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Agilent Technologies G7035A User Manual
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114
5977 Series MSD Operation Manual
4
Operating in Chemical Ionization (CI) Mode
Figure 19
NCI autotune
113
115
Table of Contents
Default Chapter
3
About this Manual
3
Table of Contents
5
1 Introduction
10
5977 Series MSD Version
10
Abbreviations Used
11
The 5977 Series MSD
13
MSD Hardware Description
15
Important Safety Warnings
17
Hydrogen Safety
19
GC Precautions
19
Precautions
22
Safety and Regulatory Certifications
24
Electromagnetic Compatibility
26
Cleaning/Recycling the Product
27
Liquid Spillage
27
Moving or Storing the MSD
27
To Replace the Primary Fuses
28
2 Installing GC Columns
31
Columns
32
To Install a Capillary Column in a Split/Splitless Inlet
34
To Condition a Capillary Column
37
To Install a Capillary Column in the GC/MS Interface
38
To Prepare the Column Ends for a CFT Fitting
41
3 Operating in Electron Ionization (EI) Mode
46
Operating the MSD from the Data System
46
Operating the MSD from the LCP
46
Modes of Operation
46
LCP Status Messages
48
To View System Status During Startup
49
LCP Menus
50
The EI GC/MSD Interface
53
Before You Turn on the MSD
55
Pumping down
56
Controlling Temperatures
56
Controlling Column Flow
56
Venting the MSD
57
To View MSD Temperature and Vacuum in Manual Tune
58
To Set Monitors for MSD Temperature and Vacuum Status
59
To Set Analyzer Temperatures from the Instrument Control View
61
To Set the GC/MSD Interface Temperature from Masshunter
63
To Monitor High Vacuum Pressure
64
To Calibrate Column Flow Linear Velocity
66
To Tune the MSD in EI Mode
69
To Verify System Performance
71
To Perform High-Mass Testing (5977 Series Msds)
72
To Open the MSD Covers
75
To Vent the MSD
76
To Open the Analyzer Chamber
78
To Close the Analyzer Chamber
80
To Pump down the MSD in EI Mode
84
To Move or Store the MSD
86
4 Operating in Chemical Ionization (CI) Mode
90
General Guidelines
90
The CI GC/MSD Interface
91
CI Autotune
93
N/A Not Available
94
To Operate the CI MSD
95
To Switch from the Standard or Inert EI Ion Source to the CI Ion Source
96
To Switch from the Extractor EI Ion Source to the CI Ion Source
97
To Pump down the MSD in CI Mode
98
To Set up the Software for CI Operation
99
To Operate the Reagent Gas Flow Control Module
101
To Set up Methane Reagent Gas Flow
104
To Use Other Reagent Gases
106
To Switch from the CI Ion Source to the Standard or Inert EI Ion Source
109
To Switch from the CI Ion Source to the Extractor EI Ion Source
110
To Perform a PCI Autotune (Methane Only)
111
To Perform an NCI Autotune (Methane Reagent Gas)
113
To Verify PCI Performance
115
To Verify NCI Performance
116
To Monitor CI Mode High Vacuum Pressure
117
5 General Maintenance
119
Before Starting
120
Electrostatic Discharge
123
Maintaining the Vacuum System
125
Maintaining the Analyzer
126
To Remove the EI Ion Source
128
To Disassemble the Standard or Inert EI Ion Source
131
To Disassemble the Extractor EI Ion Source
134
To Clean the EI Ion Source
137
To Assemble a Standard or Inert EI Ion Source
142
To Assemble the Extractor EI Ion Source
145
To Replace a Filament in an EI Ion Source
148
To Install the EI Ion Source
150
To Replace the Electron Multiplier Horn
151
101 CI Maintenance
153
General Information
154
To Set up Your MSD for CI Operation
154
To Install the CI/Extractor Interface Tip Seal
155
To Remove the CI Ion Source
157
To Disassemble the CI Ion Source
159
To Clean the CI Ion Source
162
To Assemble the CI Ion Source
164
To Install the CI Ion Source
167
To Replace a Filament in a CI Ion Source
168
4
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Agilent Technologies G7035A Specifications
General
Brand
Agilent Technologies
Model
G7035A
Category
Measuring Instruments
Language
English
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