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Shimadzu LC-40D X3 CL User Manual

Shimadzu LC-40D X3 CL
144 pages
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228-97197B
Sep. 2022
Solvent Delivery Module for Shimadzu
Liquid Chromatograph
LC-40D X3 CL
LC-40D XR CL
Instruction Manual
Read this manual thoroughly before you use the product.
Keep this manual for future reference.

Table of Contents

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Shimadzu LC-40D X3 CL Specifications

General IconGeneral
Data Sampling RateUp to 200 Hz
System ControlLabSolutions software
TypeHPLC System
Maximum Operating Pressure1034 bar
Maximum Pressure1034 bar
Flow Rate Range0.0001 mL/min
Flow Rate Accuracy±1% or 2 μL/min, whichever is greater
Flow Rate Precision<0.06% RSD
Autosampler Injection Volume0.1 to 100 μL
Detector TypesUV, Vis, PDA, Fluorescence, RID

Summary

Introduction

About This Manual

Provides a general overview and purpose of the instruction manual.

Related Documentation

Lists other manuals and documentation included with the product.

Important Notes

Highlights crucial points regarding manual usage and product handling.

Indications and Notices

Explains precaution symbols, general notices, and important information.

1 Overview

1.1 Features

Details key features of the LC system, including low flow pulsation, gradient modes, auto rinsing, and high-pressure flow.

1.2 Component Parts

Lists standard parts included with the instrument, with part numbers and quantities for verification.

1.3 Optional Parts

Describes optional units available for the instrument, such as gradient kits and mixers.

2 Parts Identification and Function

2.1 Front Panel

Identifies and describes the front panel elements, including the operation panel and power button.

2.2 Behind Front Cover

Details components located behind the front cover, such as pump heads, drain valve, and leak sensor.

2.3 Back Panel

Explains the connectors and switches on the back panel, including remote and PC connections.

2.4 Right Side and Bottom

Describes mounting holes and the leakage drain outlet on the right side and bottom of the instrument.

2.5 Operation Panel

Explains the operation panel layout, display area, LEDs, and direct keys for instrument control.

2.5.1 Display Area

Describes the information displayed on the initial screen, including flow rate, pressure, and status indicators.

2.5.2 Operation Area

Details the function of each key in the operation area, including pump, concentration, run, and purge keys.

3 Operation

3.1 Basic Operation Settings

Guides on setting flow rate, pressure limits, and compressibility for basic operation.

3.2 Instrument Operation Procedures

Covers preparation, constant flow, and constant pressure delivery modes.

3.3 Screen Types and Navigation

Overview of instrument screens and how to navigate between them.

3.4 Monitoring Screens

Explains screens for monitoring instrument status, flow, pressure, and diagnostics.

3.5 Auxiliary Functions Screen

Accesses auxiliary functions for parameter settings and operations, organized into groups.

3.6 VP Functions Screen

Accesses validation and instrument information, including product details and maintenance logs.

3.7 Creating Time Programs

Guides on creating automated sequences for solvent delivery using time programs.

3.8 Low-Pressure Gradient Delivery

Procedure for setting up and performing deliveries in low-pressure gradient mode.

3.9 System Controller Connection

Details on connecting and configuring the instrument with a system controller.

3.10 External Input/Output Terminals

Information on connecting external devices via input/output terminals.

4 Maintenance

4.1 Periodic Inspection and Maintenance

Necessity of periodic inspections for safe and proper instrument use.

4.2 Component Removal and Installation

Covers removal/installation of panel covers, filter holders, and pump heads.

4.3 Plunger Seal and Diaphragm Maintenance

Procedures for replacing plunger seals, backup rings, and diaphragms.

4.4 Check Valve and Filter Maintenance

Covers rinsing, replacing check valves, and inspecting/replacing line and suction filters.

4.5 Valve, Filter, and Tray Cleaning

Procedures for replacing drain valve, air filter, cleaning leak tray, and exterior.

5 Technical Information

5.1 LC-40D X3 CL Specifications

Specific technical parameters for the LC-40D X3 CL model, including flow rate and pressure.

5.1.2 LC-40D XR CL Specifications

Specific technical parameters for the LC-40D XR CL model, including flow rate and pressure.

5.1.3 Gradient System Specifications

Specifications for high-pressure and low-pressure gradient systems.

5.1.5 Other Specifications

Various other technical specifications, including operating temperature, dimensions, and power supply.

5.2 Maintenance Parts

Lists all parts required for maintenance, including consumables and replacement parts.

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