Detectors 5
Advanced Operation Manual 173
Use nitrogen makeup gas (instead of helium) for greater
sensitivity.
Setting parameters for FID
To set the FID parameters:
1 Verify:
• Makeup gas is configured
• Installed jet type is correct for column type
2 Press [Front Det] or [Back Det].
3 Set the detector temperature. The temperature must be
greater than 150 °C for the flame to light.
4 Set the hydrogen flow rate, if desired, and press [Off/No].
5 Change the air flow rate, if desired, and press [Off/No].
6 If using a packed column, set the FID makeup gas to
0.0/Off.
7 If using a defined capillary column, set the makeup gas
flow or combined column plus makeup gas flow.
8 Scroll to Flame and press [On/Yes]. This turns on the air
and hydrogen and initiates the ignition sequence. The
signal typically increases to 5 to 20 pA after ignition.
Verify that the flame is lit by holding a cold, shiny
surface, such as a mirror or chrome- plated wrench, over
the collector exit. Steady condensation indicates that the
flame is lit.
Air 200 to 600 450
* Detector hydrogen is pressure controlled, where the detector provides a known resistance. If using a nickel catalyst tube, the resistance
changes, and the flow rates displayed by the GC will not be accurate. Measure the actual hydrogen flow using a flow meter at the detector
vent, with all other flows turned off.
Tabl e 44 Recommended starting conditions (continued)
Verify that a column is installed or the FID column fitting is
plugged before turning on the air or hydrogen. An explosion may
occur if air and hydrogen are allowed to leak into the oven.
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