A-8
Ver.1.36
3.8.1 Connecting Auto-Shot sampler (AS-1020E) ···································································· 3-6
3.8.2 Connecting other peripheral devices ·············································································· 3-6
3.9 INSTALLING CONTROL SOFTWARE ··················································································· 3-7
3.9.1 Installing USB serial communication device driver ···························································· 3-7
3.9.2 Installing control software ···························································································· 3-8
3.9.3 Setting COM port ······································································································· 3-8
3.10 FRONT, BACK, SIDE, AND TOP VIEWS ············································································· 3-10
3.10.1 Pyrolyzer ················································································································· 3-10
3.10.2 Temperature Controller ······························································································· 3-11
CHAPTER 4 USING CONTROL SOFTWARE ···································································· 4-1
4.1 START UP AND SCREEN LAYOUT ······················································································ 4-1
4.1.1 Starting program ······································································································· 4-1
4.1.2 Screen layout ··········································································································· 4-2
4.2 BEFORE STARTING AN ANALYSIS ····················································································· 4-4
4.2.1 System configuration ·································································································· 4-4
4.2.2 Set-up interface temperature························································································ 4-6
4.3 SET-UP ANALYTICAL MODES AND OPERATION ································································· 4-7
4.3.1 Set-up for Single-Shot analysis and operation procedure ··················································· 4-7
4.3.2 Set-up for Double-Shot analysis and operation procedure ·················································· 4-9
4.3.3 Set-up for Direct EGAt analysis and operation procedure ··················································· 4-12
4.3.4 Set-up for Heart-Cut EGA analysis and operation procedure ·············································· 4-14
4.4 OTHER FUNCTIONS ······································································································· 4-17
4.4.1 Saving/loading analysis set-ups ···················································································· 4-17
4.4.2 Temperature calibration of pyrolyzer furnace and other set-ups ··········································· 4-17
4.4.3 Printing set-ups ········································································································· 4-20
4.4.4 Set-up the Py Conditioning Table ·················································································· 4-20
CHAPTER 5 FOUR ANALYSIS METHODS AND SAMPLE PREPARATION ···························· 5-1
5.1 SINGLE-SHOT ANALYSIS ·································································································· 5-1
5.2 EVOLVED GAS ANALYSIS (EGA) ························································································ 5-3
5.3 DOUBLE-SHOT ANALYSIS ································································································· 5-5
5.4 HEART-CUT ANALYSIS ····································································································· 5-7
5.5 SAMPLE PREPARATIONS ································································································· 5-9
5.6 SELECTION OF SAMPLE CUPS AND STICKS ······································································· 5-11
CHAPTER 6 MAINTENANCE ························································································· 6-1
6.1 ROUTINE MAINTENANCE ·································································································· 6-1
6.1.1 Cleaning sample cups (Eco-cup) ······················································································ 6-1
6.1.2 Replacing and cleaning quartz pyrolysis tube ······································································ 6-3
6.1.3 Interface needle ············································································································ 6-7
6.1.4 GC injection port ··········································································································· 6-8
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