Shimadzu GC-2010 User Manual

3 Basic Operation
3.15 Example of the Chromatogram
33FPD-2010
■ When analyzing phosphorus (P) components:
<Analysis conditions>
Sample : Tributyl Phosphate
Concentration 10 ng/µl (Solvent Hexane)
Injection volume: 1µl
Column: DB1-M30-025 (I.D. 0.25 mm, Length 30 mm, Non-polar, film thickness 0.25 µm)
Column oven temp. : 180°C
Injection port temp : 250°C
Detector temp : 250°C
Carrier gas : He
Flow rate conditions : Inlet pressure 150 kPa, Column flow rate 1.26 ml/min, Split ratio 1:99, and
purge flow rate 2.5 ml/min
Detector : FPD (Flame Photometric Detector)
Detector gas flow rate:Hydrogen 80 ml/min
Air 120 ml/min
Range : 10
-1
Filter signal time constant:200 msec
Shield height : 2 mm
Fig. 3.15.2

Shimadzu GC-2010 Specifications

General

Brand	Shimadzu
Model	GC-2010
Category	Security Sensors
Language	English