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METER AQUALAB User Manual

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AQUALAB
©
VSA
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METER AQUALAB Specifications

General IconGeneral
ModelAQUALAB
Accuracy (aw)±0.003 aw
Measurement Time5 minutes
Measurement Range (aw)0.03 to 1.00 aw
Temperature Range5°C to 50°C
Power Supply110-220 VAC, 50/60 Hz

Summary

1. INTRODUCTION

2. ABOUT THE VSA

2.1 MOISTURE SORPTION ISOTHERMS

Defines the relationship between water activity and moisture content, crucial for product quality and safety.

2.2 MEASUREMENT METHOD

Explains the DDI and DVS methods used by the VSA for dynamic and static isotherms.

2.3 SPECIFICATIONS

Details the technical specifications for water activity, temperature, dimensions, and compliance.

2.4 USER INTERFACE AND MENUS

Describes the instrument's interface, including tabs like Isotherm, Measurement, Configuration, and Data.

2.4.3 CONFIGURATION TAB

Provides access to various settings like calibration, date, time, regional formatting, and admin settings.

2.4.4 DATA TAB

Enables viewing, graphing, and deleting stored test data.

3. THEORY

3.1 COMBINING DVS AND DDI IN ONE INSTRUMENT

Highlights the VSA's unique capability to generate both dynamic (DDI) and equilibrium (DVS) isotherms.

3.2 HYSTERESIS

Explains hysteresis, the phenomenon where water content differs during adsorption and desorption.

3.3 NONEQUILIBRIUM

Discusses how slow diffusion can lead to apparent hysteresis, affecting measurement accuracy.

3.4 MATRIX CHANGES

Explains how physical changes in a sample matrix can affect isotherm results and apparent hysteresis.

3.5 WORKING ISOTHERMS

Describes generating working isotherms to analyze sorption characteristics from a sample's native state.

3.6 ISOTHERM MODELS

Introduces common models like BET and GAB used to predict moisture content and thermodynamic functions.

3.7 USES FOR MOISTURE SORPTION ISOTHERMS

Details applications like process control, moisture content prediction, temperature effects, and shelf life.

4. INSTALLATION

Preparation and Setup

Selecting a location, leveling the instrument, and initial physical setup procedures.

Power and Component Installation

Connecting power, installing desiccant tubes, air cylinder, and weighing pan.

Scale Stability and Water Tank

Verifying scale stability and filling the water tank for operation.

Computer Connection

Steps to install the software and connect the instrument to a computer.

5. CLEANING AND MAINTENANCE

5.1 DESICCANT REPLACEMENT

Instructions on how to replace the desiccant material when it exhausts its drying capacity.

5.2 SAMPLE CHAMBER CLEANING

Detailed procedure for cleaning the sample chamber, mirror, and sensors to maintain accuracy.

5.2.1 CLEANING KIT

Lists the supplies included in the AQUALAB Cleaning Kit for instrument maintenance.

5.2.2 CLEANING PROCEDURE

Step-by-step guide for washing, rinsing, and drying components for thorough cleaning.

5.3 CAPACITANCE FILTER REPLACEMENT

Instructions for replacing the capacitance filter if it becomes contaminated.

5.4 MAINTENANCE PACKAGES

Overview of available maintenance and calibration service packages offered by METER.

6. VERIFICATION AND CALIBRATION

6.1 WATER ACTIVITY VERIFICATION

Importance and procedure for verifying water activity calibration against standards.

6.1.1 VERIFICATION STANDARDS

Lists the available verification standards and their corresponding water activity levels.

6.1.2 VERIFICATION OF CALIBRATION

Steps to perform calibration verification and check for linear offset.

6.2 LINEAR OFFSET

Procedure for adjusting the linear offset to correct for minor calibration drifts.

6.3 ADJUSTING FOR WEIGHT MEASUREMENT OFFSET

Steps to adjust the balance offset for accurate weight measurements.

6.4 RESTORE FACTORY DEFAULTS

Instructions to restore original calibration settings to factory defaults.

6.5 ISOTHERM STANDARD COMPARISON

Performing a comparison of generated isotherms against a standard for accuracy checks.

7. RUNNING A TEST

7.1 BECOMING FAMILIAR WITH STAGES

Understanding test stages and how they contribute to an overall isotherm test.

7.2 MOISTURE ANALYSIS TOOLKIT SOFTWARE

Using the software for interfacing, data download, viewing, and test setup.

7.3 RUNNING A MOISTURE SORPTION ISOTHERM TEST

General procedure for setting up and running a moisture sorption isotherm test.

7.4 USING DDI TO INVESTIGATE GLASS TRANSITION

Specific DDI test parameters for investigating glass transition events.

7.5 CREATING A WORKING ISOTHERM

Steps to generate both adsorption and desorption curves for a working isotherm.

7.6 EDITING A RUNNING ISOTHERM TEST

How to edit a running test by adding or modifying stages.

7.7 RUNNING A WATER ACTIVITY TEST

Using the VSA as a water activity meter, including settings for capacitance or dew point sensors.

8. SAMPLE PREPARATION

8.1 COATED AND DRIED SAMPLES

Special considerations for preparing samples with coatings or that equilibrate slowly.

8.2 LOW WATER-EMITTING SAMPLES

Techniques for samples that emit water slowly, suggesting DVS over DDI.

8.3 VOLATILE SAMPLES

How to handle volatile samples that can affect sensor readings.

8.4 LOW WATER ACTIVITY

Handling samples with water activity below the instrument's detection limits.

9. SERVICE

9.1 TROUBLESHOOTING

Lists common problems and their solutions for instrument issues.

9.2 CUSTOMER SUPPORT

Contact information for customer service and technical support in North America and Europe.

9.3 REPAIR

Procedures and warranty information for instrument repairs and returning units.

9.4 TERMS AND CONDITIONS

Agreement to METER Group's terms and conditions when using instruments.

APPENDIX A. NONCONDENSING CONDITIONS FOR VSA TESTING

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