Analytik Jena SPECORD S600 User Manual

Accessories
UV VIS Spectrophotometer
SPECORD S600
User Manual

Analytik Jena SPECORD S600 Specifications

General

Brand	Analytik Jena
Model	SPECORD S600
Category	Measuring Instruments
Language	English

Summary

Notes for users

Safety instructions

Essential safety warnings for the SPECORD S600 basic equipment and proper use of accessories.

Alignment of accessories

Procedure for aligning accessories in the beam path using energy measurements for maximum signal.

Cell holder, 100 mm

Inserting the cell correctly

Correct procedure for cell placement in the 100mm holder for accurate readings.

Cell holder, 10 mm, thermostated

Holder for round cells

Installing the round cell holder in the sample chamber

Inserting the round cell

Proper method for inserting round cells into the holder for accurate positioning.

Adjustable cell holder for microcells

Installing the holder for microcells

Adjusting the cell holder

Procedure for realigning the adjustable microcell holder for optimal beam path.

6-cell changer

Installing the 6-cell changer in the sample chamber

Adjusting the 6-cell changer

Computer-assisted adjustment of the 6-cell changer for optimal cell positioning.

8-cell changer

Installing the 8-cell changer in the sample chamber

Inserting the cell changer

Adjusting the 8-cell changer

Computer-assisted adjustment of the 8-cell changer for optimal cell positioning.

Cell carousel

Installing the cell carousel in SPECORD S600

Measurement with the cell changer

14.1 Configuring parameters for the cell changer

Setting up measurement parameters for the cell changer.

Measurement without reference sample in the cell changer

Kinetic measurements with the cell changer

Using the cell changer for kinetic measurements in fast and slow modes.

Peltier-tempered accessories

15.1 General safety instructions for Peltier-tempered accessories

Essential safety warnings for all Peltier-tempered accessories.

Peltier temperature-controlled cell holder, air-cooled

Safety instructions for the use of the Peltier-tempered cell holder

Critical safety guidelines for using the air-cooled Peltier cell holder.

15.2.1 Technical data and layout

15.2.2 Installing the cell holder in the sample chamber

15.2.3 Using the cell sensor

Instructions for using the cell sensor with the Peltier cell holder.

15.2.4 Temperature control

Configuring temperature control settings for the Peltier cell holder.

Simultaneous temperature control

Configuring heating/cooling ramps using the 'Simultaneous' mode.

Peltier-tempered cell holder with external heat exchanger

Safety instructions for the use of the Peltier-tempered cell holder with heat exchanger

Critical safety guidelines for using the Peltier cell holder with an external heat exchanger.

15.3.1 Technical data and layout

15.3.2 Installing the cell holder in the sample chamber

Inserting the cell holder in the sample chamber

Inserting the cell

15.3.3 Temperature control

Configuring temperature control for the holder with external heat exchanger.

Peltier tempered 6- and 8-cell changers

Safety instructions for the use of the Peltier-tempered cell changer

Critical safety guidelines for Peltier 6- and 8-cell changers.

15.4.1 Technical data and layout

15.4.2 Installing the cell changer in the sample chamber

Adjusting the Peltier-tempered cell changers

Using the cell sensor

Instructions for using the cell sensor with Peltier cell changers.

Removing the cell changer from the sample chamber

15.4.3 Carrying out measurements with Peltier-tempered cell changers

Usage procedures for Peltier 6/8-cell changers.

Fix temperature control

Setting up constant temperature control for Peltier cell changers using 'Fix' mode.

Cyclical temperature mode

Activating and configuring temperature values using 'Cyclic' mode for Peltier cell changers.

Temperature control unit for Peltier-tempered accessories

Configuring the start temperature at the temperature control unit

Connecting the temperature control unit

Recording the inside cell temperature

Heat exchanger for Peltier-tempered accessories

Connecting the heat exchanger

Cartridge sipper system

Installing the cartridge sipper system in the sample chamber

Adjusting the flow cell

Determining the optimum pumping time for the cartridge sipper system

Measuring with the cartridge sipper system

Configurations in the measuring parameters for the sipper system.

Carrying out the sample measurement

Procedures for carrying out sample measurements with the sipper.

Absolute reflectance attachment

Functional principle

Installing the attachment in the sample chamber

Adjusting the attachment

Measurements with the attachment

Procedures for taking measurements with the reflectance attachment.

Reflection measuring attachment 11° - 60°

Installing the reflection measuring attachment in the sample chamber

Adjusting the reflection angle

Measurements with the reflection measuring attachment

Procedures for taking measurements with the reflection attachment.

Calculation of the path length and refractive index

Calculating path length and refractive index using measurement data.

Integrating sphere

Technical data

Vertical installation

Horizontal installation

20.1 Installing the integrating sphere in the sample compartment

20.2 Using the integrating sphere

20.2.1 Transmittance measurements

Procedure for performing transmittance measurements with the integrating sphere.

20.2.2 Reflectance measurements

Procedures for performing reflectance measurements with the integrating sphere.

Preparing the measurement

Loading powder samples

Reflectance measurement procedure

Step-by-step procedure for reflectance measurements.

20.3 Lamp replacement

Fiber coupling with SMA connections or with measuring sensors

Installing the adapter in the sample chamber

Adjusting the adapter