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5800
Agilent Technologies 5800 User Manual
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Operation
50
Agilent 5800 and 590
0 ICP-OES User's Guide
This page is intenionally blank.
49
51
Table of Contents
Default Chapter
3
Table of Contents
3
1 Safety Practices and Hazards
7
General
7
Verifying Safe State
8
Plasma
8
Heat, Vapors and Fumes
9
Compressed Gas Hazards
9
Electrical Hazards
10
Other Precautions
11
Warning Symbols
12
2 Introduction
15
Site Preparation Requirements
15
User Documentation
15
Conventions
16
Notes and Tips
16
ICP-OES Argon Gas Supply
16
Exhaust System
17
ICP-OES Instrument Cooling Air Supply
17
Water Chiller System
18
Drain Vessel
18
3 Installation
19
Agilent ICP-OES Instrument Overview
20
Instrument Status LED Color Coding
22
Front Power On/Off Button
22
ICP Expert Software
23
Connecting ICP Expert Software to the ICP-OES
24
Performing a Detector and Wavelength Calibration
24
Saving and Viewing the Calibration Data
25
Hardware Components Replacement
25
ICP-OES Torches
26
Torch Assembly and Disassembly
27
Assembly of the Semi-Demountable Torch
28
Assembly of the Fully Demountable Torch
31
Torch Disassembly
32
Accessories
35
Sps 4
35
Advanced Valve System (AVS) - AVS 4, AVS 6 and AVS 7
36
External Inlet Duct Adapter
36
Vapor Generation Accessory (VGA)
36
Multimode Sample Introduction System (MSIS)
36
Argon Humidifier
37
Isomist Programmable Temperature Spray Chamber
37
4 Operation
39
Analysis Checklist
39
Turning on the Instrument and Software
40
Turning on the Instrument for the First Time (or from Long Term Shutdown)
40
Running the Instrument from Standby
41
Preparing for Analysis
41
Performing a Detector and Wavelength Calibration
42
Creating/Opening a Worksheet
42
Creating a New Worksheet
42
Opening an Existing Worksheet
43
Creating a New Worksheet from a Template
43
Developing a Method
43
Running Samples
45
Printing a Report
45
Turning off the Instrument
46
Instrument Standby Mode with Argon on
46
Instrument Standby Mode with Argon off
46
Setting the Instrument to Standby Mode with Argon on or off
47
Turning off the Instrument for Long Term Shutdown
48
5 Maintenance and Troubleshooting
51
Routine
52
Cleaning
54
Torch Cleaning
54
Important
55
Acid Soak Cleaning Procedure for the Torch for Aqueous or Acid-Based Samples (One Piece and Semi-Demountable Torches)
56
Rinsing the Torch
59
Drying the Torch
61
Additional Checks after Cleaning
62
Troubleshooting
63
Spare Parts
63
Technical Support
64
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Agilent Technologies 5800 Specifications
General
Brand
Agilent Technologies
Model
5800
Category
Laboratory Equipment
Language
English
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