EasyManua.ls Logo

Shimadzu GC-2010 User Manual

Shimadzu GC-2010
88 pages
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Page #1 background imageLoading...
Page #1 background image
221-40455C
FLAME PHOTOMETRIC DETECTOR
FOR GC-2010
FPD-2010
USER’S MANUAL
Read the instruction manual thoroughly before you use the product.
Keep this instruction manual for future reference.

Questions and Answers:

Shimadzu GC-2010 Specifications

General IconGeneral
BrandShimadzu
ModelGC-2010
CategorySecurity Sensors
LanguageEnglish

Summary

Precautions for Safe Operation

General Safety Precautions

Lists essential safety measures for operating the FPD unit, including intended use, following manual instructions, and avoiding disassembly.

Outline

Principle of the FPD (Flame Photometric Detector)

Explains the working principle of the Flame Photometric Detector, including its block diagram and components.

Parts List

FPD Parts List

Lists all components and accessories included with the FPD unit, along with their part numbers and quantities.

Basic Operation

Introduction

Introduces the basic operational procedures for the FPD and references the GC-2010 manual.

Gas used

Specifies the required purity standards for carrier gas, hydrogen, and air for optimal equipment performance.

Comfirming the Filter

Details the procedure for checking and confirming the correct filter mounting for sulfur, phosphorus, or tin analysis.

Shield Ring Height Check

Explains how to adjust the shield ring height to cut noise and ensure stable analysis, depending on the injection port type.

Checking Glass Insert and Injection Port Septum

Guides on how to check the glass insert and when to replace the injection port septum for proper operation.

Mounting the Column

Describes the procedure for mounting the chromatographic column, including fixing the graphite ferrule position.

Setting the Detector Temperature

Details how to set the detector temperature using the base unit to prevent soiling and maintain performance.

Setting the Temperature of the Column Oven and the Injection Port

Explains setting temperatures for the column oven and injection port, referencing the GC-2010 manual.

Setting the Flow Rate

Guides on setting the carrier gas flow rate through the [FLOW] key and referencing the GC-2010 manual.

System Start-up

Outlines the procedure for system start-up via the [SYSTEM] key and [Start GC] function.

Setting Flow Rate of Detector Gases (Hydrogen/Air)

Details setting the flow rates for hydrogen and air, providing recommended values for sulfur and phosphorus analysis.

Igniting the FPD

Describes the procedure for igniting the FPD, including safety precautions and checking detector temperature.

Setting the Ranges and the Attenuation

Explains how to set signal range and analog signal type for analog or digital output to the data processing unit.

Baseline Check

Details the process of checking the baseline stabilization and what to do if abnormalities occur.

Example of the Chromatogram

Provides example chromatograms for analyzing sulfur and phosphorus components with specific conditions.

Method for Stopping

Outlines the procedure for safely stopping the detector, including setting gas flow rates to zero and lowering temperatures.

Key Operations

Setting the detector

Configures detector parameters such as temperature, flame status, and filter time constant via the [DET] key.

Selecting the detector

Explains how to switch between different detectors installed in the GC system using the [DET] key.

Setting the Detector Gas

Details setting the flow rates for hydrogen and air, providing specific values for sulfur and phosphorus analysis.

Detector ON/OFF

Describes how to enable or disable the FPD detector control through the on-screen interface.

Igniting and Extinguishing the Detector

Covers the procedures for igniting the detector's flame and safely extinguishing it, including critical safety warnings.

Setting the Range

Guides on selecting the appropriate signal range (attenuation) for analog output based on analysis requirements.

Zero Adjustment

Explains the process of performing zero point adjustment for the detector to ensure accurate baseline readings.

Maintenance and Inspections

Precautions for Maintenance and Inspections

Highlights critical safety warnings and procedures to follow before performing any maintenance or inspection tasks on the FPD.

Turning off the Power

Details the correct procedure for safely powering down the FPD and associated GC system components.

Cleaning and Replacing the Quartz Cylinder

Provides step-by-step instructions for cleaning or replacing the quartz cylinder to maintain detection sensitivity.

Maintenance and Replacement of the Filter

Outlines the process for cleaning or replacing the FPD's filter to prevent contamination and maintain performance.

Replacing Photomultiplier

Describes the procedure for replacing the photomultiplier, emphasizing safety precautions and careful handling.

Replacing the Battery

Guides on how to replace the backup battery for the cooling fan system, necessary when the battery degrades.

Troubleshooting

Flame Ignition Issues

Addresses causes and solutions for the FPD flame failing to ignite or going out during operation.

Abnormal Baseline

Covers common causes of abnormal baseline behavior, such as noise, drift, and meandering.

Zero Adjustment Problems

Details issues encountered when zero adjustment does not work correctly and their potential causes.

No Peak or Small Peak Issues

Explains reasons for no peaks or small peaks in chromatograms, including flame issues, filter use, and shielding.

Abnormal Peak Form

Discusses causes of abnormal peak shapes in chromatograms, such as quenching or incorrect column setup.

Other Abnormal Phenomena

Refers to GC-2010 manual for phenomena like gas leakage, temperature issues, ghost peaks, and repeatability.

Maintenance Parts

Maintenance Parts List

Lists all parts required for maintenance and replacement of the FPD, including part numbers and descriptions.

Specifications

Specifications of the FPD-2010

Presents the technical specifications of the FPD-2010, covering detection method, range, and operating conditions.

Appendix

Quenching

Explains the phenomenon of quenching in FPD detection and its impact on analysis repeatability and accuracy.

Related product manuals