows-based Mastersizer software and its functions.

Screen Layout Overview

Identifies key features of the software screen, including the title bar and menu bar.

Software Modes of Operation

Introduces the three main software modes: Easy, Menu, and Program mode.

How the Mastersizer Works

Measurement Process Overview

Describes the two main procedures: capturing scattering patterns (measurement) and analysing data using presentations.

Measurement and Data Analysis Steps

Emphasizes the importance of correct measurement procedures and outlines the stages involved.

Setup for Measurement

Explains the initial setup step to inform the software about system parameters like lens type.

Optical Alignment Procedure

Describes the automatic procedure for aligning the laser onto the detector.

Background Measurement Procedure

Explains the process of measuring background scattering to remove interference.

Adding Sample and Inspecting Concentration

Details how to add sample and monitor obscuration for correct concentration.

Measuring the Sample

States that the sample scattering pattern is measured after all preceding steps are completed.

Analysing Measurement Data

Outlines the three steps for data analysis: mode, presentation, and calculation.

Choosing the Correct Analysis Model

Explains the available analysis models and their suitability based on expected result graph shapes.

Saving Measurement Results

Details the importance of a structured approach to saving data (records, run numbers, sample files).

Making a Measurement

Sample Preparation Importance

Highlights sample preparation as a critical step for accurate measurements and discusses representative sampling.

Optical System Cleanliness

Emphasizes the importance of clean optics for accurate laser scattering measurements.

Choosing the Correct Range Lens

Guides the user on selecting the appropriate range lens based on sample size and dispersion method.

Determining the Sample Size Range

Explains how to determine the correct lens based on particle size ranges, including test measurements.

Sample Dispersion Method Considerations

Discusses the second factor in lens choice: the method of sample dispersion.

Measuring the Background

Explains the purpose of background measurement and when to take a fresh background.

Instrument Preparation Steps

Details checks for instrument connection, power, lens fitting, and beam expander.

Setting up Hardware Configuration

Guides on using the "Setup Hardware" dialogue to configure the system.

Aligning the System Optics

Describes the procedure for aligning the laser to the detector, necessary after optics changes.

Taking a Background Measurement

Explains how to perform a background measurement using the "Measure-Background" dialogue.

Adding Sample and Concentration Check

Explains how the system monitors obscuration to ensure correct sample concentration.

Measuring the Sample Final Step

Describes the final step of measuring the sample using the "Measure-Sample" dialogue.

Analysing the Measurement Data

Choosing the Correct Analysis Mode

Explains the available analysis models and their suitability based on expected result graph shapes.

Selecting the Correct Presentation

Discusses the importance of selecting the correct presentation based on sample optical characteristics.

Methods for Selecting a Presentation

Describes the different ways to select a presentation via the "Setup Presentation" dialogue.

Calculating the Final Result

Explains the final step of calculating the result after choosing optical model and presentation.

Viewing and Printing the Results

Interpreting the Results

Automating the Process

Setting Up a Measurement Sequence

Guides on setting up measurement sequences using the "Setup-Measurement Sequence" menu.

Sample Preparation

Advanced Result Processing

Maintenance Procedures

Advice for Continuous Sprays

Related product manuals