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Agilent Technologies 7200 User Manual

Agilent Technologies 7200
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Agilent Technologies
Agilent
7200 Accurate-Mass
Quadrupole
Time-of-Flight GC/MS
System
Operation Manual

Table of Contents

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Agilent Technologies 7200 Specifications

General IconGeneral
BrandAgilent Technologies
Model7200
CategoryLaboratory Equipment
LanguageEnglish

Summary

About This Manual

Introduction

Overview of the manual's structure and purpose.

Installing GC Columns

Procedures for installing GC columns in the system.

Operating in EI Mode

Steps for operating the GC/MS system in EI mode.

Operating in CI Mode

Steps for operating the GC/MS system in CI mode.

Using the Removable Ion Source

Procedures for using the removable ion source feature.

General Maintenance

Routine maintenance tasks and procedures for the GC/MS system.

Introduction

Abbreviations Used

List and definitions of abbreviations used in the manual.

System Overview and Hardware

Description of the Agilent 7200 GC/MS System and its components.

Important Safety Warnings

Critical safety information and warnings for instrument operation.

Safety and Regulatory Information

Conformance to safety standards and regulatory details.

Intended Use and Product Handling

Guidelines for intended use, cleaning, spills, and storage.

Installing GC Columns

GC Column Basics and Conditioning

Column requirements, flow limits, and conditioning procedures.

Preparing a Capillary Column

Steps to prepare a capillary column for installation.

Installing Column in GC Inlet

Procedure to install a capillary column in the GC inlet.

Installing Column in GC/MS Interface

Procedure for connecting a column to the GC/MS interface.

Preparing Column for CFT Fitting

Steps to prepare column ends for CFT fitting.

Operating in Electron Impact (EI) Mode

System Operation via Software

Using MassHunter Workstation for MS operation and control.

GC/MS Interface Operation

Description and function of the GC/MS interface.

Pre-Operation Checks and Startup

Verifying conditions and startup procedures before operating the MS.

Pumping Down and Venting the MS

Procedures for evacuating and safely venting the MS system.

Temperature and Flow Control

Managing MS and GC/MS interface temperatures and gas flows.

Vacuum Pressure Monitoring

Understanding expected vacuum levels and monitoring them.

Setting Analyzer Temperatures

Adjusting MS ion source and quadrupole temperatures.

Calibrating the GC Column

Procedure for calibrating the capillary GC column.

Collision Cell Gas Configuration

Setting up the gas and flow rate for the collision cell.

MS Autotune Procedure

Performing the autotune procedure for EI mode.

Operating in Chemical Ionization (CI) Mode

CI Mode Setup and Operation

Preparations and general procedures for operating the MS in CI mode.

CI GC/MS Interface Specifics

Details of the GC/MS interface for CI operation.

Reagent Gas Handling

Using other reagent gases, flow control module, and setting flow rates.

CI Autotune Procedure

Performing the autotune for CI mode.

Using the Removable Ion Source

Removable Ion Source Overview

Introduction to the RIS feature and its benefits.

Changing the Ion Source

Detailed, step-by-step procedure for changing the ion source.

RIS Probe Extraction Tool Operations

Procedures for installing and removing the RIS probe tool.

Analyzer Chamber Source Handling

Steps for removing the source from the analyzer chamber.

Installing Ion Source in Analyzer

Steps to install the ion source into the analyzer chamber.

General Maintenance

Maintenance Preparation and Safety

Preparatory steps, tools, supplies, and safety warnings for maintenance.

Ion Source Cleaning

Procedures for cleaning the ion source.

Vacuum System Maintenance

Periodic maintenance of vacuum system components.

Analyzer Maintenance

Procedures for maintaining analyzer components.

Disassembling the EI Ion Source

Steps for disassembling the EI ion source.

Assembling the EI Ion Source

Steps for assembling the EI ion source.

Filament Replacement

Procedures for removing and installing filaments.

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