Exercise 1 – Develop an acquisition method
Task 1. Enter acquisition parameters and acquire data
Agilent 6400 Series Triple Quad LC/MS Familiarization Guide 9
Figure 2 Select Scan Type of MS2 Scan in the QQQ tab
Table 3 MS parameters for sulfa drug mix
Parameter Value (ESI) Value (AJS ESI)
• Inlet ESI (positive polarity) AJS ESI (positive polarity)
• Scan Type MS2 Scan MS2 Scan
• Delta EMV (+) 400 V 200 V
• Mass Range 100 to 400 100 to 400
• Cell Accelerator Voltage 7 V 7 V
• Gas Temp 350 °C 350 °C
• Gas Flow 12 L/min 10 L/min
• Nebulizer 50 psi 35 psi
• Sheath Gas Temperature not applicable 400 °C
• Sheath Gas Flow not applicable 12 L/min
• Nozzle Voltage not applicable 0 V
• Capillary Voltage positive 4000 V 4000 V
• Fragmentor 100 V 100 V
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