EasyManua.ls Logo

Shimadzu RID-10A User Manual

Shimadzu RID-10A
112 pages
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Page #1 background imageLoading...
Page #1 background image
228
-
30179
DIFFERENTIAL REFRACTIVE DETECTOR
RID
-
1
OA
FOR
SHIMADZU
HIGH
-
PERFORMANCE
LIQUID
CHROMATOGRAPH
USER’S
MANUAL
Read the instruction manual thoroughly before you use the product. Keep
this
instruction
manual
with care
so
that you can use it any time you need it.
SHIMADZU
CORPORATION
CHROMATOGRAPHIC
&
SPECTROPHOTOMETRIC
INSTRUMENTS DIVISION
KYOTO,
3APAN

Table of Contents

Question and Answer IconNeed help?

Do you have a question about the Shimadzu RID-10A and is the answer not in the manual?

Shimadzu RID-10A Specifications

General IconGeneral
BrandShimadzu
ModelRID-10A
CategorySecurity Sensors
LanguageEnglish

Summary

Precautions for Safety Operation

Key Safety Operation Points

Key safety guidelines for operating the unit safely.

Instruction Manual Warning Symbol Explanations

Explains the meaning of warning symbols used in the manual for clarity.

Equipment Warning Labels

Fuse Replacement and Optical Cable Handling

Details on replacing fuses and precautions for bending the optical cable.

Installation and Handling Precautions

Ventilation Requirements

Guidelines for ventilating the room where the chromatograph is installed.

Fire Safety Precautions

Rules regarding fire usage and keeping extinguishers nearby.

Sink Installation

Importance of installing a sink nearby for flushing eyes or skin.

Corrosive Gas and Dust Avoidance

Avoidance of installation in places with corrosive gases or dust.

Electromagnetic Noise Avoidance

Avoidance of locations with intense magnetic or electromagnetic fields.

Space Requirements

Details on suitable table or stand dimensions for system placement.

Other Site Requirements

Recommendations for room temperature, avoiding direct sunlight, and vibrations.

Static Electricity Precautions

Static Discharge Accident Mechanism

Explains how static electricity can cause accidents in liquid chromatography systems.

Preventive Measures for Static Accidents

Outlines measures to prevent accidents caused by static electricity discharge.

Chapter 1 General

1.1 Outline

Provides a brief overview of the RID-10A differential refractive index detector.

1.2 Features

Highlights key features such as excellent stability, various applications, and safety measures.

1.3 Principle of Measurement

Explains the optical system and signal processing modes (A, P, L) of the detector.

1.4 Flow Schematic

Illustrates the solvent flow lines within the RID-10A detector.

Chapter 2 Parts List

2.1 Parts and Accessories

Lists all standard accessories and components included with the RID-10A.

Chapter 3 Component Location and Function

3.1 Front View

Identifies and describes the control panel and front cover opening button.

3.2 Interior of Front Cover, Right Side

Details cell inlet/outlet ports, tube holder, leak tube connection, and leak sensor.

3.3 Rear View

Identifies rear panel connectors for remote, external I/O, grounding, power, and fuse holder.

Chapter 4 Installation

4.1 Basic Installation Requirements

Covers ventilation, fire safety, sink, corrosive gas, noise, space, and environmental conditions.

4.2 Example of System Layout

Shows a typical liquid chromatograph system layout with space requirements.

4.3 Stacking Modules

Explains how to stack RID-10A modules with pumps or column ovens for safety.

4.4 Electrical Connections

Details connecting the unit to power outlets and proper grounding procedures.

4.5 Plumbing Connections

Describes connecting the solvent delivery pump, injector, column, and detector.

4.6 Connecting Recorder and Integrator

Instructions for connecting the RID-10A to a recorder and a Chromatopac integrator.

4.7 Connecting Drain Tube for Solvent Leakage

Procedures for connecting leak tubes to manage solvent leakage.

Chapter 5 Operation

5.1 Precautions for Operation

Emphasizes closing the front cover and preventing flow cell clogging.

5.2 Fundamentals of Operation

Covers turning the unit ON, display unit functions, keyboard layout, and basic operation.

5.3 Plumbing of the Flow Selection Block

Details usage and tubing connections for analytical, preparative, and large-scale modes.

5.4 Creating and Executing Time Programs

Guides on setting up and running time programs using commands like ZERO, MARK, and LOOP.

5.5 Additional Functions (AUX-FUNC)

Explains functions like TOTAL EN, CELL TEMP, AUX RANGE, EVENT, and parameter settings.

Chapter 6 Initial Performance Test

6.1 System Performance Check

Outlines the procedure for checking the performance of the HPLC system.

Chapter 7 Control from External Equipment

7.1 Connection with System Controller SCL-10A

Describes how to connect the RID-10A to the SCL-10A controller via optical cable.

7.2 Control from the SCL-10A

Details power on, CONFIG screen, main menu, parameter settings, and DET CONTROL screen.

7.3 Connecting External Input and Output Terminals

Explains connections for external input/output terminals (T.B. 1 and T.B. 2).

Chapter 8 Maintenance

8.1 Cleaning the Flow Lines

Provides procedures for cleaning flow lines to resolve baseline issues using acetone and nitric acid.

8.2 Span Adjustment

Details the process of span adjustment for modes A, P, and L using a Chromatopac or LC workstation.

8.3 Replacement of Fuse

Step-by-step instructions for replacing blown fuses in the unit.

8.4 Periodical Cleaning

Guidance on cleaning the unit's cover and panels to maintain appearance.

Chapter 9 Performance Verification

9.1 Component Validation

Describes procedures for validating individual components like lamp, temperature, and span.

9.2 System Validation

Outlines the holistic validation procedure for the entire HPLC system, focusing on repeatability.

Chapter 10 Troubleshooting

10.1 Symptoms, Causes and Remedies

Lists common symptoms, their possible causes, and recommended remedies for troubleshooting.

10.2 List of Error Messages

Explains system error messages like ROM error, RAM error, Leakage error, and Overheat error.

Chapter 11 Specifications

11.1 RID-10A Specifications

Provides detailed technical specifications for the RID-10A detector.

Chapter 12 Replacement Parts

12.1 Consumables and Repair Parts

Lists consumables like lamps and repair parts for electric and optical systems.

12.2 Optional Parts

Lists optional parts such as the flow selection block and relief valve.

Chapter 13 Reference

13.1 Solvent Characteristics

Provides a table of physical properties for various solvents used in LC.

Related product manuals