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Metrohm FOSS NIRS XDS MultiVial Analyzer User Manual

Metrohm FOSS NIRS XDS MultiVial Analyzer
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NIRS
XDS MultiVial Analyzer
Manual
8.921.8002EN

Table of Contents

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Metrohm FOSS NIRS XDS MultiVial Analyzer Specifications

General IconGeneral
TechnologyNear-Infrared Spectroscopy (NIRS)
Wavelength Range400 - 2500 nm
Sample PresentationVials
Measurement TimeSeconds per sample
ConnectivityUSB, Ethernet
SoftwareVision software
Power Requirements100-240 V AC, 50/60 Hz
Sample CapacityMultiple Vials (Automated)
Detector TypeInGaAs
Light SourceTungsten halogen lamp
Sample TypeLiquids, powders, and solids

Summary

Introduction to the XDS MultiVial Analyzer

Site Readiness and Installation Guidelines

Temperature and Humidity Requirements

Guidelines for operating temperature and humidity levels to ensure instrument performance.

General Environment Considerations

Recommendations for minimizing dust and avoiding HVAC interference for optimal instrument operation.

Vibration Precautions

Advice on installing the analyzer away from sources of vibration to prevent operational issues.

Electrical Power Specifications

Requirements for a stable AC power source with surge protection for instrument operation.

Instrument Communication Methods

Details on connecting the instrument via UTP crossover or network cable for data transfer.

Instrument Dimensions and Weight

Physical specifications of the XDS MultiVial Analyzer, including dimensions and weight.

XDS Instrument Connection Procedures

Network Connection Setup

Preferred method for instrument communication via a local area network (LAN).

Direct Connection Method

Method for connecting the instrument directly to a computer without a network.

Overview of XDS Instrument Communication

Key aspects of XDS instrument communication, including security and access protocols.

XDS Communication Protocol Flowchart

Visual representation of the XDS instrument's communication protocol and IP address assignment process.

Connecting the XDS Instrument with Vision Software

Vision Software Connection Steps

Steps to establish communication between the Vision software and the XDS instrument.

Troubleshooting Connection Problems

Guidance for resolving common issues encountered when connecting the instrument to the Vision software.

Assembly of the XDS MultiVial Analyzer

XDS MultiVial Module Operation

Introduction to Vial Analysis

Overview of the MultiVial Analyzer's design for automated vial sampling and routine analysis.

Creating Custom Vial Size Configurations

Instructions for configuring custom vial sizes within the Vision software for specific sample trays.

Spot Size Adjustment for Samples

How to adjust the illumination beam spot size for optimal analysis of small samples.

Using the Iris Adapter

Usage and installation of the Iris Adapter for scanning stationary objects.

Sample Transport Mechanism Usage

Operation of the automated sample transport mechanism for moving sample cells within the module.

Vision Software Operation

Entering and Navigating Vision Software

Steps to launch and log into the Vision software for instrument operation and data acquisition.

Vial Dialog Selection Menu

Setting up sample parameters and managing vial sequencing within the Vision software.

Instrument Diagnostics Procedures

Setup Diagnostics in Vision Software

Initial diagnostic steps required in Vision software before using the instrument for analysis.

Evaluation Diagnostics for Performance Verification

Procedures for verifying instrument performance and operation using various diagnostic tests.

Instrument Maintenance Procedures

Instrument Maintenance Overview

General information on instrument maintenance, emphasizing the sealed optical enclosure and user-serviceable parts.

Fan Filter Replacement Guide

Step-by-step guide for inspecting and replacing the instrument's fan filter.

Lamp Replacement Procedure

Procedure for safely replacing the instrument's lamp, including cooling time and part number.

Fuse Replacement Instructions

Instructions for replacing fuses, emphasizing investigation of the underlying electrical fault first.

Using the Maintenance Log

How to access and use the Maintenance Log in the Diagnostic Database to track activities.

Validation Tools and Procedures

Hardware Validation Tools

Tools and documents for validating the instrument's hardware components and accessories.

Software Validation Tools

Tools and documentation for validating the Vision Spectral Analysis Software.

21 CFR Part 11 Compliance Features

How Vision software meets regulatory requirements for electronic records and signatures.

Safety and Electrical Certification Information

Troubleshooting Common Issues

Instrument Power-Up Failure

Steps to diagnose and resolve issues where the instrument fails to power on.

Vision Communication Failure

Troubleshooting steps for establishing communication between Vision software and the instrument.

Lamp Not Turning On

Diagnosing and resolving issues related to the instrument lamp not functioning.

Wavelength Linearization Failure

Steps to troubleshoot failures in the instrument's Wavelength Linearization process.

Performance Test Failure

Diagnosing and resolving issues when the instrument fails the Performance Test.

Instrument Calibration Failure

Troubleshooting steps for instrument calibration failures, including standard positioning.

High Instrument Gain in Gain Test

Identifying potential issues when the instrument's gain readings are excessively high.

Instrument Cooling Fans Operating at Maximum Rate

Diagnosing why instrument cooling fans are operating at maximum speed.

X-Y Error Reported in Vision

Addressing X-Y positioning errors in Vision, often related to lid open or mechanism issues.

Sampling Mechanism Not Moving with Large Sample Cell

Troubleshooting when the sampling mechanism fails to move with a large sample cell.

X-Y Mechanism Not Moving with Vial Tray

Resolving issues where the X-Y mechanism does not move correctly with a vial tray.

X-Y Mechanism Crashing into Iris Adapter

Troubleshooting X-Y mechanism errors caused by interaction with the Iris Adapter.

Instrument Cooling Fans Not Operating

Diagnosing why the instrument's cooling fans are not operating.

Lifting and Transporting the Metrohm Instrument

MultiVial Shipping Position Instructions

Procedure for setting the sample carriage to the shipping position and installing protective foam.

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