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G1367A
Agilent Technologies G1367A User Manual
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273
Agilen
t 1100
Serie
s We
ll-plate
Sampl
er & M
icro We
ll-p
late Sam
pler
Referen
ce Ma
nual
Agilent T
echnologie
s
9
Specificati
ons
Perf
orm
anc
e S
pec
ific
ati
on
s
274
272
274
Table of Contents
Default Chapter
5
Table of Contents
5
Installing the Sampler
13
Site Requirements
14
Unpacking the Sampler
17
Optimizing the Stack Configuration
20
Installing the Sampler
24
Installing a Thermostatted Sampler
26
Flow Connections to the Sampler
30
Sample Trays
32
List of Recommended Plates and Closing Mat
34
List of Recommended Vials and Caps
36
Configure Well-Plate Types
38
Transporting the Sampler
41
2 Optimizing Performance
43
Optimizing Performance
44
Optimization for Lowest Carry-Over
45
Using the Automated Needle Wash
45
Using the Flush Port
46
Using an Injector Program
47
General Recommendation to Lowest Carry-Over
48
Fast Injection Cycle and Low Delay Volume
49
Overlapped Injection Mode
49
General Recommendations for Fast Injection Cycle Times
50
Precise Injection Volume
51
Draw and Eject Speed
51
Choice of Rotor Seal
53
Choice of Seat Capillary
54
Troubleshooting and Test Functions
56
Overview of the Sampler's Indicators and Test Functions
56
Status Indicators
58
Power Supply Indicator
58
Instrument Status Indicator
59
Error Messages
60
Timeout
61
Shutdown
62
Remote Timeout
63
Synchronization Lost
64
Leak
65
Leak Sensor Open
66
Leak Sensor Short
67
Compensation Sensor Open
68
Compensation Sensor Short
69
Fan Failed
70
Exhaust Fan Failed
71
Front Door Error
72
Side Door Error
73
Arm Movement Failed or Arm Movement Timeout
74
Valve to Bypass Failed
75
Valve to Mainpass Failed
76
Needle Lock Failed
77
Needle to Needle Seat Position
78
Needle Carrier Failed
79
Missing Vial or Missing Wash Vial
80
Initialization Failed
81
Metering Home Failed
82
Motor Temperature
83
Invalid Vial Position
84
Peristaltic Pump Error
85
Vessel or Wash Vessel Error
86
Vessel Stuck to Needle
87
Maintenance Functions
88
Sample Transport Self Alignment
89
Step Commands
90
Troubleshooting
91
Troubleshooting Guide for the Well Plate Sampler G1367A
93
Turn on and Initialization Steps
94
Errors Which May Occur During the Turn on and Initialization Process
95
Instrument Logbook Errors and Step by Step Repair Process
99
Fan Error (Main Fan or Exhaust Fan)
99
Initialization Error
99
Metering Sensor Error
99
Rheodyne Valve Error
100
Needle Lock Error
100
Needle into Seat Error
101
Needle / Seat Error
102
Sample Location Error
103
Needle Centering over the Vial or the Well
104
Repairing the Sampler
106
Introduction into Repairing the Sampler
106
Using the ESD Strap
107
Overview of Main Repair Procedures
108
Simple Repairs
109
Removing the Needle Assembly
110
Installing the Needle Assembly
112
Removing the Needle Carrier Assembly
114
Installing the Needle Carrier Assembly
115
Exchange the Needle Seat Assembly (G1367-87101) on the G1367A/68A Samplers
116
Exchange the Needle Seat ( G1377-87101) on the G1377A/78A Samplers
117
Exchange the Seat Capillary (G1375-87317/G1375-87300) on the G1377A/78A Samplers
118
Stator Face
119
Rotor Seal
120
Metering Seal and Plunger
122
Removing the Loop Capillary
124
Installing the Loop Capillary
126
Peristaltic Pump
128
Interface Board
129
Exchanging Internal Parts
130
Assembling the Main Cover
131
Light Protection Kit Installation
131
Top Cover and Foam
132
Removing the Top Cover and Foam
132
Installing the Top Cover and Foam
132
Transport Assembly
133
Removing the Sample Transport
133
Installing the Sample Transport
133
Sampling Unit
134
Removing the Sampling Unit
134
Installing the Sampling Unit
135
Analytical Head
136
Removing the Analytical Head
136
Installing the Analytical Head
136
Peristaltic Pump Motor
137
Removing the Peristaltic Pump Motor
137
Installing the Peristaltic Pump Motor
138
Injection-Valve Assembly
139
Removing the Injection Valve Assembly
139
Installing the Injection Valve Assembly
140
Metering-Drive Motor and Belt
141
Removing the Metering Drive Motor and Belt
141
Installing the Metering Drive Motor and Belt
142
Needle-Lock Motor and Belt
143
Removing the Needle Lock Motor and Belt
143
Installing the Needle Lock Motor and Belt
143
Main Fan
144
Removing the Main Fan
144
Installing the Main Fan
144
Exhaust Fan
145
Removing the Exhaust Fan
145
Installing the Exhaust Fan
145
MTP Main Board
146
SUD Board
149
SLS Board
151
Power Supply
152
Leak Sensor
154
Replacing the Autosampler Firmware
155
Parts and Materials
157
Sampler Main Assemblies
158
Vial Trays
160
Sampling Unit Assembly
162
Analytical-Head Assembly
165
Injection-Valve Assembly
167
Sheet Metal Kit
169
Cover Parts
170
Foam Parts
171
Power and Status Light Pipes
172
Leak System Parts
173
Well-Plate Sampler Accessory Kit G1367-68705
174
Micro Well-Plate Sampler Accessory Kit G1377-68705
175
Multi-Draw Kit G1313-68711 (Only for G1367A/68A)
176
Well-Plate Sampler Thermostat
177
Cable Overview
178
Analog Cables
180
Remote Cables
183
BCD Cables
188
Auxiliary Cable
191
CAN Cable
192
External Contact Cable
193
RS-232 Cable Kit
194
LAN Cables
195
Introduction to the Well-Plate Sampler
198
Sampling Sequence
200
Injection Sequence
202
Sampling Unit
204
Analytical Head
204
Injection-Valve
205
Needle Flush Station
206
Needle Lock
206
Needle/Sample Transport Assembly
207
Advanced Operating Modes
209
Early Maintenance Feedback (EMF)
211
EMF Counters
211
Using the EMF Counters
212
Setting the EMF Limits
212
Electrical Connections
213
Theory of Operation
215
Autosampler Control and Electronics
216
Position and Movement Sensors
217
Microtiter Plate Board (MTP)
218
Autosampler-Specific Electronics
219
Firmware Description
223
Firmware Updates
224
Optional Interface Boards
225
BCD Board
225
LAN Board
227
Interfaces
228
Analog Signal Output
229
GPIB Interface
229
CAN Interface
229
Remote Interface
230
Rs-232C
231
Setting the 8-Bit Configuration Switch
233
GPIB Default Addresses
234
Communication Settings for RS-232C Communication
235
Forced Cold Start Settings
236
Stay-Resident Settings
237
The Main Power Supply Assembly
238
8 Control Module Screens of the Well-Plate Samplers
241
Major Keys on the Agilent 1100 Control Module
242
Screens Available from the Analysis View
243
Screens Available from the System View
259
9 Specifications
273
Performance Specifications
274
A Safety Information
277
General Safety Information
278
4
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Agilent Technologies G1367A Specifications
General
Brand
Agilent Technologies
Model
G1367A
Category
Laboratory Equipment
Language
English
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