5
7.1.4 Instrument Calibration .......................................................................................... 69
7.1.5 IPV Setup (Instrument Performance Verification) ................................................... 72
7.2 Evaluation Diagnostics ................................................................................ 74
7.2.1 Performance Test .................................................................................................. 75
7.2.2 Wavelength Certification ...................................................................................... 78
7.2.3 Photometric Test .................................................................................................. 82
7.2.4 Gain Test .............................................................................................................. 86
7.2.5 7.2.5 Low Flux Test ............................................................................................... 87
8 Instrument Maintenance .............................................................................................. 90
8.1 Overview .................................................................................................... 90
8.2 Fan Filter Replacement ............................................................................... 91
8.3 Lamp Replacement ..................................................................................... 93
8.4 Fuse Replacement ..................................................................................... 100
8.5 Maintenance Log ...................................................................................... 101
9 Validation Tools ......................................................................................................... 103
9.1 Hardware Validation Tools ....................................................................... 104
9.1.1 Factory Instrument Test Guide and Results .......................................................... 104
9.1.2 Installation and Operating Qualification Documents ............................................ 104
9.1.3 NIRStandards® for Instrument Performance Verification ..................................... 104
9.1.4 Instrument Performance Certification .................................................................. 104
9.1.5 Metrohm NIRSystems Master Instrument Program .............................................. 105
9.2 Software Validation Tools ........................................................................ 105
9.2.1 Installation and Operating Qualification Documents ............................................ 105
9.2.2 Vision Certificate of Validation ............................................................................ 105
9.2.3 21 CFR Part 11 Compliance ................................................................................. 106
10 Safety and Electrical Certification ............................................................. 108
11 11.0 Troubleshooting ............................................................................... 109
12 Lifting and transporting the Metrohm instrument: ................................... 113
12.1 Instructions for MultiVial® Shipping Position ........................................... 114
12.1.1 Instructions follow .............................................................................................. 114
13 Index ........................................................................................................ 116
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