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multi EA 4000
Analytik Jena multi EA 4000 User Manual
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multi EA
4000
Elementa
ry anal
yzer
C, S and Cl solids an
alysis
Operating manual
2
Table of Contents
Default Chapter
3
Table of Contents
3
1 Basic Information
9
User Manual Notes
9
Intended Use
9
Warranty and Liability
10
2 Technical Data
11
3 Safety Instructions
13
Standards and Directives
13
Symbols and Signal Words Used
13
Safety Markings on the Analyzer
14
Technical Condition
14
Requirements for the Operating Personnel
15
Safety Instructions, Transport and Installation
15
Safety Instructions - Operation
16
General
16
Safety Instructions - Protection against Explosion and Fire
17
Safety Instructions - Electrical Equipment
17
Safety Instructions for Compressed Gas Containers and Systems
17
Handling of Auxiliary and Operating Materials
18
Safety Instructions - Service and Repair
22
Behavior During Emergencies
22
4 System Design
23
Comprehensive Overview
23
Basic Device
23
Combustion System
23
Pneumatic and Hose System
24
Fig. 1 Horizontal Furnace of the Basic Device Multi EA 4000
24
Components for Measuring Gas Drying and Cleaning
25
Fig. 2 Flow Meters at the Basic Device Multi EA 4000
25
Fig. 3 Dust Trap at the Combustion Furnace
25
Indicator and Control Elements, Connections
26
Fig. 4 Drying Tube and Halide Trap
26
Fig. 5 Status Indicators at the Basic Device Multi EA 4000
26
Fig. 6 Control Elements Behind the Front Doors of the Multi EA 4000
27
Fig. 7 Connections on the Right-Hand Side of the Multi EA 4000
27
C/S Module
28
Fig. 8 Connections on the Rear of the Multi EA 4000
28
Fig. 9 Indictors and Connections at the C/S Module
29
Cl Module
30
Coulometer Assembly and Measuring Cell
30
Fig. 10 Cl Module
30
Fig. 11 Layout of the Measuring Cell
31
Combustion Tube and Measuring Gas Drying
32
Fig. 12 Combination Electrode for Measuring Cell
32
Fig. 13 Quartz Combustion Tube with Gas Airlock
32
Measuring Gas Cleaning
33
Fig. 14 Sulfuric Acid Containers for Measuring Gas Drying
33
Fig. 15 Halide Trap and Adsorption Tube in the Cl Module
33
Connections
34
Fig. 16 Connections of the Cl Module in Combination with a C/S Module
34
Fig. 17 Connections for the Coulometric Cell at the Inside Panel of the Cl Module
34
Automatic TIC Solids Module
35
Technical Data
35
Fig. 18 Automatic TIC Solids Module
35
Layout
36
Fig. 19 TIC Reactor
36
Fig. 20 Hose Pumps at the Automatic TIC Solids Module
37
Fig. 21 Measuring Gas Drying and Cleaning at the Automatic TIC Solids Module
38
Fig. 22 Dust Trap before the Measuring Gas Inlet of the C/S Module
38
Fig. 23 Connections at the Automatic TIC Solids Module
39
Manual TIC Solids Module
40
Technical Data
40
Fig. 24 Manual TIC Solids Module
40
Layout of the Manual TIC Solids Module
41
Fig. 25 TIC Reactor of the Manual TIC Solids Module
41
Fig. 26 Flow Meter for Oxygen Flow
41
Fig. 27 Metering Pump for Acid at the Manual TIC Solids Module
42
Fig. 28 Components for Measuring Gas Drying and Cleaning at the Manual TIC Solids Module
43
Fig. 29 Connections at the Manual TIC Solids Module
43
Other Optional Accessories
44
Sampler
44
Flame Sensor
44
Scales
44
5 Measuring Method
45
TC/TS Analysis
45
TIC Analysis
45
TOC Analysis
46
Differential Method for the TOC Analysis
46
Direct Method for the TOC Analysis
46
Carbon Detection after Pyrolysis: TC-EC (Optional)
47
Data Analysis in the C/S Mode
47
Calibration Techniques
47
Day Factor
48
Method Characteristics
48
Other Calculations
49
Cl Detection
49
Data Analysis in the Cl Mode
50
End Point Routine
50
Measuring with Split / Split Factor
50
Analysis
50
6 First Commissioning
51
Site Requirements
51
Installation Conditions
51
Space Requirement
51
Energy Supply
51
Gas Supply
52
Unpacking and Placing the Analyzer
52
7 Operation
53
Switching on / Heat-Up Phase / Setup
53
C/S Measurement
54
Preparing the Multi EA 4000 and C/S Module
54
Fig. 30 Checking the Halide Trap and Drying Tube
56
Performing the C/S Measurement
57
Carbon Detection after Pyrolysis
59
Preparing the Multi EA 4000 and C/S Module
59
Performing the Carbon Detection after Pyrolysis
59
Cl Detection
61
Preparing the Multi EA 4000 for Cl Measurements
61
Preparing the Electrolyte Solution
66
Making the Measuring Cell Available
67
End Point Routine
68
Performing the Cl Measurement
69
Checking the Splitting Ratio
71
Cauterizing the Quartz Boat
72
TIC/TOC Detection with Automatic TIC Solids Module
73
Preparing the Automatic TIC Solids Module for the Analysis
73
Fig. 31 Individual Components for the Connection between the TIC Reactor and Ceramic Tube
73
Required Reagents
76
Performing the TIC Detection with the Automatic TIC Solids Module
76
Performing the TOC Detection in Accordance with the Differential Method Using the Automatic TIC Solids Module (Recommended Method)
78
TOC Measurement with Direct Detection
80
TIC Detection with the Manual TIC Solids Module
82
Prepare the Manual TIC Solids Module and Analyzer
82
Performing the TIC Measurement
82
8 Maintenance and Care
86
Basic Device Multi EA 4000
86
Clean and Maintain the Device
86
Check the Hose Connections
86
Fig. 32 Hose Connection at the Halogen Trap
86
Operation with C/S Module
87
Check and Replace the Ceramic Tube
87
Cleaning the Dust Trap
88
Replacing the Desiccant in the Drying Tube
90
Replacing the Halide Trap
91
Operation with Cl Module
92
Replacing the Sulfuric Acid/Cleaning the Sulfuric Acid Container
92
Servicing/Replacing the Quartz Glass Combustion Tube
93
Servicing the Combination Electrode
94
Servicing the Measuring Cells
96
Replacing the Adsorption Agent
96
Operation with Automatic TIC Solids Module
97
Clean the TIC Reactor of the Automatic TIC Solids Module
97
Cleaning the Condensation Coil
99
Removing and Replacing the Pump Hose
100
Cleaning the Condensate Container
102
Operation with Manual TIC Solids Module
103
Clean the TIC Reactor at the Manual TIC Solids Module
103
Replacing the Water Traps
103
9 Fault Removal
105
General Information
105
Error Messages in Multiwin
105
Indications in the Window DEVICE
111
Fig. 33 Window STATUS ANALYZER
111
Equipment Fault
113
Basic Device
113
C/S Module
113
Cl Module
115
Device Communication Errors
116
Analytical Problems
117
C/S Detection
117
Cl Detection
118
TIC Detection (Automatic TIC Solids Module)
119
TIC Detection (Manual TIC Solids Module)
119
Measurements in Pyrolysis Mode (EC)
120
10 Transport and Storage
121
Transport
121
Preparing the Analyzer for Transport
121
Transport Notes
122
Moving the Analyzer in the Laboratory
122
Storage
123
Recommissioning after Transport or Storage
124
Installing the Multi EA 4000 C/S
124
Fig. 34 Hose Diagram for Multi EA 4000 C/S
125
Fig. 35 Hose Diagram Multi EA C/S for Measurement in Pyrolysis Mode
126
Installing the Multi EA 4000 Cl
127
Fig. 36 Hose Diagram Multi EA Cl
128
Installing the Multi EA 4000 C/S Cl
129
Fig. 37 Hose Diagram Multi EA C/S Cl for C/S Measurements with Ceramic Tube and Oxygen Airlock
130
Fig. 38 Hose Diagram Multi EA C/S Cl for Cl Measurements with Quartz Tube and Argon Connection
131
Fig. 39 Hose Diagram Multi EA C/S Cl for Measurement in Pyrolysis Mode
132
Installing the Automatic TIC Solids Module
133
Fig. 40 Hose Diagram of the Automatic TIC Solids Module
134
Fig. 41 Hose Diagram Multi EA C/S with Connected Automatic TIC Solids Module
135
Installing the Manual TIC Module
136
Fig. 42 Hose Diagram Multi EA C/S with Manual TIC Solids Module
137
Fig. 43 Hose Diagram Multi EA C/S Cl with Manual TIC Solids Module
138
Connecting and Using the Sampler
139
Installing and Adjusting the Autosampler FPG 48
139
Filling the Sampler FPG 48
143
Measurement Cancellation When Using the Sampler FPG 48
143
Retrofitting the Sampler FPG 48 with a Boat Sensor
143
Retrofitting the Sampler FPG 48 with a Boat Storage
144
Fig. 44 Retrofit Kit for FPG 48 to Use the Boat Storage
144
Using the Manual Sample Feed
146
Connecting and Using the External Scales
147
11 Disposal
148
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Analytik Jena multi EA 4000 Specifications
General
Brand
Analytik Jena
Model
multi EA 4000
Category
Measuring Instruments
Language
English
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