Exercise 1 – Develop an acquisition method
Task 1. Enter acquisition parameters and acquire data
Agilent 6400 Series Triple Quad LC/MS Familiarization Guide 7
• Stop Time 2.5 min
• Post Time 3.0 min
INJECTOR
• Inj. Vol. 2.0 µL
• Injection Standard
• Draw Position 0.0 mm
UV DETECTOR
• Ch A 254 nm (4 nm BW on DAD)
• REF A (DAD only) 400 nm (80 nm BW)
COL THERM
• Temp 60 °C for the K6460 with an AJS ESI source
40 °C for ESI source
Table 2 LC parameters for sulfa drug mix (continued)
Parameter LC Parameter