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Measuring Instruments
SPECORD S600
Analytik Jena SPECORD S600 User Manual
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Cell holder
Holder for
round cells
SPECORD S600 accessories
Edition 09/2014
17
Fig.
6-2
Round cell hold
er installed i
n SPECOR
D
S600
18
20
Table of Contents
Default Chapter
3
Table of Contents
3
1 Notes for Users
7
Notes on this Manual
7
Safety Instructions
7
Caring for Accessories
8
The Sample Chamber Design of the SPECORD S600
8
Fig. 1-1 Design of the SPECORD S600
9
Fig. 1-2 Universal Holder
9
Fig. 1-3 Universal Holder Installed in SPECORD S600
9
Converting the Sample Chamber
10
Fig. 1-4 Positions of the Support Rods in the Sample Chamber
10
Alignment of Accessories
11
2 Standard Cell Holder, 50 MM
12
Fig. 2-1 Standard Cell Holder, 50 MM
12
Fig. 2-2 Installing the Cell Holder in SPECORD S600
12
Fig. 2-3 Cell Inserted Correctly in the Cell Holder
13
3 Cell Holder, 100 MM
14
Fig. 3-1 Cell Holder, 100 MM
14
4 Cell Holder, 10 MM, Thermostated
15
Fig. 4-1 Thermostated Cell Holder with 10 MM Path Length
15
Fig. 4-2 Retrofitting the Magnetic Stirrer
16
5 Cell Holder, 50 MM, Thermostated
17
Fig. 5-1 Thermostated Cell Holder, 50 or 100
17
6 Holder for Round Cells
18
Fig. 6-1 Round Cell Holder
18
Fig. 6-2 Round Cell Holder Installed in SPECORD S600
19
7 Holder for Microcells (Variable Path Length)
20
Fig. 7-1 Holder for Microcells with Variable Path Length
20
Fig. 7-2 Holder for Microcells (Variable Path Length) Installed
21
8 Adjustable Cell Holder for Microcells
22
Fig. 8-1 Adjustable Holder for Microcells with Variable Radiation Height
22
Fig. 8-2 Holder for Micro Cells (Adjustable) Installed
23
9 Holder for Cylindrical Cells
24
Fig. 9-1 Holder for Cylindrical Cells
24
Fig. 9-2 Holder for Cylindrical Cells Installed
24
10 Holder for 100 MM Absorption Tube
25
Fig. 10-1 Absorption Tube with Holders
25
6 Cell Changer
26
Fig. 11-1 6-Cell Changer for Cells with Variable Path Length
26
11.1 Installing the 6-Cell Changer in the Sample Chamber
27
Fig. 11-2 6-Cell Changer, Thermostated, with Magnetic Stirrer
27
Fig. 11-3 6-Cell Changer Installed
28
12 8-Cell Changer
30
Fig. 12-1 Layout of the 8-Cell Changer
30
12.1 Installing the 8-Cell Changer in the Sample Chamber
31
Fig. 12-2 8-Cell Changer in SPECORD S600
31
13 Cell Carousel
33
Fig. 13-1 Layout of the Cell Carousel
33
Fig. 13-2 Cell Carousel Fully Mounted
34
14 Measurement with the Cell Changer
35
14.1 Configuring Parameters for the Cell Changer
35
Fig. 14-1 Measuring Parameter Tab Accessories with Configurations for 6-Cell Changers
35
14.2 Carrying out Measurements with the Cell Changer
36
Fig. 14-2 Modes for the Cell Change During Kinetic Reactions
37
15 Peltier-Tempered Accessories
39
General Safety Instructions for Peltier-Tempered Accessories
39
15.2 Peltier Temperature-Controlled Cell Holder, Air-Cooled
40
Technical Data and Layout
40
Installing the Cell Holder in the Sample Chamber
41
Fig. 15-1 Peltier Temperature-Controlled Cell Holder, Air-Cooled
41
Using the Cell Sensor
42
Fig. 15-2 Cell Sensor
42
Temperature Control
43
Fig. 15-3 Conversion Kit for Ultra-Microcells
43
Fig. 15-4 Cover Cap and Cell Sensor for Ultra-Microcells
43
Fig. 15-5 Measuring Parameter Configuration for Peltier-Tempered Cell Holders
44
Fig. 15-6 Measuring Parameter Configuration for Peltier-Tempered Cell Holders - Temperature Control: Simultaneous
45
Care
47
Peltier-Tempered Cell Holder with External Heat Exchanger
48
Fig. 15-7 Peltier-Tempered Cell Holder with Temperature Control Unit and Heat Exchanger
48
Technical Data and Layout
49
Installing the Cell Holder in the Sample Chamber
50
Fig. 15-8 Peltier-Tempered Cell Holder with Heat Exchanger
50
Fig. 15-9 Peltier-Tempered Cell Holder Installed in SPECORD S600
51
Temperature Control
52
Care
52
15.4 Peltier Tempered 6- and 8-Cell Changers
53
Technical Data and Layout
54
Installing the Cell Changer in the Sample Chamber
55
Fig. 15-10 Layout of the Peltier-Tempered Cell Changer
55
Fig. 15-11 Peltier-Tempered Cell Changer Installed in the SPECORD S600
55
Fig. 15-12 Cell Sensor for Peltier-Tempered Cell Changers
57
Carrying out Measurements with Peltier-Tempered Cell Changers
58
Fig. 15-13 Peltier-Tempered 8-Cell Changer in the Storage Container
58
Fig. 15-14 Configuration for Peltier-Tempered Cell Changers
59
Fig. 15-15 Selection of Temperature Control: Fix
59
Fig. 15-16 Selection of Temperature Control: Cyclic
60
Fig. 15-17 Measuring Parameter Configuration for Peltier-Tempered Cell Holders - Temperature Control: Cyclic
61
Temperature Control Unit for Peltier-Tempered Accessories
62
Fig. 15-18 Displays and Switches at the Temperature Control Unit
63
Fig. 15-19 Connections on the Rear of the Temperature Control Unit
63
Fig. 15-20 Display and Keys for Temperature Adjustment at the Control Unit
64
Fig. 15-21 Temperature Curve in the Block and Inside the Cell for Different Cells
65
15.6 Heat Exchanger for Peltier-Tempered Accessories
66
Fig. 15-22 Heat Exchanger - Hose Connections and Compensation Container
66
Fig. 15-23 Heat Exchanger - Connections on the Rear
67
16 Cartridge Sipper System
69
Fig. 16-1 Layout of the Cartridge Sipper System
70
Fig. 16-2 Flow Cell with Connected Sample Intake Hose and Pump Hose
71
Fig. 16-3 Complete Hose Kit for the Cartridge Sipper System
71
Fig. 16-4 Cartridge Sipper System Installed
72
Fig. 16-5 Measuring Parameter Configurations for the Cartridge Sipper System
73
17 Holder for Solid Samples
76
Fig. 17-1 Holder for Solid Samples
76
Fig. 17-2 Installing the Holder for Solid Samples in SPECORD S600
76
18 Absolute Reflectance Attachment
77
Fig. 18-1 Absolute Reflectance Attachment
77
Fig.18-2 V- and W-Shaped Beam Paths at the Attachment
78
Fig. 18-3 Absolute Reflectance Attachment in the Sample Chamber
79
19 Reflection Measuring Attachment 11° - 60
81
Fig. 19-1 Reflection Attachment
82
Fig. 19-2 Table Tops for Reflection Attachment
82
Fig. 19-3 Beam Path in the Reflection Measuring Attachment (Viewed from the Front)
83
Fig. 19-4 Reflection Measuring Attachment Installed in the Sample Chamber
83
Fig.19-5 Example for Interference Values at a Reflection Angle of
85
20 Integrating Sphere
87
Fig. 20-1 Layout of the Integrated Sphere - Total View
88
Fig. 20-2 Integration Sphere in Vertical and Horizontal Installation
89
Installing the Integrating Sphere in the Sample Compartment
90
Fig. 20-3 Screws for Fastening the Polychromator Cover
90
Fig. 20-4 Slit Stop in Front of Polychromator
90
Fig. 20-5 Halogen Lamp of Integrating Sphere
91
Fig. 20-6 Control Unit Installed in the SPECORD S600
92
20.2 Using the Integrating Sphere
93
20.2.1 Transmittance Measurements
93
Fig. 20-7 Optical Path in Transmission Measurements
94
20.2.2 Reflectance Measurements
96
Fig. 20-8 Optical Path in Reflectance Measurements
97
Fig. 20-9 Sample Carrier with Powdered Sample
98
20.3 Lamp Replacement
99
21 Fiber Coupling with SMA Connections or with Measuring Sensors
100
Fig. 21-1 Immersion Sensor for Transmittance
100
Fig. 21-2 Adjustable Holder to Accept the Optic Fiber Adapter
100
Fig. 21-3 Optic Fiber Adapter Inserted in the Sample Chamber
102
4
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Analytik Jena SPECORD S600 Specifications
General
Brand
Analytik Jena
Model
SPECORD S600
Category
Measuring Instruments
Language
English
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