A-7
Ver.1.36
TABLE OF CONTENTS
BEFORE USING THIS PYROLYZER ················································································· A-2
PRODUCT WARRANTY ································································································· A-2
ABOUT PRODUCT SUPPORT PERIOD ············································································ A-2
FOR YOUR SAFETY ······································································································ A-3
CONTENTS IN THE PACKAGE ······················································································· A-5
TABLE OF CONTENTS ·································································································· A-7
CHAPTER 1 ABOUT MULTI-SHOT PYROLYZER ······························································ 1-1
1.1 BACKGROUND OF DEVELOPMENT ···················································································· 1-1
1.2 FEATURES OF EGA/PY-3030D ··························································································· 1-3
1.3 PERIPHEREAL DEVICES ··································································································· 1-4
1.4 SCHEMATIC OF MULTI-SHOT PYROLYZER FURNACE ·························································· 1-5
CHAPTER 2 SPECIFICATIONS ······················································································ 2-1
About cooling time of pyrolyzer furnace ························································································· 2-3
CHAPTER 3 INSTALLATION ························································································· 3-1
3.1 PREPARING INSTALLATION ······························································································ 3-1
3.1.1 Before installation ······································································································ 3-1
3.1.2 Pumping down MS (for saving installation time) ······························································· 3-2
3.2 REPIPING CARRIER GAS LINE ··························································································· 3-2
3.3 SETTING UP GC INJECTION PORT ····················································································· 3-3
3.3.1 Replacing septum nut of GC injection port ······································································ 3-3
3.3.2 Replacing septum ······································································································ 3-3
3.3.3 About injection port liner······························································································ 3-3
3.4 SETTING UP PYROLYZER FURNACE ·················································································· 3-3
3.4.1 Installing quartz pyrolysis tube to pyrolyzer ····································································· 3-3
3.4.2 Attaching interface union and needle ············································································· 3-3
3.4.3 Mounting pyrolyzer on GC ··························································································· 3-3
3.5 CONNECTING TEMPERATURE CONTROLLER ····································································· 3-4
3.5.1 Connecting power cable to outlet ·················································································· 3-4
3.5.2 Connecting to control PC ···························································································· 3-4
3.5.3 Hooking up remote signal cable ···················································································· 3-4
3.6 CONNECTING COOLING GAS LINE ···················································································· 3-4
3.6.1 About cooling gas ······································································································ 3-4
3.6.2 Connecting temperature controller and pyrolyzer······························································ 3-4
3.7 CONNECTING FURNACE PURGE GAS TUBE ······································································· 3-5
3.7.1 When He or N2 is used as a carrier gas ········································································· 3-5
3.8 INSTALLING PERIPHERAL DEVICES ··················································································· 3-6
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