SAMPLE ANALYISIS- RAFFINATE
12. Connect the syringe to the solvent cap and pull plunger up to fill syringe. Fill
syringe with at least 10ml of solvent.
13. Invert the syringe so that the bubble floats to the tip. Depress the plunger to
remove the air bubbles and get the syringe volume to exactly 10ml. A tissue may
be used to catch any excess solvent.
NOTE: It is important to ensure the syringe has exactly 10ml of solvent for
accurate results.