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Analytik Jena
Measuring Instruments
SPECORD 200
Analytik Jena SPECORD 200 User Manual
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11
13
Table of Contents
Table of Contents
3
Introduction
7
Safety Notes
8
Fig. 1-1 Sample Compartment
9
Care of Accessories
9
Sample Compartment of SPECORD
9
Basics of SPECORD Alignment
9
Adjustment of Zeroth Order
10
Changing the Position of the Carrying Rails
10
Fig. 1-2 Carrying Rails Mounted in Bottom Position
10
Universal Holder
13
Description and Use
13
Description
13
Fig. 2-1 Universal Holder
13
Fig. 2-2 Attaching and Clamping the Universal Holder
14
Using the Universal Holder
14
100 MM Cylindrical Cell (Absorption Tube)
15
Description
15
Inserting the 100Mm Cylindrical Cell
15
Fig. 3-1 100 MM Cylindrical Cell
15
Description and Use
15
Care and Transportation of Cylindrical Cell
16
Solid Sample Holder
17
Description and Use
17
Using the Holder and Inserting the Sample
17
Fig. 4-1 Solid Sample Holder
17
Fig. 4-2 Solid Sample in Holder Slide
17
Fig. 5-1 Holders for Cylindrical Cells
19
Fig. 5-2 10 MM Thermocell (Cylindrical)
19
Description and Use
19
Using the Holder for Cylindrical Cells
19
Description
19
Holder for Cylindrical Cells
19
Holder for Round Cells
21
Description and Use
21
Description
21
Using the Holder for Round Cells
21
Fig. 6-1 Holder for Round Cells
21
Holder for Semi-Microcells and Microcells
23
Description and Use
23
Holder for Semi-Microcells
23
Fig. 7-1 Holder for Semi-Microcells
23
Adjustable Holder for Microcells, Non-Thermostatted, (8.5 MM / 15 MM Beam Height)
24
Fig. 7-2 Holder for Microcells (Adjustable) with Beam Heights of 8.5 MM and 15 MM (Adjustable)
24
Fig. 7-3 Holder for Microcells (Adjustable)
25
Adjustable Holder for Microcells, Non-Thermostatted (8.5 MM Beam Height)
25
Thermostatted Cell Holder
27
Description and Use
27
Description
27
Using the Thermostatted Cell Holder
27
Connection and Installation in Sample Compartment
27
Fig. 8-1 Thermostatted Cell Holder
27
Inserting the Magnetic Stirrer
28
Fig. 8-2 Inserting the Magnetic Stirrer Coil
28
Fig. 9-2 HPLC Cell
31
Adjustable Cell Holder, Thermostatted
31
Fig. 9-1 Adjustable Thermostatted Cell Holder
31
Inserting the Cell
32
Aligning the Cell
32
6-Cell Changer, Thermostatted
33
Description and Use
33
Design
34
Fig. 10-1 Thermostatted Cell Holder and Driving Unit
34
Fig. 10-2 Thermostatted Cell Holder with Magnetic Stirrer
34
Installation and Insertion in Sample Compartment
35
Installation of Magnetic Stirrers
35
Fig. 10-3 Installation of Magnetic Stirrer
35
Fig. 10-4 Cell Holder with Quick-Lock Tube Coupling
36
Connection to a Thermostat
36
Installation in Sample Compartment
37
Fig. 10-5 Installation of Cell Changer
37
Operation
38
Settings in Measurement Parameters Window
38
Fig. 10-6 Accessories Tab - Cell Changer
39
Measurements with the 6-Cell Changer
40
Operating Modes of Cell Changers
40
Fig. 10-7 Cell Changer -Operating Modes
40
8-Cell Changer
43
Removal of Transport Lock on Non-Temperature-Controlled 8-Cell Changer
43
Fig. 11-1 Transport Lock on Non-Temperature-Controlled 8-Cell Changer
43
Fig. 11-2 8-Cell Changer
44
Installation of 8-Cell Changer
44
Design of 8-Cell Changer
44
Operation of the 8-Cell Changer
46
Software Settings
46
Measurements with the 8-Cell Changer
47
Use of Two 8-Cell Changers
47
Staggered Operation of Two 8-Cell Changers for more than 8 Samples
48
Synchronous Operation of Two 8-Cell Changers
49
Cell Carousel
51
Description and Use
51
Design
51
Fig. 12-1 Cell Carousel - Driving Unit and Sample Tray
51
Fig. 12-2 Cell Carousel Installed in Sample Compartment
52
Installation in Sample Compartment
52
Operation
53
Peltier Temperature-Controlled Cell Holders/Cell Changers
55
Peltier Temperature-Controlled Cell Holder, Air-Cooled
56
Fig. 13-1 Peltier Temperature-Controlled 1X Cell Holder with Control Unit
56
Safety Notes
57
Technical Data of Peltier Temperature-Controlled Cell Holder, Air-Cooled
58
Design of Peltier-Temperature-Controlled Cell Holder, Air-Cooled
59
Fig. 13-2 Peltier Temperature-Controlled Cell Holder, Air-Cooled
59
Installation of Peltier Temperature-Controlled Cell Holder in SPECORD
60
Fig. 13-3 Installation of the PTC 100 in the Sample Compartment
60
Fig. 13-4 Sample Compartment Cover with Cables Threaded through
61
Care
62
Fig. 13-5 Bottom of Peltier Temperature-Controlled 1X Cell Holder
63
Safety Notes for the Use of the Peltier Temperature-Controlled Cell Holder with Heat Exchanger
64
Peltier Temperature-Controlled Cell Holder with Heat Exchanger
64
Technical Data of Peltier Temperature-Controlled Cell Holder with Heat Exchanger
66
Design of Peltier Temperature-Controlled Cell Holder with Heat Exchanger
68
Installation of the Cell Holder in the SPECORD
68
Fig. 13-6 Peltier Temperature-Controlled Cell Holder with Heat Exchanger
68
Fig. 13-7 Cell Temperature Measuring Sensor PT100
70
Peltier Temperature-Controlled 6-Cell Changer
71
Use
71
Fig. 13-8 Peltier Temperature-Controlled 6-Cell Changer with SPECORD ® 210
71
Safety Notes
72
Technical Data of Peltier Temperature-Controlled 6-Cell Changer
73
Design of Peltier Temperature-Controlled 6-Cell Changer
75
Fig. 13-9 Design of Peltier Temperature-Controlled 6-Cell Changer
75
Installation of the Peltier-Temperature-Controlled 6-Cell Changer
76
Fig. 13-10 Installation of Peltier Temperature-Controlled 6-Cell Changer in the SPECORD
76
Fig. 13-11 Cell Measuring Sensor for the Peltier Temperature-Controlled 6-Cell Changer
78
Settings in Winaspect ® Software
79
Fig. 13-12 Options for Peltier Temperature-Controlled 6-Cell Changer for SPECORD
79
Measurement Procedure
80
Peltier Temperature-Controlled 8-Cell Changer
81
Safety Notes
82
Technical Data of Peltier Temperature-Controlled 8-Cell Changer
83
Design of Peltier Temperature-Controlled 8-Cell Changer
85
Fig. 13-13 Design of Peltier Temperature-Controlled 8-Cell Changer
85
Installation of Peltier Temperature-Controlled 8-Cell Changer
86
Fig. 13-14 Cell Measuring Sensor for the Peltier Temperature-Controlled 8-Cell Changer
89
Fig. 13-15 Options for Peltier Temperature-Controlled 8-Cell Changer for SPECORD
90
Settings in Winaspect ® Software
90
Measurement Procedure
91
Connection and Operation of Temperature Control Unit
92
Connecting the Temperature Control Unit
92
Fig. 13-16 Back Panel of Temperature Control Unit
92
Settings on Temperature Control Unit
93
Fig. 13-17 Front Panel of Temperature Control Unit
93
Fig.13-18
94
Replacing Fuses on the Temperature Control Unit
95
Connection and Operation of the Heat Exchanger
96
Preparing the Coolant
96
Connecting the Heat Exchanger
96
Fig. 13-19 Heat Exchanger, Front Panel
96
Fig.13-20
96
Replacing Fuses on the Heat Exchanger
97
Cassette Sipper
99
Intended Use
99
Design of Cassette Sipper
99
Fig. 14-1 Design of Cassette Sipper
99
Mounting the Cassette Sipper
100
Mounting the Tube Set
100
Fig. 14-2 Tube Set for Cassette Sipper
100
Mounting the Sipper in the Sample Compartment
101
Fig. 14-3 Cassette Sipper Mounted in SPECORD
101
Adjusting the Flow Cell
102
Sample Measurement
103
Settings on the PC
103
Fig. 14-4 Device Driver, Accessories Tab with Selected Sipper Option
103
Performing a Sample Measurement
104
Care and Maintenance
105
APG 53/100 XYZ Autosampler
107
Intended Use
107
Safety Notes
107
Design and Installation of the APG 53/100
108
Fig. 15-1 APG 53 (Front View)
108
Fig. 15-2 Connections of APG53 (Rear Panel)
109
Connecting the XYZ Autosampler to the SPECORD
110
Sample Measurement
112
Fig. 15-3 Accessories Tab - APG 53 Selected
112
Finding the Appropriate Pump Time
113
Fig. 16-1 Fiber-Coupling Adapter with Measuring Probe
115
Design and Function of Fiber Coupling with Measuring Probe
115
Description and Use
115
Fiber Coupling for Measuring Probes
115
Design and Function of the Fiber Coupling with SMA Connectors
116
Installation of the Adapter in the Sample Compartment
116
Alignment of Fiber Coupling
116
Absolute Reflectance Attachment
117
Description and Use
117
Design
117
Fig. 17-1 Absolute Reflectance Attachment
117
Installation in Sample Compartment
118
Operating Principle
118
Fig. 17-2 Beam Geometry in Absolute Reflectance Attachment
118
Adjustment
119
Measurements with the Absolute Reflectance Attachment
119
Care and Maintenance
120
Variable Angle Reflectance Attachment
121
Description and Use
121
Design and Operating Principle
121
Fig. 18-1 Reflectance Attachment with Large Sample Table
121
Fig. 18-2 Mirror and Small Tabletop
122
Fig. 18-3 Optical Path in Reflectance Attachment (Front View)
122
Installation in Sample Compartment
123
Adjusting the Angle of Reflection
123
Measuring with the Reflectance Attachment
123
Calculating the Reflectance
123
Calculating Pathlength and Refractive Index
124
Fig. 18-4 Example of Interferences at an Angle of Reflection Θ = 60
124
Technical Data
125
Care and Maintenance
125
Integrating Sphere
127
Description and Use
127
Design of Integrating Sphere
128
Fig. 19-1 Integrating Sphere with Accessory Items
128
Measurements with the Integrating Sphere
129
Transmittance Measurements
129
Fig. 19-2 Optical Path in Transmittance Measurements
130
Reflectance Measurements
131
Fig. 19-3 Optical Path in Reflectance Measurements
132
Fig. 19-4 Integrating Sphere with Sample-Loading Fixture
133
Technical Data
135
Figures
137
4
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Analytik Jena SPECORD 200 Specifications
General
Brand
Analytik Jena
Model
SPECORD 200
Category
Measuring Instruments
Language
English
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