Table of contents BÜCHI Labortechnik AG
iv Operation Manual SyncorePlus
5 Installation..........................................................................................................................20
5.1 Before installation .............................................................................................................................. 20
5.2 Installation site................................................................................................................................... 20
5.3 Establishing electrical connections.................................................................................................... 20
5.4 Securing against earthquakes ........................................................................................................... 21
5.5 Connecting the instrument to the control system............................................................................... 21
5.6 Installing the condenser..................................................................................................................... 21
5.6.1 Installing the condenser......................................................................................................... 22
5.6.2 Connecting the coolant to the condenser ..............................................................................23
5.6.3 Connecting the vacuum pump to the condenser ...................................................................23
5.6.4 Connecting the vacuum hose for the heater cover ................................................................23
5.6.5 Installing the cap nut (Polyvap and Analyst configuration only).............................................24
5.6.6 Installing the vapor sensor (Option)....................................................................................... 24
5.7 Installing the waste vessel (SPE configuration only) ......................................................................... 25
6 Preparing the instrument for a configuration .................................................................27
6.1 Preparing a Polyvap configuration..................................................................................................... 27
6.2 Preparing an Analyst configuration.................................................................................................... 29
6.3 Preparing a SPE configuration .......................................................................................................... 32
6.3.1 Position SPE advanced valves ..............................................................................................34
7 Operation............................................................................................................................35
7.1 Operating the control panel ............................................................................................................... 35
7.1.1 Layout of the control panel.....................................................................................................35
7.1.2 Status panel...........................................................................................................................35
7.1.3 Setting the evaporation temperature...................................................................................... 36
7.1.4 Setting the cooling water follow-up time ................................................................................36
7.2 Carrying out an evaporation (with control system) ............................................................................ 36
7.3 Carrying out an evaporation (without control system) ....................................................................... 37
7.3.1 Preparing the instrument........................................................................................................ 37
7.3.2 Starting an evaporation..........................................................................................................37
7.3.3 Ending an evaporation........................................................................................................... 38
7.3.4 Shutting down the instrument ................................................................................................38
8 Cleaning and servicing .....................................................................................................39
8.1 Regular maintenance work................................................................................................................ 39
8.2 Locking and unlocking the rotation .................................................................................................... 40
8.3 Moving and retrieving the heating plate into a pre-defined position .................................................. 40
8.4 Adjusting the unbalance compensation............................................................................................. 40
8.5 Testing the vortex movement ............................................................................................................ 41
9 Help with faults ..................................................................................................................42
9.1 Troubleshooting................................................................................................................................. 42
9.2 Error messages ................................................................................................................................. 43
9.3 Changing the fuse.............................................................................................................................. 45
10 Taking out of service and disposal..................................................................................46
10.1 Taking out of service.......................................................................................................................... 46
10.2 Disposal............................................................................................................................................. 46
10.3 Returning the instrument ................................................................................................................... 46
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