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Agilent Technologies 5977 MSD User Manual
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*G7077-90026*
G7077-90026
© Agilent T
echnologies, Inc.
Printed in USA, June 2016
Agilent T
echnologies
227
Table of Contents
Default Chapter
1
Operating Manual
1
Safety Notices
2
About this Manual
3
Table of Contents
7
1 Introduction
14
5977B Series MSD Version
14
Abbreviations Used
15
The 5977B Series MSD
17
MSD Hardware Description
19
Important Safety Warnings
21
Hydrogen Safety
23
GC Precautions
24
Precautions
26
Safety and Regulatory Certifications
28
Electromagnetic Compatibility
30
Intended Use
31
Cleaning/Recycling the Product
31
Accidental Liquid Spillage
31
Moving or Storing the MSD
31
To Replace the Primary Fuses
32
2 Installing 7890 GC Columns
36
Columns
36
To Install a Capillary Column in a Split/Splitless Inlet
38
To Condition a Capillary Column
41
To Install a Capillary Column in the GC/MS Interface Using the Self-Tightening Column Nut
42
To Install a Capillary Column in the GC/MS Interface Using a Standard Column Nut
47
To Install the Interface Tip Seal
50
To Calibrate Column Flow Linear Velocity
52
The GC/MSD Interface for a 7890B Series GC
55
3 Intuvo 9000 GC Column Maintenance
58
Columns
58
Conditioning Columns
59
Tips and Hints
59
To Replace an Intuvo GC Column
61
To Replace an Intuvo 9000 GC Gasket
65
To Install a Column Guard or Jumper Chip
66
To Replace the 9000 GC/MS Tail
70
To Condition an Intuvo Capillary Column
74
To Install the Interface Tip Seal
76
The GC/MS Interface for a 9000 Series GC
77
4 Operating in EI Mode
80
Operating the MSD from the DS
80
Operating the MSD from the GC Control Panel
81
Configuring the MSD through the Web User Interface (WUI)
85
To Change the Network Settings of the MSD
85
Emodule Mini Display Readout
88
Front Panel Instrument Status LED
88
Before You Turn on the MSD
89
Pumping down
90
Controlling Temperatures
90
Controlling Column Flow
90
Controlling Jetclean Hydrogen Flow
91
Venting the MSD
91
To View MSD Temperature and Vacuum in Manual Tune
93
To Set Monitors for MSD Temperature and Vacuum Status
95
To Set Analyzer Temperatures from the Instrument Control View
98
To Set the Masshunter 7890 GC/MSD Interface Temperature
100
To Monitor High Vacuum Pressure
101
To Tune the MSD in EI Mode
104
To Set the Operation Mode for the Optional Jetclean System
106
To Set the Jetclean Parameters for the Clean Only Mode
107
To Verify EI System Performance
108
To Perform High-Mass Testing
109
To Open the MSD Covers
112
To Vent the MSD
113
To Pumpdown the MSD
116
5 Operating in CI Mode
120
General Guidelines
120
CI Autotune
121
To Operate the CI MSD
123
To Pumpdown the MSD in CI Mode
124
To Set up the Software for CI Operation
125
To Operate the Reagent Gas Flow Control Module
127
To Set up Methane Reagent Gas Flow
130
To Use Other Reagent Gases
132
To Perform a PCI Autotune (Methane Only)
135
To Perform an NCI Autotune (Methane Reagent Gas)
137
To Verify PCI Performance
139
To Verify NCI Performance
140
To Monitor CI Mode High Vacuum Pressure
141
6 General Maintenance
144
Before Starting
144
Electrostatic Discharge
148
Maintaining the Vacuum System
149
Maintaining the Analyzer
150
To Open the Analyzer Chamber
152
To Remove the EI HES
154
To Connect/Disconnect Wiring to the EI HES
156
To Disassemble the EI HES
157
To Clean the EI HES
160
To Assemble the EI HES
163
To Remove the EI HES Filaments
168
To Install the EI HES Filament
170
To Install the EI HES
171
To Remove the EI XTR, SS, or Inert Source
172
To Connect/Disconnect Wiring from the EI XTR, SS, and Inert Sources
173
To Disassemble the EI SS or EI Inert Source
174
To Disassemble the EI XTR Source
177
To Clean an EI XTR, SS, or Inert Source
180
To Assemble an EI SS or Inert Source
185
To Assemble the EI XTR Source
188
To Replace a Filament in an EI XTR, SS, or Inert Source
191
To Install the EI XTR, SS, or Inert Source
193
To Replace the Electron Multiplier Horn
194
To Close the Analyzer Chamber
196
101 CI Maintenance
198
General Information
198
To Set up Your MSD for CI Operation
198
To Switch from the EI HES to the CI Source
199
To Remove the EI HES Radiator
200
To Connect/Disconnect Wiring to the EI HES Radiator
201
To Install the CI Source Radiator
202
To Switch from the CI Source to the EI HES
204
To Remove the CI Source Radiator
206
To Install the EI HES Radiator
208
To Switch from an EI XTR, SS, or Inert Source to the CI Source
209
To Switch from the CI Source to an EI XTR, SS, or Inert Source
210
To Remove the CI Source
211
To Connect/Disconnect Non-HES Model Wiring from the CI Source
212
To Connect/Disconnect EI HES Model Wiring to the CI Source
213
To Disassemble the CI Source
214
To Clean the CI Source
217
To Assemble the CI Source
220
To Remove the CI Source Filament
223
To Install a CI Source Filament
224
To Install the CI Source
225
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Agilent Technologies 5977 MSD Specifications
General
Brand
Agilent Technologies
Model
5977 MSD
Category
Measuring Instruments
Language
English
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