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Advanced Instruments 3250 User Guide
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109
Mode:
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Serial Number:
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Softwar
e Re
vision:
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Sample Probe Number:
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Block Probe Number:
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Date
Problem/
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ymptom
Action
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e L
og
Appendix H
3250
108
110
Table of Contents
Copyright
2
Hot-Line ™ Service
2
Table of Contents
3
Safe Use
7
Symbol Conventions
7
General Cautions
8
FCC Requirements
9
Supplies, Parts and Accessories
10
Calibrators and Standards
12
Foreword
14
Intended Use
14
Principles of Freezing-Point Osmometry
15
Instrumentation
16
Freezing-Point Thermodynamics
16
Definitions
18
Installation and Setup
20
Step 1 - Find a Location for the Instrument
20
Step 2 - Obtain Additional Items
20
Step 3 - Unpack the Instrument
21
Step 4 - Install the Heat Transfer Fluid
22
Step 5 - Load Printer Paper (Figure 1)
23
Step 6 - Power up the Instrument
25
Step 7 - Prime the Heat Transfer Fluid Pump
25
Step 8 - Run a Diagnostic Test
27
Step 9 - Set Date and Time
27
Step 10 - Set Language Preference
27
Step 11 - Check Initial Factory Calibration
28
Step 12 - Proceed to Chapter 2
28
Instrument Operation
29
Hazardous Material Cautions
29
Function of Major Components
30
Operating Head (Figure 3, Item 1)
30
Freezing Chamber (Figure 3, Item 8)
30
Measurement and Control Circuits (Inside)
31
Electronic Circuits (Inside)
31
Display Panel (Figure 3, Item 4)
31
Keypad (Figure 3, Item 4)
32
Printer (Figure 3, Item 9)
33
Supervisor/Operator Keyswitch (Figure 5)
33
Power Module (Figure 5)
34
Port (Figure 5)
34
Barcode Port (Figure 5)
34
Sample Preparation
35
Sample Handling
35
Repeatability Tips
36
Verifying Calibration Daily
37
Sample Test Procedure
38
Sample Test Errors
41
Changing Operating Settings
42
Select Setup Item
43
Set Block bin
44
Set Sample bin
44
Dis/Enable I.D
45
Set Stir Amplitude
45
Set Date/Time
46
Dis/Enable Beeper
46
Set Serial Rate
47
Dis/Enable Xon/Xoff
47
Serial Number
47
Select Language
48
Product/Test
48
Data Capture
48
Assistance
48
Set "Buzz" Amplitude
48
Set "Buzz" Point
49
Select Range
50
Zero Calibration
51
Using the RS-232 Port
51
Standards and Quality Control
52
Repeatability and Accuracy
52
Standards and Controls
52
Maintenance of Standards
53
Quality Control Implementation
53
Calibration
55
Calibration Procedure
55
Calibration Notes
57
Troubleshooting and Service
58
Service and Maintenance Cautions
58
Obtaining Service
60
To Return an Instrument for Repair or Replacement
61
Routine Maintenance
62
Shutdown and Storage
62
Troubleshooting Checks
63
Internal Diagnostic Tests
64
Statistics
65
Recall Results
66
A/D Tests
66
Stir/Freeze Test
68
Probe bin Test
68
Display/Print Test
70
Beeper Test
70
Keypad Test
70
Head Up/Down Test
71
Event Record
71
Fuse Replacement
71
Sample Probe Checks and Replacement
73
Mandrel, Probe, and Stir/Freeze Wire Alignment
77
Alignment Using the Alignment Tool
77
Alternate Method-Using a Sample Tube Containing 0.2 Ml of Water
79
Stir/Freeze Amplitude Adjustment
80
Troubleshooting Table
83
Product Specifications
90
Regulatory Notices
93
Warranty and Warranty Duties
97
Supplemental RS-232 Information
101
Symbol Definitions
104
Product Disposal and Recycling
107
Service Log
109
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Advanced Instruments 3250 Specifications
General
Brand
Advanced Instruments
Model
3250
Category
Measuring Instruments
Language
English
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