Agilent Technologies 5975 MSD Service Manual

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CONDITIONS for DIP/7000 Triple Q MS/MS
DIP Ready / Bereit
DIP method
check_EI_scan.dip (40°C for 1 min, 40-350°C at 1.0°/s, 350°C for 5
min)
MS/MS Ready
MS method DIP_EI_Scan.M
MS aux temp 280°C
Tune file atunes.ei.tune.xml
Ion Sorce EI
Aquisition mode SCAN
Scan Type MS1 Scan
Stop Mode By Stop Time
Stop time 10 min
Column flow 0.5 ml/min
Solvent delay 0.3 min
Time filter enabled yes
Time filter peak width
0.7 s
Use gain no
EMV Use tune setting (Delta EMV=0)
Mass range (low) 100.0
Mass range (high) 600.0
Scan time 100 ms
Threshold 0
Step size 0.1 amu
MS quad temp
(Q1 + Q2)
150°C
MS ion source temp :
230°C
Sample triglyceride standard
Push rod tip A: for liquid samples, B: for solid samples
Sample volume 1 µl
PROCEDURE
Set up the Methods
1. Load method DIP_EI_Q1.M for the 5975 MSD (MS ChemStation) or DIP_EI_Scan.M
for the 7000 Triple Q MS/MS.
2. Select the actual autotune using Instrument/Select MS Tune File (ATUNE.U or
atunes.ei.tune.xml).
3. Save the method to “…\1\METHODS\” as “DIP_EI_Q1.M” resp. “DIP_EI_Scan.M”
4. Print the method and verify that method and conditions are the same.
5. Load method “check_EI.dip” for the DIP-system (via DIP software, see DIP manual).

Agilent Technologies 5975 MSD Specifications

General

Brand	Agilent Technologies
Model	5975 MSD
Category	Laboratory Equipment
Language	English