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Analytik Jena multi EA 4000 User Manual

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multi EA 4000
Elementary analyzer
C, S and Cl solids analysis
Operating manual

Table of Contents

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Analytik Jena multi EA 4000 Specifications

General IconGeneral
BrandAnalytik Jena
Modelmulti EA 4000
CategoryMeasuring Instruments
LanguageEnglish

Summary

Basic Information

Intended Use

Details the analyzer's application for C, S, Cl detection in solids and paste-like samples.

Warranty and Liability

Outlines warranty terms, liability, and exclusions for misuse or unauthorized modifications.

Technical Data

General and Procedural Characteristics

Details analyzer specs: dimensions, mass, digestion principle, methods, gas supply.

Electrical and Environmental Specifications

Covers connection voltage, power, PC interface, and operating/storage conditions.

Minimum Equipment and Cl Module Data

Lists minimum system requirements and Cl module technical data.

Safety Instructions

Symbols and Signal Words

Defines warning symbols (Warning, Caution, Hot Surface, Electric Shock) and their meanings.

Safety Markings on the Analyzer

Describes safety symbols attached to the analyzer and their importance.

Technical Condition

Emphasizes maintaining the analyzer's technical safety and operational condition.

Operating Personnel Requirements

Details qualifications, training, and responsibilities for operating personnel.

Transport and Installation Safety

Covers safety during transport, installation, and general precautions.

General Operation Safety

General safety rules for operating the analyzer, including equipment checks.

Explosion and Fire Protection

Safety guidelines to prevent explosions and fires during operation.

Electrical Equipment Safety

Safety rules for working with the analyzer's electrical components.

Compressed Gas Systems Safety

Safety precautions for handling compressed gases used by the analyzer.

Handling Auxiliary and Operating Materials

Guidelines for safe handling of chemicals and materials used with the analyzer.

Service and Repair Safety

Safety guidelines for performing maintenance and repair tasks on the analyzer.

Behavior During Emergencies

Procedures and precautions to follow during emergency situations.

System Design

Comprehensive Overview

Describes the modular design and main components of the multi EA 4000 system.

Basic Device Components

Details the main components of the analyzer's basic device.

Combustion System

Explains the furnace, combustion tube, and gas supply for digestion.

Pneumatic and Hose System

Describes the hose system and gas flow control mechanisms.

Gas Drying and Cleaning Components

Explains dust trap, drying tube, and halide trap for gas conditioning.

Indicator and Control Elements

Identifies LEDs, switches, and connection points on the analyzer's front and rear.

C/S Module

Details C/S module versions, detectors, and measurement principles (VITA method).

Cl Module

Lists main components of the Cl module and its control electronics.

Cl Module Measuring Cell

Describes the two versions of the measuring cell and their specifications.

Cl Module Combustion Tube and Gas Drying

Explains the quartz tube, gas airlock, and drying system for Cl detection.

Cl Module Gas Cleaning

Details the halide trap and adsorption tube for cleaning the measuring gas.

Cl Module Connections

Shows connections for the Cl module, both standalone and with C/S module.

Automatic TIC Solids Module

Introduces the automatic TIC solids module for TIC/TOC detection.

Automatic TIC Solids Module Technical Data

Provides technical specifications for the automatic TIC solids module.

Automatic TIC Module Layout

Details the TIC reactor and pneumatic/hose system of the automatic TIC module.

TIC Module Gas Drying and Cleaning

Details condensation coil, drying tube, and halide trap for the TIC module.

Automatic TIC Solids Module Connections

Shows rear connections for the automatic TIC solids module.

Manual TIC Solids Module

Introduces the manual TIC solids module for TIC detection.

Manual TIC Solids Module Technical Data

Provides technical specifications for the manual TIC solids module.

Manual TIC Module Layout

Details the TIC reaction chamber and gas flow adjustment.

Manual TIC Module Acid Supply

Details the acid metering pump and supply for the manual TIC module.

Manual TIC Module Gas Drying and Cleaning

Explains drying and cleaning components for the manual TIC module.

Manual TIC Solids Module Connections

Shows connections for the manual TIC solids module.

Other Optional Accessories

Covers sampler, flame sensor, and external scales.

Sampler (Autosampler FPG 48 and Manual Feed)

Describes the autosampler FPG 48 and manual feed for sample supply.

Flame Sensor

Explains the optional flame sensor for Cl detection.

External Scales

Describes the use of external scales for automatic weight transfer.

Measuring Method

TC/TS Analysis

Explains simultaneous detection of Total Carbon and Total Sulfur.

TIC Analysis

Details the detection of Total Inorganic Carbon in samples.

TOC Analysis

Explains Total Organic Carbon analysis methods (Differential/Direct).

Differential TOC Method

Describes the differential method for TOC analysis.

Direct TOC Method

Describes the direct method for TOC analysis.

Carbon Detection After Pyrolysis (TC-EC)

Explains the optional TC-EC detection method after pyrolysis.

C/S Mode Data Analysis

Details calibration methods and functions for parameters.

Day Factor for Calibration

Explains the use of a day factor to check and correct calibrations.

Method Characteristics

Defines terms like standard deviation, variation coefficient, and correlation coefficient.

Other Calculation Methods

Covers average value, standard deviation, and boat blank value calculations.

Cl Detection Method

Explains the process of chlorine detection and its reaction equations.

Cl Mode Data Analysis

Explains end point routine, split factor measurement, and analysis reporting.

First Commissioning

Site Requirements

Specifies environmental and location requirements for analyzer installation.

Space Requirement

Outlines the necessary space for the analyzer and peripherals.

Energy Supply

Details electrical connection requirements and safety precautions.

Gas Supply

Covers responsibilities for gas supply and connection hoses.

Unpacking and Placing the Analyzer

Instructions for safely unpacking and installing the analyzer.

Operation

Switching On, Heat-Up, and Setup

Step-by-step guide for switching on, setup, and warm-up phases.

C/S Measurement Preparation

Instructions for fitting the ceramic tube into the furnace for C/S measurements.

Halide Trap and Drying Tube Check

How to check and prepare the halide trap and drying tube.

Performing C/S Measurement

Step-by-step guide to perform a C/S measurement.

Carbon Detection After Pyrolysis Preparation

Preparation steps for carbon detection after pyrolysis.

Performing Carbon Detection After Pyrolysis

Step-by-step guide for performing carbon detection after pyrolysis.

Cl Measurement Preparation

Instructions for inserting the quartz tube into the furnace for Cl detection.

Flame Sensor and Sulfuric Acid Container Connection

Steps for connecting the optional flame sensor and sulfuric acid container.

Electrolyte Solution Preparation

Provides the procedure for preparing the electrolyte solution for Cl detection.

Measuring Cell Availability

Instructions for filling and connecting the measuring cell.

End Point Routine

Describes performing the end point routine for the coulometric measuring cell.

Performing Cl Measurement

Step-by-step guide for performing a Cl measurement.

Splitting Ratio Check

How to check and correct the splitting ratio for Cl measurements.

Quartz Boat Cauterization

Instructions for cauterizing quartz boats before use or after contamination.

Automatic TIC Solids Module Preparation

Steps to prepare the automatic TIC solids module and attach the reactor.

Required Reagents for TIC Detection

Lists the reagents needed for TIC detection.

Performing TIC Detection (Automatic)

Step-by-step guide for performing TIC detection.

TOC Detection (Differential Method)

Guide for performing TOC detection using the differential method.

TOC Measurement (Direct Detection)

Step-by-step guide for performing TOC detection using the direct method.

Manual TIC Solids Module Preparation

Steps to connect and prepare the manual TIC solids module.

Performing TIC Measurement (Manual)

Step-by-step guide for performing TIC detection with the manual module.

Maintenance and Care

Basic Device Maintenance

Covers maintenance intervals, cleaning, and hose connection checks.

C/S Module Maintenance

Includes maintenance intervals, ceramic tube check, and dust trap cleaning.

Desiccant and Halide Trap Replacement

Guides for replacing desiccant in drying tubes and halide trap components.

Cl Module Maintenance

Covers maintenance intervals, sulfuric acid handling, and electrode servicing.

Measuring Cell and Adsorption Agent Servicing

Instructions for servicing measuring cells and replacing adsorption agent.

Automatic TIC Solids Module Maintenance

Covers maintenance intervals and cleaning of TIC reactor and condensation coil.

Pump Hose and Condensate Container Maintenance

Guides for replacing pump hoses and cleaning condensate containers.

Manual TIC Solids Module Maintenance

Covers maintenance intervals, TIC reactor cleaning, and water trap replacement.

Fault Removal

General Information and Error Messages

Info on log files and common multiWin error messages with causes/remedies.

Device State Indications

Explains status indicators and color meanings in the DEVICE STATE window.

Equipment Faults (Basic Device and C/S Module)

Lists common errors for basic device and C/S module with solutions.

Analytical Problems (C/S, Cl, TIC Detection)

Discusses common analytical problems and solutions for various detection methods.

Pyrolysis Mode (EC) Measurement Problems

Common problems and solutions for EC measurements in pyrolysis mode.

Transport and Storage

Analyzer Transport Preparation

Safety precautions and steps for preparing the analyzer for transport.

Transport Notes and Moving Analyzer

General notes for transport and safety instructions for moving within the lab.

Analyzer Storage Requirements

Specifies environmental conditions and procedures for storing the analyzer.

Recommissioning After Transport/Storage

Details connections for installing modules after transport or storage.

Connecting and Using the Sampler

Steps for connecting and adjusting the FPG 48 autosampler.

Sampler Gripper Adjustment

How to adjust gripper positions (sliding, ejection rail) using software.

Sampler Filling and Retrofitting

Instructions for filling sampler, handling cancellations, and retrofitting sensors.

Retrofitting Sampler with Boat Storage

Steps for retrofitting the sampler with a boat storage.

Using the Manual Sample Feed

Instructions for using the manual sample feed.

External Scales Connection and Use

Steps for connecting and using external scales for sample weight transfer.

Disposal

Environmental Protection Guidelines

General guidance on proper waste disposal according to legal guidelines.

Disposal of Sulfuric Acid

Disposal instructions for neutralized sulfuric acid.

Disposal of Magnesium Perchlorate

Disposal instructions for neutralized magnesium perchlorate.

Analyzer and Component Disposal

Disposal instructions for the analyzer and its electronic components.

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