D2 PHASER User Manual
DOC-M88-EXX141 V5 – 01.2015
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D2 PHASER User Manual
Caution!
Read the manuals ‘D2 PHASER Introductory User Manual’ and ‘D2 PHASER – From
Unpacking to the First Measurement – Quick Start Guide’ completely before
switching on the D2 PHASER instrument.
Table of contents
Introduction ................................................................................................................ 1
Basics and principle of operation ............................................................................ 3
Design of the diffractometer ..................................................................................... 4
Goniometer ...................................................................................................................................... 4
X-ray tube ......................................................................................................................................... 4
Slit systems, slit and Soller modules and other passive optics ................................................ 6
Primary divergence slit systems ................................................................................................ 6
Secondary detector slit systems ................................................................................................ 6
Slit module.................................................................................................................................. 6
K filter module .......................................................................................................................... 7
Absorber module ........................................................................................................................ 7
Soller slit module ........................................................................................................................ 7
Airscatter screen modules .......................................................................................................... 7
Sample holder .................................................................................................................................. 8
Sample Changer .............................................................................................................................. 8
Detectors .......................................................................................................................................... 8
Silicon strip detector LYNXEYE ................................................................................................. 9
XFlash detector .......................................................................................................................... 9
Operation of the D2 PHASER ................................................................................. 10
Transport and positioning of the instrument ............................................................................. 10
Switching on the instrument ........................................................................................................ 10
Switching off the instrument ........................................................................................................ 11
Warning and status lamps ............................................................................................................ 11
Operational controls and connection plugs ............................................................................... 11
Front door of the instrument ........................................................................................................ 11
Measurement with the D2 PHASER ............................................................................................. 11
Configuration and settings of primary section .......................................................................... 12
Configuration and settings of sample section .......................................................................... 12
Configuration and settings of secondary section ..................................................................... 13
Start measurement with commander ....................................................................................... 13
Start measurement with joblist ................................................................................................. 14
Start element analyses with the program SPECTRA .............................................................. 14
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