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Agilent Technologies 7890B User Manual

Agilent Technologies 7890B
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Agilent Technologies
Agilent 7890B
Gas Chromatograph
Operation Manual

Table of Contents

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Agilent Technologies 7890B Specifications

General IconGeneral
BrandAgilent Technologies
Model7890B
CategoryLaboratory Equipment
LanguageEnglish

Summary

Introduction to Agilent 7890B GC

Chromatography Using a GC

Explains the fundamental steps of gas chromatography using a GC system.

The Operating Panel

Describes the GC's operating panel: display, status lights, keypad, beeping, and blinking setpoints.

Operating Basics for Agilent 7890B GC

Overview of GC Operations

Outlines the various tasks involved in operating the Agilent 7890B GC.

Instrument Control Methods

Explains GC control via data system or keypad, including method/sequence loading.

Starting Up the GC

Provides step-by-step instructions for starting up the Agilent 7890B GC.

Shutting Down the GC (Short Term)

Details the procedure for safely shutting down the GC for short periods.

Shutting Down the GC (Long Term)

Outlines the steps for a complete shutdown of the GC for extended periods.

Correcting GC Operational Problems

Guides users on identifying and resolving common GC operational issues and fault messages.

Keypad Operation on Agilent 7890B GC

The Run Keys

Explains the function of keys used to start, stop, and prepare the GC for sample runs.

GC Component Keys

Describes keys for setting temperature, pressure, flow, and other operational parameters for GC components.

The Status Key Usage

Details how to use the Status key to view status and customize display order.

The Info Key for Parameter Help

Explains how the Info key provides context-sensitive help for parameters, showing valid ranges or actions.

General Data Entry and Navigation Keys

Covers keys used for inputting data, clearing entries, navigating displays, and making selections.

Supporting Keys for GC Operation

Describes keys for time display, post-run programming, accessing logs, options, and configuration.

Method Storage and Automation Keys

Explains keys for loading/storing methods and sequences locally on the GC for automation.

Keypad Control with Agilent Data System

Outlines how the keypad functions for status viewing and basic operations when an external data system controls the GC.

The Service Mode Key

Details the Service Mode key for setup, leak checks, and accessing advanced service settings.

Understanding GC Status Indicators

Explains GC status indicators, including status board LEDs, alert tones, and error conditions.

Accessing GC Logs

Describes access to run, maintenance, and system event logs for operational tracking and GLP support.

Methods and Sequences in GC Operation

What is a GC Method?

Defines a GC method as a set of settings for analyzing a specific sample.

Method Parameters

Lists parameters saved in a method, including temperature programs, gas types, and inlet/detector settings.

Loading GC Methods

Explains the effect of loading active and stored methods on GC setpoints and readiness.

Creating GC Methods

Details the process of creating a GC method by saving setpoints for components.

Understanding GC Sequences

Defines a sequence as a list of samples to be analyzed with associated methods, including priority and post-sequence events.

Creating GC Sequences

Explains how to create sequences, including priority, subsequences, and post-sequence events.

Automating GC Analysis and Development

Describes how data systems automate analysis, method development, and sequence creation via digitized detector output.

Running GC Methods and Sequences via Keypad

Running GC Methods from Keypad

Explains how to load, run, and abort methods using the GC keypad, including manual and ALS injections.

Running GC Sequences from Keypad

Details how to load, start, pause, stop, and abort sequences using the GC keypad.

Agilent GC Chromatographic Checkout Procedures

About Chromatographic Checkout

Provides an overview of tests to confirm GC and detector performance against factory standards.

Preparing for GC Chromatographic Checkout

Lists recommended parts and preparation steps for performing checkout tests on inlets and consumables.

Checking FID Detector Performance

Details the procedure for verifying the performance of the Flame Ionization Detector (FID), including baseline output.

Checking TCD Detector Performance

Outlines the steps for checking the performance of the Thermal Conductivity Detector (TCD), including baseline output.

Checking NPD Detector Performance

Provides instructions for verifying the performance of the Nitrogen Phosphorus Detector (NPD), including output specifications.

Checking uECD Detector Performance

Describes the procedure for checking the performance of the Ultra-electron Capture Detector (uECD), including baseline output.

Checking FPD+ Performance (Sample 5188-5953)

Details checking FPD+ performance for phosphorus and sulfur using a specific sample and related filters.

Checking FPD+ Performance (Sample 5188-5245, Japan)

Covers FPD+ performance checks for phosphorus and sulfur with a Japanese sample and related filters.

Checking FPD Performance (Sample 5188-5953)

Outlines FPD performance checks for phosphorus and sulfur using a specific sample and related filters.

Checking FPD Performance (Sample 5188-5245, Japan)

Details FPD performance checks for phosphorus and sulfur with a Japanese sample and related filters.

Agilent GC Resource Conservation

Resource Conservation Overview

Explains how the GC uses an instrument schedule to conserve resources like electricity and gases.

Creating Sleep Methods

Describes creating sleep methods to reduce gas and power usage during inactive periods, considering detectors and columns.

Wake and Condition Methods

Details methods for waking the GC from sleep or conditioning it for operation, specifying restore options.

Setting Up the GC for Resource Conservation

Guides on creating and using an Instrument Schedule for resource conservation, including wake/condition choices.

Editing the GC Instrument Schedule

Explains how to edit, delete, or add items to the GC's instrument schedule for automated operations.

Creating or Editing Sleep, Wake, or Condition Methods

Provides steps for creating or modifying sleep, wake, and condition methods, noting parameter limitations.

Manually Putting the GC to Sleep

Instructs on how to manually put the GC into a low-power sleep state via the instrument schedule.

Waking the GC from Sleep

Explains the options for waking the GC from a sleep state, including restoring methods or running condition methods.

Early Maintenance Feedback (EMF) on Agilent GC

Early Maintenance Feedback (EMF) Overview

Introduces EMF counters for tracking consumable usage and maintenance needs to prevent performance degradation.

GC EMF Counter Types

Differentiates between injection and time-based counters for GC components and their tracking logic.

EMF Counter Thresholds

Explains the two warning thresholds (Service Due, Service Warning) for EMF counters and their independent setting.

Default EMF Counter Thresholds

Describes using default thresholds as a starting point for EMF counter settings and adjusting them based on application.

Available EMF Counters for GC Components

Lists common EMF counters available for various GC components and parts, noting variability based on installed options.

Enabling or Changing EMF Counter Limits

Guides on enabling or modifying limits for EMF counters using the GC keypad and selecting threshold values.

Disabling an EMF Counter

Provides steps to disable specific EMF counters on the GC by setting their thresholds to 'Off'.

Resetting an EMF Counter

Explains how to reset an EMF counter to zero after maintenance or when a Service Due threshold is passed.

EMF Counters for Autosamplers

Details EMF counter functionality for Agilent autosampler systems, depending on model and firmware version.

EMF Counters for MS Instruments

Explains how EMF counters are tracked by the GC or the MS itself when connected to an MS instrument.

GC-MS Features and Communications

GC-MS Communications Overview

Describes how the GC and MS instrument communicate and interact, focusing on venting and shutdown events.

Venting the MSD

Explains the process and GC behavior during MSD venting, including flow adjustments and state management.

MS Shutdown Events

Lists events that trigger an MS shutdown in the GC and the GC's response, such as aborting runs and setting temperatures.

Setting Up an MS Vent Method

Details creating a specific method for safely venting the Mass Spectrometer, including temperature and flow settings.

Manually Preparing GC for MS Venting

Explains how to manually load the MS Vent method for preparing the GC for venting.

Manually Exiting MS Vent State

Provides instructions for exiting the MS Vent state manually, with CAUTIONary notes on flow settings.

Using GC When MSD is Shut Down

Guides on using the GC when the MSD is offline for maintenance or repair, including disabling communications.

Enabling or Disabling MS Communications

Explains how to control communication between the GC and the MS via the Aux Det settings.

Configuration of Agilent 7890B GC Components

About GC Configuration

Introduces the two-part configuration process for GC accessory devices: assigning resources and setting properties.

Assigning GC Resources to Devices

Details assigning power and communication resources to GC accessory devices, changing their state from Unconfigured to Configured.

Setting Configuration Properties

Explains how to set constant hardware setup properties for configured devices, like gas type and temperature limits.

General Configuration Topics

Covers unlocking GC configuration and the Ignore Ready parameter for readiness determination.

Configuring the GC Oven

Describes oven parameters like temperature limits, equilibration time, cryo cooling, and slow cool down modes.

Configuring Front and Back Inlets

Covers configuring gas type and coolant settings for front and back inlets, including PTV/COC coolant options.

Configuring GC Columns

Details parameters for defining capillary column properties like length, diameter, film thickness, and inlet/outlet connections.

Configuring Composite Columns

Explains configuring composite columns with multiple segments and heating zones, specifying lengths for each.

Configuring LTM Columns

Describes configuration for Low Thermal Mass (LTM) columns and LTM Series II modules, noting parameter limitations.

Configuring the Cryo Trap

Covers configuration of a cryo trap, including its connection to GC, heater, coolant, and user-configurable parameters.

Configuring Detectors (Front, Back, Aux)

Details configuring makeup/reference gas, lit offset, and FPD heaters for various detectors.

Configuring Analog Outputs

Explains configuring analog output speeds and using the fast peaks feature for detector data output.

Configuring the Valve Box

Covers assigning GC power to valve box heaters and their temperature control configuration.

Configuring Thermal Auxiliaries

Details assigning power to auxiliary thermal zones and configuring specific heater types like MSD, nickel catalyst, and AED.

Configuring PCM Modules (A, B, C)

Explains configuring Pressure Control Modules (PCM), including gas type, mode, and channel settings.

Configuring Aux EPC Pressure Channels

Details assigning GC communication sources to Aux EPC modules and configuring pressure channels with gas types.

Configuring GC Status Displays

Covers the ready/not ready status table and configuring the order of the setpoint status table.

Setting GC Time and Date

Explains setting the GC's time and date, including time zone, and using the stopwatch function.

Configuring GC Valves

Details configuring valves, including sampling, switching, multiposition types, and remote start options.

Configuring Injectors (Front/Back)

Covers sampler recognition and configuration for 7693A, 7650A, and 7683 ALS systems, including tower positions.

Configuring the 7683 ALS Sample Tray

Explains configuring the 7683 ALS sample tray, including grip offset and barcode reader settings for data input.

Instrument Configuration Settings

Covers instrument serial number entry, auto prep run, zeroing data files, and host connection requirements for readiness.

Using the Optional Barcode Reader

Describes using barcode readers for inputting configuration data, their power, installation, and scanning procedures.

Options for Agilent GC Customization

About GC Options Menu

Introduces the Options menu for functions usually set on installation and seldom changed afterward.

GC Calibration Procedures

Explains calibration procedures for EPC modules, flow/pressure sensors, columns, and other GC components.

Configuring GC Communication (IP Address)

Details configuring the GC's IP address for network (LAN) operation, including DHCP and manual IP settings.

Keyboard and Display Settings

Covers keyboard lock, key click, warning beeps, radix type, display saver, and language settings for user interface customization.

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