What to do if I see no peaks with my Frontier EGA/PY-3030D?
If you observe no peaks, there might be a gas leak. Inspect the joints between the column and the GC injection port, and replace the septum. Alternatively, there may be no signal from the GC detector, in which case you should consult your GC operation manual. Another possibility is that the ITF needle is clogged; inspect it and replace it if necessary.
Why are the peaks broad on my Frontier EGA/PY-3030D Industrial Equipment?
Broad peaks can occur due to a degraded column; if this is the case, replace the column. It could also be caused by abnormal diffusion from the pyrolyzer furnace up to the column inlet, in this case, raise the split ratio. If the pyrolysis temperature is too low, increase it by 100ºC.
What to do if the Frontier EGA/PY-3030D Industrial Equipment furnace will not heat?
If the furnace will not heat, first ensure that the heater setting is ON by checking the furnace box in the configuration software. If the heater setting is already ON, check if the breaker is off and reset the main breaker on the rear panel of the controller.
Why is there peak tailing in my Frontier EGA/PY-3030D Industrial Equipment?
Peak tailing can be caused by a degraded column, in which case you should replace it. It could also be due to abnormal diffusion from the pyrolyzer furnace up to the column inlet; increase the split vent flow. If the pyrolysis temperature is too low, increase the pyrolysis temperature by 100ºC.
What causes poor reproducibility of pyrograms in Frontier Industrial Equipment?
Poor reproducibility of pyrograms can be attributed to several factors. There may be a gas leak, check section 7.3 for details. Ensure the pyrolysis temperature is properly set (set furnace 50ºC higher than end temperature observed in EGA thermogram). Also, make sure the sample amount and shape are uniform. Depending on samples, good reproducibility may not be obtained. If the problem persists, check the system with polystyrene standard.
What to do if I have low recovery of high boiling compounds and peak tailing with Frontier EGA/PY-3030D Industrial Equipment?
If you're experiencing low recovery and peak tailing of high boiling compounds, the ITF and injector temperature may be too low. Increase the temperature, for example, from 200ºC to 300ºC. Do not set GC injector temperature over 350ºC unless absolutely necessary. Also, if using GC/MS, the ITF temperature may be too low, increase the temperature.
What does it mean if my Frontier EGA/PY-3030D Industrial Equipment is making a beep sound?
A beep sound indicates that the sensor cable is either not connected or there is a contact failure. Ensure the cable from the pyrolyzer is properly connected to the connector labeled POWER, SENSOR at the rear of the controller. It can also mean sensor failure that needs repair.
Why is there abnormal temperature with my Frontier Industrial Equipment?
Abnormal temperature can be due to sensor contact failure. Check to see if the sensor cable from the pyrolyzer is properly connected. It could also be an error in temperature calibration, in this case, redo the calibration. Sensor circuit failure may also be the cause, that needs repair.
What causes abnormal ghost peaks in the high temperature region of my Frontier EGA/PY-3030D?
Abnormal ghost peaks in the high-temperature region may occur because not all pyrolyzates have eluted from the column. Use a Selective Sampler to prevent high boiling compounds from getting into the column. Use a high-temperature resistant column and bake the column after each run. Another cause could be septum debris in the insert liner, so clean the insert liner. Lastly, the pyrolysis tube might be contaminated; see section 6.1.2 for details.
What to do if the cooling fan is not running on my Frontier Industrial Equipment?
If the cooling fan is not running, first make sure it is not blocked by a foreign object or gas tubing. If it is not blocked, fan failure may be the cause, that needs repair. Check that the fan power cable is properly connected, if it is, repair is needed.
General| Brand | Frontier |
|---|---|
| Model | EGA/PY-3030D |
| Category | Industrial Equipment |
| Language | English |
Defines warning symbols and signal words used in the manual and product.
Explains the historical context and evolution of Py-GC technology.
Summarizes the key features and capabilities of the EGA/PY-3030D pyrolyzer.
Lists and describes peripheral devices that expand the system's analytical capabilities.
Provides a diagram illustrating the components of the multi-shot pyrolyzer furnace.
Details guaranteed performance metrics for analytical conditions, including reproducibility.
Describes specifications for the pyrolyzer furnace, sampling, interface, and samplers.
Lists functions and specifications of the temperature controller unit.
Lists standard accessories included with the pyrolyzer system.
Provides specifications for power, dimensions, and recommended GC/MS systems.
Lists optional peripheral devices, consumables, and accessories available for the system.
Outlines necessary items and preparations before installing the pyrolyzer.
Explains how to redirect the carrier gas line for pyrolyzer installation.
Details the procedure for setting up the GC injection port for pyrolyzer interface.
Guides on installing the quartz pyrolysis tube and interface components.
Instructions for connecting the temperature controller to the PC and GC.
Describes how to connect the cooling gas line for the pyrolyzer.
Explains the connection of the furnace purge gas tube for oxidation protection.
Guides on connecting optional peripheral devices to the temperature controller.
Details the process of installing the USB driver and control software.
Provides views and labels of the pyrolyzer and temperature controller panels.
Explains how to start the software and describes the screen layout and elements.
Covers system configuration and setting up accessory devices before analysis.
Details setup procedures for Single-Shot, Double-Shot, EGA, and Heart-Cut analyses.
Describes saving/loading set-ups, temperature calibration, and printing options.
Describes the single-shot analysis method, instrument configuration, and sample prep.
Explains EGA, its instrument configuration, and analysis example.
Details the double-shot analysis method, including thermal desorption and pyrolysis.
Describes the heart-cut EGA technique, instrument setup, and analysis example.
Provides guidance on preparing samples for analysis, including safety precautions.
Lists and describes various sample cups and sticks for different analytical purposes.
Covers cleaning of sample cups, pyrolysis tubes, and interface needles.
Details periodic maintenance for the pyrolyzer furnace, GC injection port, and controller.
Lists symptoms, causes, and solutions for pyrolyzer furnace issues.
Lists symptoms, causes, and solutions for temperature controller problems.
Provides procedures for common issues like gas leaks and needle clogging.
Lists error codes from the control software and their possible solutions.
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