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Agilent Technologies 7890 Series User Manual

Agilent Technologies 7890 Series
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Agilent Technologies
Agilent 7890 Series
Gas Chromatograph
Advanced Operation Manual

Table of Contents

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Agilent Technologies 7890 Series Specifications

General IconGeneral
BrandAgilent Technologies
Model7890 Series
CategoryLaboratory Equipment
LanguageEnglish

Summary

Agilent 7890 Series Gas Chromatograph

Advanced Operation Manual

The main title of the manual.

Notices

Manual Part Number

Identifies the specific manual part number for this document.

Edition

Lists the publication date and edition of the manual.

Safety Notices

CAUTION

Denotes a hazard that could result in product damage or data loss.

WARNING

Denotes a hazard that could result in personal injury or death.

Firmware Version

3 Inlets

Using Hydrogen

Safety warnings for using hydrogen (H2) as carrier gas.

Inlet Overview

Comparison table of GC inlet types and their characteristics.

Carrier Gas Flow Rates

Recommended carrier gas flow rates for various column sizes.

About Gas Saver

Explanation of the gas saver feature to reduce carrier flow.

Pre Run and Prep Run

Procedure to restore GC setpoints for injection.

About Heaters

Information on GC heater connectors and their locations by module.

About the Split/Splitless Inlet

Description of the Split/Splitless inlet and its operating modes.

Split/Splitless inlet split mode overview

Explanation of the split injection mode and its pneumatics.

Split/Splitless inlet splitless mode overview

Explanation of the splitless injection mode and its pneumatics.

The S/SL inlet pulsed split and splitless modes

Details on pulsed split and splitless modes for the S/SL inlet.

Split/Splitless inlet split mode minimum operating pressures

Minimum recommended inlet total flow and operating pressures for split mode.

Selecting the correct S/SL inlet liner

Guidance on choosing appropriate liners for split and splitless modes.

Vapor Volume Calculator

Tool to determine if a liner is suitable for a method.

Setting parameters for the S/SL split mode

Configuration of parameters for the S/SL inlet in split mode.

Selecting parameters for the S/SL splitless mode

Step-by-step guide for splitless injection parameters.

Setting parameters for the S/SL pulsed modes

Parameters for S/SL pulsed modes.

About the Multimode Inlet

Overview of the Agilent Multimode (MMI) Inlet System and its modes.

Septum tightening (MMI)

Procedure for tightening septum retainer nuts on the MMI inlet.

Heating the MMI

Explanation of MMI temperature programming and additional ramps.

Cooling the MMI

Information on cryogenic cooling options for the MMI inlet.

MMI split mode minimum operating pressures

Minimum recommended inlet total flow and operating pressures for MMI split mode.

Selecting the correct MMI liner

Guidance on choosing appropriate liners for MMI split mode.

MMI split and pulsed split modes

Explanation of MMI split and pulsed split modes.

MMI splitless and pulsed splitless modes

Description of MMI splitless and pulsed splitless modes.

MMI solvent vent mode

Details on using the MMI solvent vent mode for large volume injections.

MMI Direct Mode

Explanation of MMI Direct Mode for on-column like behavior.

To develop a MMI method that uses large volume injection

Recommended procedure to change from splitless to solvent vent mode.

Multiple injections with the MMI

Technique for concentrating analytes using multiple injections with MMI.

About the Cool On-Column Inlet

Introduction to the Cool On-Column Inlet and its benefits.

Retention gaps

Importance of using retention gaps to protect the analytical column.

COC inlet temperature control

Information on CryoBlast and temperature control for COC inlet.

About the PTV Inlet

Overview of the Agilent Programmed Temperature Vaporization (PTV) Inlet System.

PTV sampling heads

Description of available septum and septumless heads for the PTV inlet.

Heating the PTV inlet

Details on PTV temperature programming and additional ramps.

Cooling the PTV inlet

Information on cooling options for the PTV inlet.

PTV inlet split and pulsed split modes

Explanation of PTV split and pulsed split modes.

Setting parameters for split mode operation

Configuration of parameters for PTV split and pulsed split modes.

4 Columns and Oven

About the Oven

General description of the GC oven and its capabilities.

Oven safety

Safety precautions related to opening and operating the oven door.

Configuring the Oven

Steps to set maximum temperature and other oven configuration parameters.

About Oven Temperature Programming

Explanation of oven temperature programming with single and multiple ramps.

About the column modes

Explanation of available column flow and pressure modes.

Backflushing a Column

Explanation of column backflushing, its benefits, and warnings.

Nickel Catalyst Tube

Information about the Nickel Catalyst Tube accessory.

5 Detectors

About Makeup Gas

Explanation of makeup gas usage and modes in GC detectors.

About the FID

Description of the Flame Ionization Detector (FID) operation and components.

About the TCD

Description of the Thermal Conductivity Detector (TCD) operation.

About the uECD

Description of the micro-cell detector (uECD) and its operation.

About the NPD

Overview of the Nitrogen-Phosphorus Detector (NPD) and its features.

About the FPD+

Description of the Flame Photometric Detector Plus (FPD+) operation.

About the FPD

Description of the Flame Photometric Detector (FPD) operation.

7 GC Output Signals

About Signals

Explanation of GC output signals to data handling devices.

Signal Types

Assigning detector signals using Mode/Type and selecting signal types.

Analog Signals

Adjusting analog signal using Zero and Range parameters.

Digital Signals

GC digital outputs to Agilent data systems.

Column Compensation

Correcting for rising baseline in temperature programmed analysis.

8 Auxiliary Devices

About Auxiliary Pressure Control

Explanation of pressure units and control modules (PCM, Aux PCM).

About Aux Thermal Zone Control

Configuration of auxiliary thermal zones for temperature control.

About Cryo Trap Control

Parameters for configuring an auxiliary zone as a cryo trap.

About Auxiliary Detectors

Information on supporting auxiliary detectors like TCD and AIB.

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