GE Analytical Instruments ©2006 Index-5 DML 14291 Rev. A
Start-up............................................................ 4-18
Thermal Mass Flowmeter............................... 5-2
Cable................................................................5-2
Cable Clamp...................................................5-3
Clamp ..............................................................5-3
Tools .....................................................................4-2
Vacuum Pump Setup...........................................4-4
Adding Oil...................................................... 4-4
Connect Power Cord and Turn On Power
Switch....................................................... 4-9
Installing Inlet Fitting................................. 4-5
Installing Pump Outlet Fitting.................. 4-6
Installing the Chemical Trap and Vacuum
Hose .......................................................... 4-7
Installing Trap Mounting Bracket............. 4-5
Installing Pump Inlet Fitting................................ 4-5
Installing the charcoal trap....................................4-6
Installing the Chemical Trap and Vacuum Hoses
.............................................................................. 4-7
Installing the Chemical Trap Mounting Bracket.4-
5
Installing the Pump Outlet Fitting ..................... 4-6
K
Keypad......................................................1-6, 1-10, 3-1
KMnO
4
...........................................................................
6-1
L
Leak Check for Purge Vessel.............................13-5
Lifetime of zero air filter .......................................6-1
Light Leak Test..................................................15-10
Linear Range and Off-scale Peak..................12-10
Liquic Measurements
Opening the Gas Bubbler............................13-12
Liquid Measurement
Supplies ............................................................11-1
Gases............................................................ 11-1
Lab Equipment...........................................11-1
Reagents...................................................... 11-1
Liquid measurements
Measurement of Iron-bound NO ..................14-3
Setup of Purge Vessel....................................11-2
Liquid Measurements........................................ 13-10
Adjustment of Liquid Level ...................12-3, 13-5
Adjustment of Purge Gas Flow Rate12-3, 13-4
Analysis of Samples and Standards........ 13-10
Anti-foaming Agent........................................11-7
Apparatus for Nitrate Reduction ...............13-1
Apparatus for Nitrite Reduction ................12-1
Background Nitrite...................................... 12-12
Cell Pressure..................................................... 12-3
Cleaning the Bubbler Tubing.................... 13-15
Cleaning the gas Bubbler.............................. 13-15
Cleaning the Purge Vessel......................... 12-14
COM Port interval
........................................... 11-10
Deproteinization.................................12-12, 13-10
Dynamic Headspace Analysis ......................14-6
Foaming problems..............................12-12, 13-10
Headspace Measurement of Nitric Oxide.14-4
Apparatus ....................................................14-4
Smaple collection ......................................14-5
Standards.....................................................14-6
Inert Gas Supply ............................................... 11-5
Injection Technique.............................12-9, 13-9
Leak Check for Purge Vessel........................13-5
Linear Range and Off-scale Peak ............ 12-10
Long-term maintenance of the purge vessel
and bubble...................................12-16, 13-16
Nitriae Contamination............................... 13-10
Nitrite Contamination................................ 12-10
Nitrosothiols....................................................14-1
Copper(I)/Iodide/Iodine Reagent
Preparation of the Reducing Agent.14-2
Treatment of Plasma Sample ...........14-3
Copper(I)/Iodide/Iodine Reagent............14-2
Cu(I)/Cysteine Reagent
Preparation of Reducing Agent ........14-1
Cu(I)/Cysteine Reagent.............................14-1
Preparation of Nitrosothiols Standards 14-
2
Preparation of S-Nitroso-Albumin.........
14-2