Analytik Jena SPECORD S600

To Next Page

To Previous Page

Service:

Analytik Jena AG

Kundendienst

Konrad

-Zuse-Str. 1

07745 Jena

Germany

Phone:

Hotline: + 49 (0) 3641 / 77-7407

Fax: + 49 (0) 3641 / 77-7449

-Mail: service@analytik-jena.de

General information about Analytik Jena AG

on the internet: http://www.analytik-jena.de

Copyrights and Trademarks

SPECORD and WinASPECT are registered trademarks of Analytik Jena AG.

Microsoft, Windows XP/VISTA/7/8, MS Excel are registered trademarks of Microsoft Corp.

The identification with ® or TM is omitted in this manual.

Documentation number: 211:512.23

Edition – September 2014

Technical documentation made by:

Analytik Jena AG

This documentation describes the state of this product at the time of publishing. It need not

necessarily agree with future versions of the product.

Subject to change!

Main Page

Default Chapter3
- Table of Contents3
1 Notes for Users7
- Notes on this Manual7
- Safety Instructions7
- Caring for Accessories8
- The Sample Chamber Design of the SPECORD S6008
- Fig. 1-1 Design of the SPECORD S6009
- Fig. 1-2 Universal Holder9
- Fig. 1-3 Universal Holder Installed in SPECORD S6009
  - Converting the Sample Chamber10
- Fig. 1-4 Positions of the Support Rods in the Sample Chamber10
  - Alignment of Accessories11
2 Standard Cell Holder, 50 MM12
- Fig. 2-1 Standard Cell Holder, 50 MM12
- Fig. 2-2 Installing the Cell Holder in SPECORD S60012
- Fig. 2-3 Cell Inserted Correctly in the Cell Holder13
3 Cell Holder, 100 MM14
- Fig. 3-1 Cell Holder, 100 MM14
4 Cell Holder, 10 MM, Thermostated15
- Fig. 4-1 Thermostated Cell Holder with 10 MM Path Length15
- Fig. 4-2 Retrofitting the Magnetic Stirrer16
5 Cell Holder, 50 MM, Thermostated17
- Fig. 5-1 Thermostated Cell Holder, 50 or 10017
6 Holder for Round Cells18
- Fig. 6-1 Round Cell Holder18
- Fig. 6-2 Round Cell Holder Installed in SPECORD S60019
7 Holder for Microcells (Variable Path Length)20
- Fig. 7-1 Holder for Microcells with Variable Path Length20
- Fig. 7-2 Holder for Microcells (Variable Path Length) Installed21
8 Adjustable Cell Holder for Microcells22
- Fig. 8-1 Adjustable Holder for Microcells with Variable Radiation Height22
- Fig. 8-2 Holder for Micro Cells (Adjustable) Installed23
9 Holder for Cylindrical Cells24
- Fig. 9-1 Holder for Cylindrical Cells24
- Fig. 9-2 Holder for Cylindrical Cells Installed24
10 Holder for 100 MM Absorption Tube25
- Fig. 10-1 Absorption Tube with Holders25
6 Cell Changer26
- Fig. 11-1 6-Cell Changer for Cells with Variable Path Length26
  - 11.1 Installing the 6-Cell Changer in the Sample Chamber27
- Fig. 11-2 6-Cell Changer, Thermostated, with Magnetic Stirrer27
- Fig. 11-3 6-Cell Changer Installed28
12 8-Cell Changer30
- Fig. 12-1 Layout of the 8-Cell Changer30
  - 12.1 Installing the 8-Cell Changer in the Sample Chamber31
- Fig. 12-2 8-Cell Changer in SPECORD S60031
13 Cell Carousel33
- Fig. 13-1 Layout of the Cell Carousel33
- Fig. 13-2 Cell Carousel Fully Mounted34
14 Measurement with the Cell Changer35
- 14.1 Configuring Parameters for the Cell Changer35
- Fig. 14-1 Measuring Parameter Tab Accessories with Configurations for 6-Cell Changers35
  - 14.2 Carrying out Measurements with the Cell Changer36
- Fig. 14-2 Modes for the Cell Change During Kinetic Reactions37
15 Peltier-Tempered Accessories39
- General Safety Instructions for Peltier-Tempered Accessories39
- 15.2 Peltier Temperature-Controlled Cell Holder, Air-Cooled40
- Technical Data and Layout40
- Installing the Cell Holder in the Sample Chamber41
- Fig. 15-1 Peltier Temperature-Controlled Cell Holder, Air-Cooled41
  - Using the Cell Sensor42
- Fig. 15-2 Cell Sensor42
  - Temperature Control43
- Fig. 15-3 Conversion Kit for Ultra-Microcells43
- Fig. 15-4 Cover Cap and Cell Sensor for Ultra-Microcells43
- Fig. 15-5 Measuring Parameter Configuration for Peltier-Tempered Cell Holders44
- Fig. 15-6 Measuring Parameter Configuration for Peltier-Tempered Cell Holders - Temperature Control: Simultaneous45
  - Care47
  - Peltier-Tempered Cell Holder with External Heat Exchanger48
- Fig. 15-7 Peltier-Tempered Cell Holder with Temperature Control Unit and Heat Exchanger48
  - Technical Data and Layout49
  - Installing the Cell Holder in the Sample Chamber50
- Fig. 15-8 Peltier-Tempered Cell Holder with Heat Exchanger50
- Fig. 15-9 Peltier-Tempered Cell Holder Installed in SPECORD S60051
  - Temperature Control52
  - Care52
  - 15.4 Peltier Tempered 6- and 8-Cell Changers53
  - Technical Data and Layout54
  - Installing the Cell Changer in the Sample Chamber55
- Fig. 15-10 Layout of the Peltier-Tempered Cell Changer55
- Fig. 15-11 Peltier-Tempered Cell Changer Installed in the SPECORD S60055
- Fig. 15-12 Cell Sensor for Peltier-Tempered Cell Changers57
  - Carrying out Measurements with Peltier-Tempered Cell Changers58
- Fig. 15-13 Peltier-Tempered 8-Cell Changer in the Storage Container58
- Fig. 15-14 Configuration for Peltier-Tempered Cell Changers59
- Fig. 15-15 Selection of Temperature Control: Fix59
- Fig. 15-16 Selection of Temperature Control: Cyclic60
- Fig. 15-17 Measuring Parameter Configuration for Peltier-Tempered Cell Holders - Temperature Control: Cyclic61
  - Temperature Control Unit for Peltier-Tempered Accessories62
- Fig. 15-18 Displays and Switches at the Temperature Control Unit63
- Fig. 15-19 Connections on the Rear of the Temperature Control Unit63
- Fig. 15-20 Display and Keys for Temperature Adjustment at the Control Unit64
- Fig. 15-21 Temperature Curve in the Block and Inside the Cell for Different Cells65
  - 15.6 Heat Exchanger for Peltier-Tempered Accessories66
- Fig. 15-22 Heat Exchanger - Hose Connections and Compensation Container66
- Fig. 15-23 Heat Exchanger - Connections on the Rear67
16 Cartridge Sipper System69
- Fig. 16-1 Layout of the Cartridge Sipper System70
- Fig. 16-2 Flow Cell with Connected Sample Intake Hose and Pump Hose71
- Fig. 16-3 Complete Hose Kit for the Cartridge Sipper System71
- Fig. 16-4 Cartridge Sipper System Installed72
- Fig. 16-5 Measuring Parameter Configurations for the Cartridge Sipper System73
17 Holder for Solid Samples76
- Fig. 17-1 Holder for Solid Samples76
- Fig. 17-2 Installing the Holder for Solid Samples in SPECORD S60076
18 Absolute Reflectance Attachment77
- Fig. 18-1 Absolute Reflectance Attachment77
- Fig.18-2 V- and W-Shaped Beam Paths at the Attachment78
- Fig. 18-3 Absolute Reflectance Attachment in the Sample Chamber79
19 Reflection Measuring Attachment 11° - 6081
- Fig. 19-1 Reflection Attachment82
- Fig. 19-2 Table Tops for Reflection Attachment82
- Fig. 19-3 Beam Path in the Reflection Measuring Attachment (Viewed from the Front)83
- Fig. 19-4 Reflection Measuring Attachment Installed in the Sample Chamber83
- Fig.19-5 Example for Interference Values at a Reflection Angle of85
20 Integrating Sphere87
- Fig. 20-1 Layout of the Integrated Sphere - Total View88
- Fig. 20-2 Integration Sphere in Vertical and Horizontal Installation89
  - Installing the Integrating Sphere in the Sample Compartment90
- Fig. 20-3 Screws for Fastening the Polychromator Cover90
- Fig. 20-4 Slit Stop in Front of Polychromator90
- Fig. 20-5 Halogen Lamp of Integrating Sphere91
- Fig. 20-6 Control Unit Installed in the SPECORD S60092
  - 20.2 Using the Integrating Sphere93
  - 20.2.1 Transmittance Measurements93
- Fig. 20-7 Optical Path in Transmission Measurements94
  - 20.2.2 Reflectance Measurements96
- Fig. 20-8 Optical Path in Reflectance Measurements97
- Fig. 20-9 Sample Carrier with Powdered Sample98
  - 20.3 Lamp Replacement99
21 Fiber Coupling with SMA Connections or with Measuring Sensors100
- Fig. 21-1 Immersion Sensor for Transmittance100
- Fig. 21-2 Adjustable Holder to Accept the Optic Fiber Adapter100
- Fig. 21-3 Optic Fiber Adapter Inserted in the Sample Chamber102

Analytik Jena SPECORD S600 - Page 2

Table of Contents

Related product manuals