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Metrohm 860 KF User Manual
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11.1 Scope of delivery 2.860.0010
￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭
52
￭￭￭￭￭￭￭￭
860 KF Thermoprep
Qty.
Order no.
Description
1
6.2060.010
Cable support
Used with 860 KF Thermoprep.
1
6.2063.010
Sample holder for 6.2419.007 sample vials
(6 mL)
1
6.2419.007
Sample vial 6 ml / 100 pieces
6.1448.050 septum caps. Used for KF-determinations with oven.
Volume (mL):
6
1
6.2621.110
Crimping tongs
Crimping tongs for sealing 6 mL sample vials (6.2419.000,
6.2419.007).
Length (mm):
210
59
61
Table of Contents
Default Chapter
5
Table of Contents
5
1 Introduction
9
Instrument Description
9
Instrument Components
9
Intended Use
10
About the Documentation
10
Symbols and Conventions
10
Safety Instructions
11
General Notes on Safety
11
Electrical Safety
11
Personnel Safety
12
Flammable Samples and Solvents
13
Recycling and Disposal
13
2 Overview of the Instrument
14
Figure 1 Front 860 KF Thermoprep
14
Figure 2 Rear 860 KF Thermoprep
15
3 Installation
16
Setting up the Instrument
16
Packaging
16
Checks
16
Location
16
Connecting the Mains Cable
16
Figure 3 Connecting the Mains Cable
16
Mounting the Guidance Rod
17
Figure 4 Loosen the Adapter
17
Figure 5 Mounting the Guidance Rod
18
Figure 6 Mounting Tubing
18
Figure 7 Fix the Adapter
19
Figure 8 Guidance Rod Mounted
19
Mounting the Sample Insert
20
Figure 9 Mounting the Sample Insert
20
Mounting the Needles
21
Figure 10 Mounting the Needles
21
Mounting the Heating Tubing
22
Figure 11 Mounting the Heating Tubing (View from Rear)
22
Figure 12 Connecting the Heating Tubing
23
Mounting the Dust Filter
24
Assembling the Drying Flask
24
Figure 13 Mounting the Dust Filter
24
Figure 14 Preparing the Drying Flasks
24
Figure 15 Mounting the Tubings
25
Air/Nitrogen Connector
26
Figure 16 External Gas Supply Connection
26
Inserting the Heating Tube into the KF Titration Cell
27
Figure 17 Coulometric KF Titration Cell
27
Figure 18 Volumetric KF Titration Cell
28
4 Operation
30
Switching the Instrument on and off
30
The Keypad
30
Figure 19 Mains Switch
30
Figure 20 Keypad and Operating Unit
30
The Display
31
Display Elements
31
Status Display
31
Figure 21 Main Dialog
31
Error Messages
32
Modifying Numerical Values and Settings
33
Selecting from a Selection List
33
Modifying Numerical Values
33
Parameters
34
Configuration
35
5 Performing a Determination
37
Conditioning the System
37
Preparing the KF Titration Cell
37
Preparing the 860 KF Thermoprep
38
Figure 22 Insert the Sample Vessel into the Oven
39
Figure 23 Move the Guide Head down
39
Figure 24 Insert the Needle
40
Determining the Blank Value
41
Determining Samples
42
6 Handling and Maintenance
44
General
44
Care
44
Quality Management and Validation with Metrohm
44
7 Troubleshooting
46
Problems and Their Solutions
46
8 Appendix
47
Practical Instructions
47
Literature
48
9 Technical Data
49
Oven
49
Gas Flow
49
Outlet Heating
49
Mains Connection
50
Safety Specifications
50
Electromagnetic Compatibility (EMC)
50
Ambient Temperature
51
Reference Conditions
51
Dimensions
51
10 Conformity and Warranty
52
Declaration of Conformity
52
Warranty (Guarantee)
53
Quality Management Principles
54
Scope of Delivery 2.860.0010
56
Optional Accessories
63
5
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Metrohm 860 KF Specifications
General
Brand
Metrohm
Model
860 KF
Category
Laboratory Equipment
Language
English
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