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SI Analytics TitroLine 7500 KF User Manual

SI Analytics TitroLine 7500 KF
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TitroLine®
7500 KF
TITRATOR
OPERATING INSTRUCTIONS

Table of Contents

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SI Analytics TitroLine 7500 KF Specifications

General IconGeneral
BrandSI Analytics
ModelTitroLine 7500 KF
CategoryLaboratory Equipment
LanguageEnglish

Summary

Operating Instructions TitroLine® 7500 KF

Chapter 1: Technical Specifications

1.1 Summary of Specifications

Provides a concise overview of the TitroLine® 7500 KF's applications and capabilities.

1.2 Detailed Specifications

Details technical specifications including CE sign, country of origin, allowed fluids, and measurement inputs.

1.3 Warning and Safety Information

Outlines crucial safety guidelines, warnings, and precautions for operating the TitroLine® 7500 KF.

Chapter 2: Unpacking and First Operation

2.1 Unpacking the Titrator

Instructions for carefully unpacking the TitroLine® 7500 KF and its modules.

2.2 Installation and Connection

Guidance on installing and connecting the titration stand and vessel to the titrator.

2.3 Connecting Accessories and Devices

Details on connecting external devices like printers, keyboards, and balances to the titrator.

2.4 Setting the Country Language

Procedure for setting the preferred language for the titrator's interface.

2.5 Interchangeable Unit WA Setup

Instructions for installing and setting up the interchangeable unit WA.

2.6 Positioning and Replacing Units

Guidance on how to correctly position and replace interchangeable units on the base unit.

2.7 Initial Filling or Rinsing

Procedure for the initial filling or rinsing of the entire interchangeable unit.

2.8 Filling Titration Vessel with Solvent

Steps for filling the titration vessel with the appropriate solvent.

2.9 Replacing Glass Cylinder and Piston

Instructions for safely replacing the glass cylinder and PTFE piston.

Chapter 3: Working with the Titrator

3.1 Front Keyboard Operation

Explanation of the functions and usage of the titrator's front keyboard.

3.2 Display Information

Description of the titrator's graphical LCD display and its capabilities.

3.3 Manual Controller (Mouse)

Details on using the manual controller ('mouse') for dosing and sample preparation.

3.4 External PC Keyboard

Mapping of keys and functions for an external PC keyboard connected to the titrator.

3.5 Menu Structure Overview

Overview of the titrator's menu structure and navigation paths.

3.6 Main Menu Functions

Explanation of the main menu and its primary functions like method selection.

3.6.1 Standard KF Titration Methods

Description of pre-defined standard methods for Karl Fischer titration.

3.6.2 Automatic KF Titration

Guide to performing automatic Karl Fischer titrations, including preconditioning.

3.6.3 Dosage Operations

Instructions for executing dosing methods and operations on the titrator.

3.6.4 Preparing Solutions

Details on using the 'Preparing solutions' method for creating solutions.

Chapter 4: Method Parameters

4.1 Method Editing and Creation

Steps for editing existing methods or creating new titration methods.

4.2 Default Methods Selection

How to select and use the pre-configured default titration methods.

4.3 Copying Methods

Procedure for copying existing titration methods to create new ones.

4.4 Deleting Methods

Instructions on how to delete existing titration methods.

4.5 Printing Methods

Options for printing the currently selected method to a printer or USB drive.

4.6 Changing Method Parameters

Detailed guide on modifying various parameters for titration methods.

4.6.1 KF and Dead Stop Titration Modes

Explanation of KF and Dead Stop titration modes and their applicable parameters.

4.6.2 Result Settings

Configuration options for how titration results are displayed and calculated.

4.6.2.1 Calculation Formula

Selection and configuration of calculation formulas for titration results.

4.6.2.2 Sample Weight and Volume

Setting sample quantity input methods: manual, automatic, fixed weight or volume.

4.6.2.3 Formula Unit Selection

Choosing the unit (e.g., %, ppm, ml) for formula calculations and results.

4.6.2.4 Formulae for Solution Preparation

Specific calculation formulas available for the 'Prepare Solutions' mode.

4.6.2.5 Decimal Digits Configuration

Setting the number of decimal places for titration results (2-6).

4.6.2.6 Statistics Calculation

Enabling and configuring automatic calculation of mean value and relative standard deviation.

4.6.2.7 Global Memories for Results

Saving titration results into global memories for further calculations.

4.6.3 Titration Parameters

Setting key titration parameters like waiting time, step size, and endpoint criteria.

4.6.5 Dosing Parameters

Configuration of dosing speed, filling speed, and maximum dosing/titration volumes.

4.6.6 Sample Identification

Options for inputting manual, automatic, or no sample identification.

4.6.7 Documentation Settings

Choosing documentation formats (short, standard, GLP) for printing or saving results.

Chapter 5: System Settings

5.1 Interchangeable Unit - Reagents

Information stored on the RFID transponder for interchangeable units, including reagent data.

5.2 RS232 Settings

Configuration of device address and parameters for RS232 interfaces.

5.3 Date and Time Settings

Setting the current date and time for the titrator.

5.4 Password Protection

Information regarding password activation (currently not implemented).

5.5 Reset to Factory Settings

Procedure for resetting all settings to factory defaults, including data deletion warning.

5.6 Printer Configuration

Settings for connecting and configuring compatible printers.

5.7 Device Information Display

Accessing information about the titrator, such as software version and serial number.

5.8 System Tone Settings

Adjusting the volume for system sounds and keypad feedback.

5.9 Software Update Procedure

Steps for updating the titrator's device software using a USB stick.

Chapter 6: Data Communication

6.1 General Information on Communication

Overview of RS232-C and USB-B interfaces for device communication.

6.2 Chaining Multiple Devices (Daisy Chain)

Concept and procedure for connecting multiple devices in a chain via RS232-C.

6.3 RS-Communication Instruction Set

Command structure and syntax for RS-communication with the titrator.

Chapter 7: Connections

7.1 Connecting Analytical Balances

Detailed guide on connecting analytical balances via RS232-C for data transfer.

7.2 Balance Data Editor

Functionality for editing, adding, or deleting balance data entries.

7.3 Connecting Printers

Instructions for connecting and configuring printers for outputting results.

Chapter 8: Maintenance and Care

Chapter 9: Storage and Transportation

Chapter 10: Recycling and Disposal

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